1,4-Bismethanesulfonates of the Stereoisomeric ... - ACS Publications

1,4-Bismethanesulfonates of the Stereoisomeric Butanetetraols and Related Compounds. Peter W. Feit. J. Med. Chem. , 1964, 7 (1), pp 14–17. DOI: 10.1...
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14

1’ETE:H

\+-:istre:ited with lithium duriiiniirii hj-dride in the presence ~l

c.hloride to maintain acidity. Iluring the decornposition i ) f t h e hydride complex tlie pH of the solution was never : 1 l l c i w d t ~ rise i above 5. The product, isolated by continuous rstmction rsith ethyl acetate, x a s S7 mg. of 6-meth.r.lthiopurine. :hniiiiirii

I\-. I