Znorg. Chem. 1991, 30, 1157-1 159
Mo-Mo' Mo-Br( 1) Mo-Br(2) Mo-S Mo-S' Mo-O PC(1I) PC(21) PC(31) PC(41) C(1 1 ) C ( 12)
2.857 (2) 2.610 (2) 2.616 (3j 2.279 (5) 2.259 (5) 1.67 (1) 1.88 (2) 1.75 (3) 1.77 (2) 1.82 (2) 1.44 (4)
C(I2)C(13) C(13)C(14) c(21 j c ( 2 2 j C(22)C(23) C(23)C(24) C( 3 1)C(32) C( 3 2 ) C ( 33) C( 33)-c( 34) C( 4 1) C ( 4 2 ) C(42)C(42)'
1.54 (3) 1.36 16) 1.29 (3j 1.50 (4) 1.40 (4) 1.50 (3) 1.52 (4) 1.44 (4) 1.54 (2) 1.49 (2)
Mo'-Mo-Br( 1) Mo'-MO-Br( 2) Mo'-Mo-S Mo'-Mo-S' Mo'-Mo-O Br( I )-Mo-Br( 2) Br( I)-Mo-S Br( 1 )-Mo-S' Br( 1)-Mo-O Br(Z)-Mo-S Br(Z)-Mo-S' Br(Z)-Mo-O S-Mo-S' S-Mo-O S'-Mo-O MbS-Mo' C(ll)-P-C(2I)
130.23 (7) 127.78 (7) 50.7 ( I ) 51.3 ( I ) 102.7 (6) 79.41 (8) 147.5 (2) 81.0 ( I ) 104.9 (5) 80.9 (1) 141.4 (2) 109.3 (7) 99.2 (2) 105.9 (5) 107.7 (7) 78.0 (2) 107 ( I )
C(1 l)-PC(31) C(Il)-P-C(41) C(2 1)-PC(3 1) C( 2 I)-P-c(41) C(3I)-P
