MEETINGS
24th ACS Middle Atlantic Regional Meeting The 24th ACS Middle Atlantic Regional Meeting will be held May 23-25 on the Madison Campus of Fairleigh Dickinson University in suburban Morristown, N.J., within a short commuting distance from New York City. It will be hosted by the ACS North Jersey Section. The formal program consists of some 250 papers, including symposia featuring invited speakers, contributed general and poster presentations, free tutorials, workshops, two awards symposia—the student undergraduate award and the research in chromatography award—and the awards presentation dinner. Bassam Shakhashiri of the National Science Foundation will deliver the awards dinner address, "Communicating Science." There will be 19 organized symposia in analytical chemistry, biochemistry, chemical education, and inorganic, medicinal, organic, physical, and polymer chemistry. These symposia will cover the specific topics of spectroscopic analysis, analytical pharmaceutical chemistry, drug metabolism, protein chemistry, advances in biotechnology, precollege and college chemical education, solid-state inorganic chemistry, coordination chemistry/organometallics, computer modeling and drug design, organometallics for organic synthesis, new organic synthetic methods, photochemistry and spectroscopy, functional polymers, polymer recycling, polymer rheology, degradable plastics, and polymer blends. In addition, two conferences, the Chromatography Topical Group and the Teachers Affiliates Conference, will be held. A special interest symposium, organized by Ned D. Heindel with eight invited speakers, will discuss "Life after the Big Company: Post-Retirement Opportunities for Chemists." Free tutorials in polymer chemistry, polymer characterization and properties, controlled drug delivery, computer-aided experimental design, microscale laboratory, and employment strategies will be conducted for applicants by special reservation. Three workshops on career planning, scientific writing, and laboratory safety will be available by advance
SPECIAL EVENTS
TUESDAY 5:00-8:00 PM—Meeting Registration, Recreation Building 6:30-8:30 PM—Wine and Cheese Reception, Recreation Building
WEDNESDAY 8:00 AM-5:00 PM—Meeting Registration, Recreation Building 8:30 AM—Opening Ceremony, R. Donaldson, president, Fairleigh Dickinson University, Dreyfuss Building Main Auditorium 9:00 AM-5:00 PM—ACS National Employment Clearing House, Student Center Conference Room 9:00 AM-5:00 PM—Chemistry/Instruments Exhibit, Recreation Building 9:00 AM-5:00 PM—Art Exhibit, Recreation Building
12:30 PM—Women Chemists Luncheon, Student Center Raingarden 9:00 AM-5:00 PM—Conference: Chromatography Topical Group, Second Floor Dreyfuss Buidling Auditorium A, B, and C B. McPherson, C Ace 9:00 AM-noon—Tutorial: Life after the Big Company: Post-Retirement Options for Chemists, Dreyfuss Building, Room 212. N. Heindel, F. Dammont 2:00-5:00 PM—Tutorial: Employment Strategies, Dreyfuss Building, Room 212. T. Connors, C Ace 9:00 AM—5:00 PM—Tutorial: ComputerAided Experimental Design, Dreyfuss Building, Room 211. R. Strange 11:00 AM-2:00 PM—Poster Sessions. Recreation Building 8:30 AM-3:30 PM—Workshop: Laboratory Safety, Science Building Auditorium S-11. J. Kaufman, F. Dammont 9:00 AM-5:00 PM—Workshop: Scientific Writing, Friendship Library. J. Brown 5:30 PM—Jersey BBQ, Picnic Grounds
registration (see registration form on page 50). For additional information about the laboratory safety workshop contact James Kaufman, (617) 237-1335. A chemistry/instruments exhibit and art exhibit will be held Wednesday and Thursday from 9 AM to 5 PM in the Exhibit Hall, Recreation Building. The art exhibit will be hung on the walls of the Exhibit Hall in the Recreation Building. The Employment and Career Services Office of ACS will hold a National Employment Clearing House (NECH) during the meeting. Registration will be held Tuesday, May 22, from 5 to 8 PM in the general registration area. NECH will be open from 8 AM to 5 PM Wednesday, May 23, and Thursday, May 24, and from 8 AM to noon on Friday, May 25. For candidate or employer registration forms, call John Michael Sophos toll free at (800) 227-5558 or write to Employment & Career Services Office, ACS, 1155—16th St., N.W., Washington, D.C. 20036. A free, informal wine and cheese party for early arrivals, a "Jersey Barbeque," and the Women Chemists Luncheon will round out the special programs. Meeting participants are encouraged to register in advance (see form on page 50). On-site registration facilities will be open on Tuesday, May 22, preceding the meeting, in the afternoon and evening, from 8 AM to 5 PM on Wednesday and Thursday, and from 8 to 10 AM on Friday. Meeting and most other information on local points of interest, restaurants, and visits to New York City will be provided at the courtesy desks. On-campus dormitory housing is available. Reservations should be made in advance using the form on page 50. Hotel accommodations must be made directly with the hotel (see listing of hotels and motels on the registration form). For additional information on MARM call the following committee members: general chairman, R. W. J. Carney, (201) 277-5492; program chairman, S. W. Shalaby, (201) 218-3078. THURSDAY 8:00 AM-5:00 PM—Meeting Registration, Recreation Building 9:00 AM-5:00 PM—ACS National Employment Clearing House, Student Center Conference Room 9:00 AM-5:00 PM—Chemistry/Instruments Exhibit, Recreation Building 9:00 AM-5:00 PM—Art Exhibit, Recreation Building 9:00 AM-5:00 PM—Tutorial: Polymer Chemistry, Dreyfuss Building, SecondFloor Auditorium A. E. M. Pearce, D. Lohse 9:00 AM-5:00 PM—Tutorial: Microscale Laboratory, Science Building S-4. R. M. Pike, M. J. Smith 11:00 AM-2:00 PM—Poster Sessions. Recreation Building 2:00-5:00 PM—Workshop: Career Planning, Friendship Library. J. Brown 1:00-3:00 PM—MARM Steering Committee Meeting, Dreyfuss Building, Room 214
3:00-5:00 PM—MARM Local Section Officers/Councilors Meeting, Dreyfuss Building, Room 214 7:00 PM—Awards Banquet, B. Shakhashiri, speaker, Madison Hotel
FRIDAY 8:00 AM-10:00 AM—Meeting Registration, Recreation Building 9:00 AM-noon—ACS National Employment Clearing House, Student Center Conference Room 9:00 AM-noon—Tutorial: Polymer Characterization and Properties, Dreyfuss Building, Second-Floor Auditorium A. T. K. Kwle, K. Levon, D. Lohse 9:00 AM-noon—Tutorial: Controlled Drug Delivery, Dreyfuss Building, Second-Floor Auditorium B. Y. Chien, C. Town 9:00 AM-noon—Workshop: Career Planning, Friendship Library. J. Brown 9:00 AM-noon—Workshops: Beilstein Database, Dreyfuss Building, Room 107. I. R. Baylouny
March 26, 1990 C&EN
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Meetings
ANALYTICAL C. Ace, A. Greenberg, Chairmen WEDNESDAY AFTERNOON
3:25—19. Drug Assay Development. XXIII. Simultaneous Assay for Cocaine(C), Norcocaine(NC), Benzoylecgonine(BE) and Ecgonine Methyl Ester(EME) in Human Biofluids by GC/MS. T. Magulre, W. D. Darwin, E. J. Cone 3:45—20. Drug Assay Development. XXIV. Determination of Cocaine in Air by Capillary Gas Chromatography/Mass Spectrometry. D. Yousefnejad, E. J. Cone
Dreyfuss Building, Room 101 Spectroscopic Analysis
C. L. Ace, Presiding 2:00—1. Use of NMR Shift Reagents in the Simultaneous Detection of Optical Isomers and the Separation of Overlapping Resonances. M. L. Lau, A. L. Cholli 2:20—2. Structural and Dynamic Aspects of Novel Bromide Spiro-Enamino Ketals. A. L. Cholli, M. L. Lau, K. Gala 2:40—3. Quantitative Interproton Distance Measurements by Nuclear Magnetic Resonance. Tze-MIng Chan, D. C. Galgarno, R. M. Osterman, C. A. Evans 3:00—4. 1H NMR Study of Substituted 2,3Diphenylthiazolidin-4-Ones. J. Tlerney, M. McCoy 3:30—5. Identification of Contaminants in Recycled Process Gas by GC/MS. K. Bachour, A. Cheng, P. Albright, S. Jones, L. Gorman 3:50—6. Characterization of Polyimide Thin Films by Pyrolysis Mass Spectrometry. E. R. Johnson, B. J. Bachmann 4:10—7. Unsubstituted Polyaromatic Hydrocarbons (PAHs) in Extracts of Coal Fly Ash. M. D. Applequist
THURSDAY MORNING Dreyfuss Building, Room 101 Contemporary Topics
S. Mookherjea, Presiding 9:00—8. Contemporary Topics in Analytical Chemistry. F. Zahne 9:45—9. Clay Minerals. M. Woomer, R. Parmely, D. Wampler, P. Schettler, J. Curtis, T. Watson 10:00—10. Fractionation. S. Finklestine, S. Croyle, R. Parmely, P. Schettler 10:20—11. 4,4'-Bis(Dimethylamino)Thiobenzophenone as a Potential Mustard and Lewisite Sensing Coating for OpticalBased Microsensors. T. J. Novak, V. D. Henderson, J. A. Parsons 10:40—12. Square-Wave Voltammetry of Selected Neurotransmitters on Graphite Fiber Microelectrodes. M. Wojclechowski, K. M. Chlada 11:00—13. Environmental Weathering of Activated Carbon: Spectroscopic Examination of Metal Impregnants. L. Isaacson, R. Lamontagne, E. Petersen, J. Rossln 11:20—14. Chemical Shift in Auger Electron Spectroscopy. R. L. Oplla 11:40—15. Scanning Tunneling Microscopy To Characterize and Modify Surfaces. E. Garfunkel THURSDAY AFTERNOON Dreyfuss Building, Room 101 Pharmaceutical Analysis A. Greenberg, Presiding 2:00—16. Pharmaceutical Analysis. P. Lane 2:45—17. Drug/Assay Development. XXI. Solid-Phase Extraction (SPE) of Buprenorphine from Human Biofluids. W. D. Darwin, E. J. Cone 3:05—18. Drug Assay Development. XXII. Evaluation of the Abuscreen Ontrak Assay for Qualitative Detection of Cocaine Metabolite in Human Urine. S. L. Dlckerson, E. J. Cone
BIOCHEMISTRY C. Town, Chairman
Dreyfuss Building, Room 103 Biological Chemistry
C. Town, Presiding 2:00—Remarks by Chairman 2:10—21. Soybean Lipoxygenase Cofactors Iron and PQQ. D. M. Calderone, M. J. Gibian, M. Petersheim 2:30—22. Anion Control of a Dehydrogenase Reaction. L. Liu, W. P. Huskey 2:50—23. Surface-Modified Amperometric Biosensors. A. M. Yacynych, R. J. Geise, E. R. Reynolds 3:30—24. Biosynthesis of Unusual Polyamides Containing Glutamic Acid. S. A. Giannos, D. L. Kaplan, R. A. Gross 3:50—25. Energy Coupling in the Mechanism of Nicotinic Acid Phosphoribosyltransferase from Salmonella typhimurIum. A. VlnHsky, C. T. Grubmeyer 4:10—26. Preliminary Findings on Yeast Tolerance to 1 M Ca 2 + . S. LI, M. Petersheim, D. Burke 4:30—27. Biodegradation of Polymers Using Free and Immobilized Microorganisms. S. S. Cofer, S. S. Godbole, J. T. Jung, B. S. Sanji
Science Building S-10, S-11 General Papers E. J . Colicelli, Presiding 2:00—54. Chemistry of Photography and Its Place in the Chemistry Curriculum. (Class Demonstrations). D. T. Lee 3:15—55. ICE Laboratory Leadership Program. A. Johnson 4:15—56. New Jersey Core Course Proficiencies in Science. D. H. Cook
INORGANIC M. DiGiussepe, Chairman
CHEMICAL EDUCATION M. J. Smith, Chairman
Dreyfuss Building, Room 105 General Papers R. Tomkins, Presiding 9:00—40. Youth in Engineering and Science Program. N. M. Tooney, S. McRae, J. Conti 9:25—41. Partners in Science—a Summer Internship for High School Students. D. Levlne 9:50—42. Secondary Students Experience Science in College. M. L. Maler 10:15—43. Program for Access to Science Study (PASS). M. Welner, M. Roth 10:50—44. General Chemistry Problem Solving: Memorizing or Thinking? G. J. Beichl 11:15—45. Applied Chemistry Misconceptions That Survive the General Chemistry Course. J. W. Judklns
Dreyfuss Building, Room 103
WEDNESDAY AFTERNOON
Protein Chemistry
Dreyfuss Building, Room 105
M. Sardana, Presiding
General Papers
9:00—Introductory Remarks 9:10—28. Observation of Thiamin Diphosphate and Intermediates Bound to it on Pyruvate Decarboxylase. S. Menon-Rudolph, J. Cheng, F. Jordan 9:30—29. Preliminary Crystallographic Data for Brewer's Yeast Pyruvate Decarboxylase in the a 4 Homotetrameric Form. B. Farrenkopf, F. Jordan, F. Dyda, W. Furey, S. Swaminathan, M. Sax 9:50—30. Purification of Organophosphorus Acid Hycholase from Halophile Bacteria. B. Dhingra, L. H. Walls 10:30—31. Staining Techniques for Gycoproteins after Polyacrylamide Slab Gel Electrophoresis. B. C. Sullivan, J. J. Basch, E. L Malin 10:50—32. Folding of Denatured Subtilisins with the Aid of Exogenous Pro-Subtilisin and Synthetic Pro-Peptides. Z. Zhu, P. W. Cash, F. Jordan, M. Inouye 11:10—33. Calculation of Atomic Charges in Charged Molecules Using a Simple Orbital Electronegativity Method. J. Mullay
THURSDAY AFTERNOON Dreyfuss Building, Room 103 Drug Metabolism
THURSDAY MORNING Dreyfuss Building, Room 106 Solid-State Chemistry
WEDNESDAY MORNING
THURSDAY MORNING
W. A. Garland, W. M. Levin, Presiding
March 26, 1990 C&EN
THURSDAY AFTERNOON
WEDNESDAY AFTERNOON
2:00—34. Distribution of 1-Amino-benzotriazol in Male Rats after Administration of a 100 mg/kg Oral Dose. L. Henderson, W. Garland, M. Mortillo and C. Town
48
2:30—35. Determination of 14C-Acitretin and Its Metabolites in Human Plasma. F. Rubio, L. Henderson, W. A. Garland, A. Szuna, C. Town 2:50—36. Characteristics of Immobilized Hog Liver Microsomal Biocatalyst in Chlorpromazine-N-Oxide Preparation. I. Valvis, D. Lischick, D. Shen, S. S. Sofer 3:30—37. In-Vitro Synthesis of Nitroxide Free Radicals by Liver Microsomes. S. S. Sofer, D. Shen, I. Valvis, D. Lischick 3:50—38. Quantitation of the Enantiomers of Rimantadine and Its Hydroxylated Metabolites in Plasma by GC-MS. P. P. Davis, N. Choma, E. K. Fukuda 4:10—39. Quantification of Endogenous Retinoic Acid in Human Plasma. C. A. Huselton, B. E. Fayer, W. A. Garland, D. J. Liberato
M. J. Smith, Presiding 2:00—46. Banning Laboratory Textbooks in the Organic Laboratory: an Approach to Developing Organization Skills. E. J. Colicelli 2:25—47. Chemistry and Industry—a New Course for Students Majoring in Business and Business-Related Subjects. G. MHra 2:50—48. Use of Interfacing Software in Relaxation Kinetics Laboratory. G. W. Simmons, S. A. Robertson, D. Zeroka, and J. E. Sturm 3:20—49. NSF's Plans for Undergraduate Education. R. F. Watson 3:55—50. Instrument and Laboratory Improvement Program at NSF. N. M. Roscher 4:25—51. Undergraduate Faculty Enhancement Program at NSF. N. M. Roscher
THURSDAY MORNING Science Building S-10, S-11 General Papers
B. Finn, Presiding 9:00—52. Mastering Thermochemical Concepts. (Class Demonstrations). A. C. Breyer 10:45—53. A College's View of High School Chemistry Preparation. M. Pearsall
D. N. Buckley, M. Greenblatt, Presiding 9:00—57. Metallic Hydrides: Fundamental Properties and Energy-Related Applications. G. G. Llbowitz 9:45—58. Structural and Transport Properties of Tl^PbxSrjjCuOs (0.0 < x < 0.50). M.-H. Pan, M. Greenblatt 10:05—59. Synthesis and Characterization of Pb2Sr2-xMo.5+xCao.5Cu308+d- E. A. Hayrl, J. Z. Larese 10:35—60. Synthesis and Properties of Bi 2 - x Pb x + Xa n _ iCun04+2n+«(n = 1,2, and 3; x < 0.3, and y < 0.15). H. T. Shlh, M. Greenblatt 10:50—61. Synthesis, Transport, and Microstructural Properties of Nd185Ceo.i5CuO4-5. J.-G. Lee, K. V. Ramanujachary, M. Greenblatt 11:10—62. Studies of Oxides, Carbonates, and Sulfates as Iron Corrosion Products Using the Laser Raman Microprobe. R. G. Herman, C. E. Bogdan, A. J. Sommer 11:30—63. Reactions of Size-Selected Silicon Clusters, Sin + With 0 2 . U. Ray, K. M. Creegan, M. F. Jarrold
THURSDAY AFTERNOON Dreyfuss Building, Room 106 Coordination/Organometallic Chemistry
H. Murray, T. X. Neenan, Presiding 2:00—64. Cyclohexadienyl Acylmetallates of Manganese and Their Application to the Synthesis of Cyclohexadienes from Arenes. J. B. Sheridan, R. S. Padda 2:20—65. Cyclopentadienyl Manganese Dicarbonyl n3-Allyl Cations: Electrophilicity and Acidity. A. M. Rosan, C. Cavallaro, E. Cordova 2:40—66. 7rans-bis(5-acyloxy-1,2,3-773-cyclohexenyl)palladium Complexes by Palladium(ll)-Promoted Addition of Acylates to 1,4-Cyclohexadienes. Y.-H. Chen, W. A. Metz, B. C. Soderberg, B. Akermark, S. S.Hall 2:45—67. Chemistry of Mono- and Bimetallic Polypyridyl Complexes. D. L. Carlson, J. A. Baiano, W. R. Murphy 3:20—68. Synthesis, Properties, and Substitution Reactions of [Ru(PdtoXCI)(CH3CN)](PF6): Cis and Trans Isomer Characteristics Compared. Y. Ru, A. W. Addison 3:40—69. Photophysics and Photochemistry of Ru(ll) Complexes Containing 2,2':2,4":2',4>"'-Quaterpyridine and Its Analogues. S. A. Tysoe, R. J. Morgan, A. D. Baker, T. C. Strekas, H. D. Gafney
4:00—70. Synthesis of BkJentate Bicyclo [3.2.1] Oct-2-Ene Complexes of Manganese. C. J. Wang, J. B. Sheridan 4:20—71. Transmetalation of Tetranuclear Cathecholatocopper(li) Complexes [NCuX]4Yn(N=N,N-Diethylnicotinamide; X = CI, Br, I; Y = 3,4,5,6-Tetrahalocatecholate; n = 1 or 2) with M(NS)2 Reagents (NS = S-Methyl Isopropylidenehydrazinecarbodtthioate) in Aprotic Solvents. M. A. ElSayed, A. El-Toukhy, K. Z. Isamael, A. A. Maradne, G. Davies
MEDICINAL CHEMISTRY C. Town, Chairman WEDNESDAY AFTERNOON Dreyfuss Building, Room 107 Current Topics
P. Sprague, Presiding 2:00—72. Synthesis of Desthio Analogs of Cilastatin as Potential Inhibitors of the Mammalian ^-Lactamase, Renal Dipeptidase (Oehydropeptidase-1, DHP-1). J. E. Brown, D. W. Graham 2:30—73. Synthesis and Antitumor Activity of Ellipticine Carbamates against Human Lung Cancer Cell Lines. S. P. Modi, S. Archer 2:50—74. Bromination of Psoralens as Pathways to Improved Photo-Activated Dermatologic Pharmaceutical. R. K. Rapp, N. D. Heindel, E. Akyea, J. D. Laskin 3:30—75. Thiophene Analogues of Ketanserin and Ritanserin as Selective 5-HT2 Antagonists. J. B. Press, R. K. Russell, J. J. McNally, R. A. Rampulla. J. A. Keiser, C. Scott, J. B. Moore Jr., R. Falotico, S. J. Offord, A. J. Tobia 3:50—76. 7-Oxabicycloheptane Thromboxane A 2 Receptor Antagonists: StructureActivity Relationships. S. E. Hall, M. Nakane, J. A. RekJ, W. Han, D. N. Harris, M. L. Ogletree 4:10—77. C3 Substitution in Benzazepinone Calcium Channel Blocking Agents. D. M. Floyd, S. D. Kimball, J. C. Barrish, J. Z. Gougoutas, M. F. Malley, S. Moreland, S. A. Hedberg
THURSDAY MORNING Dreyfuss Building, Room 107 Computer Modeling and Drug Design C. Cook, Presiding 9:00—Introductory Remarks 9:10—78. Molecular Orbital Study of Amilorkte Analogs. C. Plant, C. A. Venanzi, T. J. Venanzi 9:30—79. Computerized Analysis of Structural Classes Tested in the NCI Anti-HIV Assay. D, Lednteer, L. Hodes, V. L. Narayanan 9:50—80. Triaryltins as Fungal Agents against Ceratocystis Ulmi. G. Eng, G. Hamilton, R. Ramsammy 10:30—81. Channel Catfish Taste Receptor Agonists Containing Modifications of the Alpha Carboxyl Group of L-Alanine. K. Leftnerls, B. Bryant, J. Brand 10:50—82. Bis(Dibenzophospholyl- 1)Ethane: an Alternate Synthesis, X-Ray Crystal Structure, Two Gold(l) Coordination Complexes; and Their Antitumor Activity. D. T. Hill, D. S. Eggleston, P. W. Baures, G. R. Girard, L. F. Faucette, R. K. Johnson, B. M. Sutton
W. Miles, Chairman
11:25—101. Synthesis and Chemistry of Thieno[4,3,2-de]Tricyclic Ring System. R. A. Rampulla, R. K. Russell, C. E. van Nievelt, D. H. Klaubert 11:45—102. Polyamine Synthesis Using Triazones. S. Knapp, M. Bastos
ORGANIC
WEDNESDAY MORNING
THURSDAY AFTERNOON
Dreyfuss Building, First-floor Auditorium
Dreyfuss Building, First-floor Auditorium
Contemporary Topics
Contemporary Topics
P. A. Zucker, Presiding
C. K. McClure,
9:00—83. Asymmetric Synthesis Using a New Class of Chiral Phosphines. S. Wilson, A. Pasternak 9:50—84. Taxol A-B Ring System via an Anionic Oxy-Cope Rearrangement. P. A. Zucker, J. A. Lupia 10:10—85. Further Studies of Electrophilic Substitutions of Aryltrimethylsilanes. L. A. Jacob, B.-L. Chen 10:45—86. Oxygen Scrambling and Stereochemistry during the Trifluoroethanolysis of Optically Active 2-Butylbrosylate. P. E. Dietze, M. Wojciechowski 11:05—87. 17 0 and 13C NMR of the Tautomeric Equilibrium in the Enol Forms of the 1,3-Diketones. A. J. Leffler 11:25—88. Nitro Olefins in One-Pot, ThreeComponent Reactions. G. H. Posner, R. D. Crouch 11:45—89. Condensation of Arylsulfonyl and Alkoxysulfonyl Isocycanates with Methyl-Substituted 2-Methoxy-3,4-dihydro-2H-pyrans. E. Jao, S. S. Hall
2:00—103. Chemistry and Biochemistry Aspects of Enediyne Antitumor Antibiotics. J. Gollk 2:50—104. Electrochemical Oxidation of Thiamin-Bound Enamine Intermediates: a Model to Pyruvate Ferredoxin Oxidoreductase. G. Barletta, F. Jordan, J. Schlegel 3:10—105. Preparation of the Fenoprofen Intermediate, 2-(3-phenoxyphenyl)-propionitrile. N. J. O'Reilly, W. S. Derwin, H. C.Lin 3:45—106. Thiamin Chemistry Revisited: Nucleophilic or Carbene Mechanism? Y.T. Chen, F. Jordan 4:00—107. Cyclitol Precursor to Glycosidase Inhibitors. S. Knapp, A. B. J. Naughton 4:15—108. Synthesis of Valienamine Conjugates. S. Knapp, T. G. M. Dahr, A. B. J. Naughton 4:40—109. Diels-Alder Reaction of Furo[3,4-d]Pyrimidine-2,4-Diones: a New Route to Some Quinazoline-2,4-Dione Derivatives. J. J. McNally, J. B. Press 4:45—110. Facile Synthesis of Substituted a,/?-Unsaturated Acids. A. Chaudhary, E. W. Robb, M. S. Mannas
WEDNESDAY AFTERNOON Dreyfuss Building, First-floor Auditorium
Presiding
2:50—121. Microftitration of Streptomyces rimosusr. Cell Harvesting Process Studies. L. A. BeHIn, H. C. Hollein, C. S. Slater 3:10—122. Mechanisms for Heat Generation in the "Cold Fusion" Experiment. Y. K. Kamath 3:40—123. Durability of Fatty Acid Monolayers from Reciprocal Sliding Measurements. D. D. Dominguez, R. L. Mowery 4:00—124. Gas Agitation of Baths in Electrogalvanizing. J. F. Rakszawski 4:20—125. Mechanistic and Kinetic Modelling of High Alcohol Synthesis over AlkaliPromoted MoS2 Catalysts. R. G. Herman, J. G. Santiesteban, K. J. Smith, K. Klier FRIDAY MORNING Dreyfuss Building, Room 102 Photochemistry and Spectroscopy R. S. Strange, Presiding 9:00—126. Photochemical Approach to Integrated Optics. H. D. Gafney, E. Mendoza, E. Wolkow 9:30—127. Photocatalyzed Conversion of C0 2 to CH4. S.-P. Xu, T. Kawai, H. D. Gafney 9:55—128. Photophysical Properties of Ru(bpy)32+ Adsorbed onto Porous Vycor Glass. J. Fan, S. Tysoe, H. D. Gafney 10:20—129. Rydberg States of CH 4 + . S. Raynor, J. Polynlak 10:45—130. Theoretical Prediction of Vibrational Circular Dichroism Spectra. D. Zeroka, G. R. Famini, J. O. Jensen, A. H. Carrieri, C. F. Chabalowski 11:10—131. Spin-Lattice Relaxation of Xenon Adsorbed in Na Y-Zeolite. M. L. Smith, C. Dybowski
FRIDAY MORNING Organometallic Synthesis
Methods
in
Organic
Dreyfuss Building, First-floor Auditorium
POLYMERS
General Topics
D. Lohse, Chairman
W. H. Miles, Presiding 2:00—90. Synthetic Approaches to Ristocetin A. A. J. Pearson, S. H. Lee, F. Gouzoules, J. G. Park 2:45—91. Practical Modification of Noyori/ Akutagawa Hydrogenation: Synthesis of (-Hndolizidine 223AB. D. Taber 3:45—92. Lithiation and Ring-Opening Reactions of Epoxytetrahydronaphthalene Chromium Complexes. D. J. Wink, P. C. Nirchio 4:05—93. Diastereoselectivity in the Reaction of Chiral Nucleophiles with Organomanganese Arene Complexes. W. H. Miles, H. R. Brinkman, D. Feng 4:25—94. a-Cyclopropylarylalkanes by Tandem Condensation-Reduction of Aryl Aldehydes and Ketones. F. Llotta, L. M. Diaz. S. S. Hall 4:45—95. Synthesis of c/s-Tetrahydroactinidiolide and Dihydroactinidiolide via an Organopalladium Cyclization Strategy. W. A. Metz, P. Myshkin Oe Capite, S. S. Hall
THURSDAY MORNING Dreyfuss Building, First-floor Auditorium
R. Baylouny, Organizer, Presiding 9:00—111. Use of Dispersed Metal Catalysts for Promoting Organometallic Reactions. S. T. O'Leary, R. L. Augustine 9:20—112. Triplet Lifetimes of Deuterated Benzopyrenes. J. C. Selbles 9:40—113. Selective Dimerization of Dienenoid Compounds of Plant Oils. D. DeSoi, R. H. Craver Sr., P. S. Landis 10:10—114. An Unexpected Pericyclic Reaction between Propiolic Ester and a 2Vinyl Benzofuran. M. Puar, P. M. DeCapite etal. 10:45—115. Selectivity-Temperature Relationship and Organic Reactions at - 7 0 °C to-100°C.J.VIt 11:00—116. Thermal Rearrangement of Some Tetrahydro-1,3-oxazine Ak>xides. Synthesis of 2-Alkyl-7-aryl-tetrahydro1,6,2-dioxazepines. M. L. Lann, S. Saba 11:20—117. Radical Based Annulations of lodo Lactams. S. Knapp, F. S. Gibson 11:40—118. Photochemistry of 4-Acylisoxazoles. R. R. Sauers, L. M. Hadel, A. A. Scimone, T. A. Stevenson
Synthesis
T. Walsh, Presiding 9:00—98. Synthesis of Macrocyclic Natural Products. J. A. Marshall 9:50—97. Use of Pentacovalent Oxaphosphorane Chemistry in the Development of New Methology for the Synthesis of Natural Products. C. K. McClure, K.-Y. Jung, C. Grote 10:10—98. Synthesis and NMR Spectra of Monobromo-8-Hydroxyquinolines. D. D. Clarke, H. Gershon 10:45—99. Concise Route to the Oxathiazepine Containing Eudistomin Skeleton and Some Carba-Analogs. M. P. Kirkup, B. B. Shankar, S. W. McCombie, A. K. Ganguly 11:05—100. Progress toward the Ezomycin Octose. S. Knapp, W.-C. Shieh
WEDNESDAY MORNING Dreyfuss Building, Room 104 Functional Polymers J. Dias, Presiding 9:00—132. Functional Polyolefins via Borane Monomers and Transition-Metal Catalysts. T. C. Chung 9:30—133. Synthesis and Characterization of Model Linear and Star-Branched Polycaprolactones. M. Sori, S. Stivala, S. Berkowitz 10:00—134. Interfacial Adhesion of Sulfonated Polystyrene lonomers and Glass Fibers: the Effect of Ion Content. D. M. Elley-Bristow, M. Belliner, M. Hara 10:30—135. Concentration and Temperature Dependence of lonomer Solutions: Sulfonated Polystyrene lonomers in Toluene. J. Bodycomb and M. Hara 11:00—136. Aggregation Behavior of lonomers: Styrene-Methacrylic Acid lonomers in Low-Polarity Solvent. V. Goel, M. Hara 11:30—137. Mechanical Properties of Poly(Methyl Methacrylate) (PMMA) Based lonomers. X. Ma, M. Hara
PHYSICAL CHEMISTRY WEDNESDAY AFTERNOON
R. Strange, Chairman THURSDAY AFTERNOON Dreyfuss Building, Room 102 General Topics C. S. Slater, Presiding 2:00—119. New Directions in Membrane Science and Engineering. C. W. Slater, P. J. Hickey 2:30—120. Advances in Membrane Pervaporation for the Separation of Liquid Mixture. H. L. Fleming
Dreyfuss Building, Room 104 Blends and Physical Properties P. Soskey, Presiding 2:00—138. High-Temperature Polymer Blends. P. Chen, M. Glick, M. Jaffe 2:30—139. NMR Study of Polyisoprene/Poly(vinylethylene) Miscible Blends. K. J. McGrath, J. B. Miller, C. M. Roland. C. A. Trask, A. N. Garroway 3:00—140. Deformation Mechanisms of lonomer Blends: Sulfonated Polystyrene lonomer/Polystyrene. M. Bellinger, M. Hara
March 26, 1990 C&EN
49
Meetings
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3:30—141. Rheological Behavior of Polyolefin Blends Modified through Reactive Processing. D. W. Yu, C. G. Gogos, M. Xanthos 4:00—142. Deformation and Agglomeration in Filled Rubber. C. M. Roland, K. Peng 4:30—143. Dilatometric Measurements of Thermoset Polymers during Cure. A. W. Snow, J. P. Armistead
11:00—161. Effect of Cations on the Solution Viscosity of PVP. I. Higher Salt Concentrations. R. D. Andrews, K. Y. Paik 11:30—162. Effect of Cations on the Solution Viscosity of PVP. II. Lower Salt Concentrations. K. Y. Palk, R. D. Andrews
THURSDAY MORNING
STUDENT RESEARCH
11:20—178. Study of the Effects of Ionic Strength on the Reduction Potential of Hemoglobin. K. C. Salomonsson, L. H. Rickard 11:40—179. Effects of pH on the Electron Transfer Reactions of Hemoglobin. L. R. Garrett, L. H. Rickard 2:00—180. Zirconium PyrophosphateBased Solid Solutions as Electrolytes. G. Gechllk, P. P. Tsai, M. Greenblatt
Dreyfuss Building, Room 104 Plastics Recycling
M. J. Smith, Chairman
POSTERS
E. M. Phillips, Presiding 9:00—144. Plastics Recycling: from a Vision to a Reality. E. A. Fox 9:25—14S. Postconsumer Plastics Recycling Collection: Source of a New Raw Material from Municipal Solid Waste. D. Haneslan 9:50—146. New Developments in Sortation Technology. H. Frankel, R. Renfree 10:15—147. Economics of Reclamation of General Plastics from Postconsumer Wastes. E. M. Phillips 10:40—148. Effect on Properties of Commingled Waste Plastics with the Introduction of Polystyrene Waste. T. J. Nosker, R. W. Fenfree, D. R. Morrow 11:05—149. Markets and Applications for Recycled Plastics Materials. R. A. Bennett 11:30—150. Recycling of Discarded Plastic Fishing Gear by Melt Processing. A. Patel, S. S. Dagli, P. G. Kellecher, M. Xanthos
THURSDAY AFTERNOON Dreyfuss Building, Room 104 Degradable Plastics
R. Forster, Presiding 2:00—151. Overview of Enhanced Degradable Plastics Technologies and Their Applications in Solid Waste Management. A. LAndrady 2:30—152. Biodegradable Polymeric Film—Methodology and Comparison. S. G. Gilbert, A. Yabannavar, R. Bartha 3:00—153. Hydrodegradable Polyester Resins. B. Gordon 3:30—154. Overview of Photodegradable Poly(ethylene-co-carbon monoxide). R. Forster 4:00—155. Degradation of Plastics Using Simulated Laboratory Exposures. R. A. Gross, S. McCarthy, C. Bruell, D. L. Kaplan 4:30—156. Potentially Degradable Plastics for Marine Applications. X. Chen, S. H. Patel, K. E. Gonsalves
WEDNESDAY AFTERNOON Dreyfuss Building, Room 213 Research in Chromatography Award
WEDNESDAY MORNING & AFTERNOON
L. Lakritz, Presiding
Recreation Building
2:05—163. Applications of Analytical Chemistry in the Study of Biological Materials. T. J. DIFeo, A. W. Addison 2:20—164. Novel Approach for Screening Bioactive Compounds. L. Prol, D. C. Shelly 2:35—165. Equilibrium and Kinetic Studies of the Interaction between Protein and Immobilized Ligand. T.-J. Fu, A. Carlson 3:00—166. Gas-Solid Diffusion and Equilibrium Parameters by Tracer Pulse Chromatography. J. R. Hufton, R. P. Danner 3:35—167. Analysis of a Miniature Optical Fiber Fluorescence Detector for Micro HPLC. M. A. Ruberto, D. C. Shelly 3:50—168. Analysis of Response Factors for Dansyl Amino Acids Using Micro HPLC with Laser-lnduced-Fluorescence Detection. S. DeFalco, D. C. Shelly 4:05—169. Use of Adsorption Chromatography Cartridges for Separation of Polar Compounds from Heated Frying Fats. A. P. Handel, L. A. Bobnak, J. J. Mttolo 4:20—170. Effects of Cell Growth Stimulants on Oxalyl Thiolesters Concentrations in Animal Cells as Determined by Reversed-Phase Ion-Pairing High-Performance Liquid Chromatography. C. Yang, A. M. Mastro, G. A. Hamilton 4:35—171. Completed Studies of Factors Promoting Growth and Alkaloid Production of Peyote [Lophophora Williams II, (Lem) Coulter] Callus Tissues IV. W. R. Obermeyer, A. D. Marderosian THURSDAY MORNING & AFTERNOON Dreyfuss Building, Room 212 Undergraduate Research Symposium M. Smith, Presiding
FRIDAY MORNING Dreyfuss Building, Room 104 R neology
C. Tsenoglou, Presiding 9:00—157. Quantitative Determination of Molecular Weight Distributions from Melt Rheological Properties. W. H. Tumlnello, N. Cudre-Mauroux, W. J. McGrory 9:30—158. Rheological Behavior of Highly Filled Suspensions. D. M. Kalyon, U. Yilmazer, B. Aral 10:00—159. Viscoelasticity of Polybutadiene Blends with Variable Microstructure. C. Tsenoglou, S. Bhakuni 10:30—160. Measurement of Rheological Properties of Cheese Using Oscillatory Rheometer. E. J. Nolan, J. J. Shieh
9:00—172. Synthesis and Characterization of Polyacetylene Prepared with High-Temperature Treated Catalyst. G. A. Arbuckle, C. G. Clark 9:20—173. Intramolecular Activation of a CH Bond by Manganese in Chelate Complexes. J. M. Ressner, J. E. Thornton, C. S. Kraihanzel. V. O'Brien 9:40—174. Comparison between Exact and Approximate Methods for Calculating Molecular Electrostatic Potential Surfaces. N. U. M. Shyamantha, C. Plant, C. A. Venanzi, T. J. Venanzi 10:10—175. Mild, Convenient Method for Oxidation of Some Organic Functional Groups with Ruthenium Tetroxide. M. B. Cichowicz, R. G. Saylor 10:30—176. Lactone Intermediate as an Alternative Activating Function in Linking Amino-Pharmaceuticals to Dextran. M. A. Kauffman, B. Weber, E. Akyea, N. D. Heindel, H. Zhao 10:50—177. Development of an Enzyme Immunoassay for Detection and Quantification of Nicotine Metabolites in Urine. S. Amesur, D. E. Nadig. N. D. Heindel, R. S. Niedbala, K. J. Schray.
Poster Session I
R. Baylouny, F. Lang, Presiding
—195. Method for Rapid Isolation of IgM from Sera. K. P. Rowland, P. T. Nix —196. Detection of Illegal Drugs in Race Horses. K. Thomas, K. Loninetti, S. M. P. Coakley —197. Souping Up Race Horses. K. C. Macdonald, J. Luty, S. M. P. Coakley —198. 13 C NMR Shift-Structure Mapping. F. Benett, C. Rock —199. Using MACCS-3D To Estimate a "Pharmacophore" for a Series of Active Compounds. M. Miller, C. Rock —200. Mossbauer Studies of the Speciation of Triphenyltins in the Chesapeake Bay. R. A. Lucero, M. A. Otieno, G. Eng —201. Investigation of Individual Polymer Chains by Transmission Electron Microscopy (TEM). Y. P. Carkjnan, F. Cosandey, M. Hara, M. Bellinger, P. Jar, Y. Wang —202. Changes in Poultry Litter Toxicity with Simulated Acid Rain. S. Krishnamurthy, G. C. Gupta —203. Changes in Poultry Litter Biochemical Oxygen Demand and Toxicity with Age. M. A. Doherty, G. C. Gupta —204. Characterization of the Near-Infrared Spectral Bands of Acyclic and Cyclic Imides. P. J. McNeilly, S. E. Krikorian —205. Dimethyl-4-Phosphonocrotonal Ethylene Acetal: a New Reagent for the Four Carbon Homologation of Aldehydes to Dienals. A. Monaghan, I. M. Taffer, R. E. Zipkin —206. Dimethyl-4-Phosphonocrotonal Ethylene Acetal. R. Sivakumar, J. Prol, A. Monaghan, I. M. Taffer, R. E. Zipkin
11:00 AM-2:00 PM—181. Synthesis and Photophysical Properties of a Mixed Metal Ru(ll)/Pt(ll) Complex Containing the bisBidentate Bridging Ligand 4',7'-Phanthrolino-5',6':5,6-Pyrazine. R. J. Morgan, S. A. Tysoe, H. D. Gagney, T. C. Strekas, A. D. Baker —182. Synthesis, Coordination Chemistry, and Catalytic Properties of Soluble Ion Tetrazaporphyrins. J. P. Fitzgerald —183. Electrochemistry and Kinetics of Hydrolysis of Nickel Complexes with Pentadentate Ligands. J. M. Lyon —184. Intercalate Binding of Mixed Ligand RETIRED CHEMISTS Complexes of Ru(ll) with DNA. T. C. Strekas, A. D. Baker, R. Morgan, S. Chatterjee —185. Development and Characterization N. D. Heindel, Chairman of Chiral Pentacovalent Spirophospholenes. C. K. McClure, C. W. Grote —186. New Synthesis of 3-lndazolones. J. WEDNESDAY MORNING P. Demers, D. H. Klaubert —187. Cultivating Problem-Solving in the Dreyfuss Building, Room 212 Undergraduate Organic Laboratory: a Practical "Roadmap" Problem. E. A. Har- L Life after the Big Company: PostRetirement rlson Jr. —188. Solvation Changes Accompanying N. D. Heindel, Presiding Proton Transfer. T. E. Casamasslna, W. P. Huskey 9:00—207. The Big Picture: Employment —189. Synthesis and Herbicidal Activity of Trends and Retirement Options. N. D. the Pyridine Analogs of Methyl erythroHeindel and threo-4-Cyano-3,4-Diphenylbuty9:10—208. Charles A. Dana Institute for rates. D. A. Chlarello, S. S. Szucs Scientists Emeriti: an Academic-Industrial —190. Cation Complexes of a Cyclic UreaResearch Opportunity. G. deStevens Anisole Spherand: an Examination of the 9:30—209. Technology Transfer from AciDesign Concept of Host Preorganization. demia to Industry. L. E. A. Godfrey P. V. Maye, C. A. Venanzi 9:50—210. Volunteer Opportunities: How — 1 9 1 . A Rearrangement of 4-AminothioTo Avoid Obsolescence. T. R. Russell and carbonyloxazoles to 5-Aminothiazoles. R. K. Neuman Synthetic and MINDO/3 MO Studies. S. L. 10:10—211. New Company Startup—OpCorrao, M. J. Macielag, I. J. Turchi portunities and Pitfalls. F. W. Mlcheiotti —192. Novel, Convergent Approach to the 10:30—212. Entrepreneurism: Part II. D. A. Synthesis of Polyunsaturated Fatty Acids. Lima R. Sivakumar, J. Prol, A. Monaghan, I. M. 10:50—213. High Cost of Panic: Writing/ Taffer, R. E. Zipkin Publishing as a Post-Retirement Option. P. J. Wlngate 11:10—214. From Chemist to Historian of THURSDAY MORNING & Chemistry. O. T. Benfey AFTERNOON 11:30—215. Specialty Consulting and Teaching. S. M. Gerber Recreation Building Poster Session II
R. Baylouny, F. Lang, Presiding 11:00 AM-2:00 PM—193. Electronic Decay of Core Hole Excited States in Molecular Oxygen. D. Lapiano-Smith, K. Lee, C. I. Ma, K. T. Wu, D. M. Hanson —194. New Immunoassay Detection Method for Fentanyl Compounds. K. P. Gibson, T. A. Durrant, P. T. Nix
YOUNGER CHEMISTS
WEDNESDAY AFTERNOON Dreyfuss Building, Room 212 Employment Chemists
Strategies
for
Younger
T. Conners, Presiding 2:00—216. Employment Strategies for Younger Chemists. T. Conner, D. McNamara, B. Taraszewski, N. Dee 3:10—Panel Discussion
March 26, 1990 C&EN
51
Meetings
12th Symposium on Biotechnology for Fuels & Chemicals
THURSDAY 8:00 AM-noon—Registration. Main Lobby
Whaley Hall Session 4 Bloengineerlng Research
H. R. Bungay, J. S. Watson, Cochalrmen
The 12th Symposium on Biotechnology for Fuels 6x Chemicals will be held at the Riverside Motor Lodge, Gatlinburg, Tenn., May 7-11. The symposium is sponsored by the ACS Division of Biochemical Technology and governmental and industrial organizations. It brings together world leaders in the fields of biotechnology for fuels, chemicals, and biotechnological aspects of environmental control. Thirty-five invited oral presentations and more than 80 invited posters are scheduled. Advances in biotechnology continue to provide alternatives that will have an impact on the future economic production of fuels and chemicals. This symposium provides a forum for presentation of new research results and exchange of ideas. The chairman of the symposium is Elias Greenbaum; the cochairman is Charles E. Wyman. Early registration is encouraged be-
TUESDAY 9:00 AM-5.00 PM—Registration. Main Lobby Whaley Hall 8:30 AM—Welcome and Introduction to the Symposium. E. Greenbaum
cause of a facility-imposed restriction of about 250 participants. Registration is $230 if received before April 13 ($250 after April 13). The registration fee includes a Tuesday evening banquet, Wednesday luncheon buffet, refreshment breaks, and a copy of the published proceedings. Lodging at the Riverside Motor Lodge, Gatlinburg, Tenn. 37738, phone (615) 436-4194, is $45.50 per day single or double occupancy. Registration and housing forms are included. Make checks payable to 12th Symposium on Biotechnology, and send to Deborah J. Weaver, Oak Ridge National Laboratory, P.O. Box 2008, Oak Ridge, Tenn. 37831-6194. For more information, call Mrs. Weaver at (615) 5760446; fax (615) 574-6442. Registration at the symposium will be in the main lobby from 6 to 10 PM Monday; Tuesday from 9 AM to 5 PM; and Wednesday through Friday from 8 AM to noon. 3:45—12. Glutamate Production from C0 2 and N0 3 ~ by a New Biosolar Reactor Using Immobilized Marine Cyanobacteria. T. Matsunaga, N. Nakamura, H. Takeyama 4:10—13. Oil Production by Wild, Micropropagated Plants, Calli and Suspended Cells of Euphorbia characias L. M. Femandes-Ferrelra, M. S. S. Pais, J. M. Novais 4:35—14. Microbial Extraction of Beet Pulp Pectin. K. M. Ghanem, A. H. El-Refai. M. A. El-Gazaerly
Thermal, Chemical, and Biological Processing
A. O. Converse, R. J. Evans, Cochalrmen 8:40 AM—Introduction 8:45—1. Development of a Differential Volume Reactor System for Soil Biodegradation Studies. O. F. Webb, T. J. Phelps, P. R. Bienkowski, P. M. DiGrazia. G. D. Reed, J. M. H. King. D. M. White, G. S. Sayler 0:10—2. Biomass-to-Gasoline: Catalyst and Feedstock Effects. R. J. Evans, F. Agblevor. T. A. Milne 9:35—3. Effect of Carbonization Heating Rate on Charcoal and Activated Carbon Yields. C. E. Martin, K. R. Purdy, C. P. Kerr, S. Dubayeh, T. A. Garr 10:20—4. Avoiding Digester Imbalance through Real-Time Feedback Control of Dilution Rate. P. Pullammanappallil, J. Harmon, D. P. Chynoweth, G. Lyberatos, S. A. Svoronos 10:45—5. Methane Production from Beet Pulp. K. M. Qhanem, A. H. El-Refai, M. A. El-Gazaerly 11:10—8. Effect of Temperature on the Glucose Yield Kinetics and HF-Adsorption/Desorption Profiles of the Solvolysis of a Single Lignocellulose Wafer in Anhydrous Hydrogen Fluoride (HF) Vapor. G. L. Rorrer, M. C. Hawley, D.Lamport 11:35—7. Ammonia Freeze Explosion (AFEX) Process: a Practical Lignocellulose Pretreatment. M. T. Holtzapple, J-H. Jun, B. E. Dale
Session 2 Applied Biological Research I
N. W. Y. Ho, K. Grohmann, Cochalrmen 1:30 PM—Introduction 1:40—8. Ethanol Fermentation of Lignocellulose Hydrolysates. B. Hahn-Hagerdal, T. Linden, T. Senac, K. Skoog 2:05—0. Synergism of Endo- and Exoglucanase and o-Glucosidase That Compose Cellulase on Hydrolysis of Cellulose. M. FuJIi, T. Homma, K. Ooshima. M. Taniguchi 2:30—10. Improvement of Cellulase Production in Tricho derma. D. K. Sandhu, S. Bawa 2:55—11. Cloning of the Clostridium acetobutylicum Acetoacetate Decarboxylase Gene and Its Expression in Escherichia coll. D. J. Petersen, G. N. Bennett
52
March 26, 1990 C&EN
WEDNESDAY 8:00 AM-noon—Registration. Main Lobby
Whaley Hall Session 3 Applied Biological Research II
S. Lien, B. D. Faison, Cochalrmen 8:40 AM—Introduction 8:45—15. Growth of Aerobic Bacteria on Alkali-Solubilized Lignite. J. K. Polman, C. R. Breckenridge, P. R. Dugan, D. R. Quigley 9:10—16. Production of Lignin Peroxidase by Streptomyces viridosporus. T. P. Adhl, R. A. Korus, D. L. Crawford 9:35—17. Utilization of Cheese Whey for Production of aAmylase Enzyme. P. Bajpai, N. Verma, J. K. Neer, P. K. 10:20—18. Submerged Culture versus Solid-State Culture for Cardboard Bioconversion to Protein-Enriched Biomass. A. S. El-Nawawy, R. Al-Daher 10:45—19. Bioconversion of L-carnitine Precursor in Monoor Two-Liquid Phase System. G. Bare, J.-B. Hubert, Ph. Jacques, R. Rikir, Ph. Thonart 11:10—20. Performance of Trickle-Bed Bioreactors for Converting Synthesis Gas to Methane. D. E. Kimmel, K. T. Klasson, E. C. Clausen, J. L. Gaddy 11:35—21. Metabolic Modeling of Fumaric Acid Production by Rhizopus arrhizus. I. C. Gangl, W. A. Weigand, F. A. Keller
Special Topic Discussion Groups 7:00-9:00 PM—Venture Capitalists' View of Biotechnology for Fuels and Chemicals. F. R. Landtberger —Emerging Biotechnologies. R. M. Butcne
8:40 AM—Introduction 8:45—22. Critical Review and Evaluation of Bioproduction of Organic Chemicals. S. A. Leeper, G. F. Andrews 9:10—23. Biological Production of Acetaldehyde from Ethanol Using Nongrowing Pichia Pastoria Whole Cells. H.-K. Chiang, W. W. Fish, G. Foutch 9:35—24. Enzymatic Hydrolysis of Starch in a Fixed-Bed Pulsed Flow Reactor. A. Sanroman, R. Chamy, M. J. Nunez, J. M. Lema 10:20—25. Design of a Membrane-Based Integrated Ethanol Production Process. W. J. Groot, R. G. J. M. van der Lans, K. Ch. A. M. Luyben 10:45—26. Thermophilic Ethanol Production: Investigation of Ethanol Yield and Tolerance in Continuous Culture. L. R. Lynd, H-J. Ahn, G. Andersen, P. Hill, D. S. Kersey 11:10—27. Evaluation of a Multicompartment Bioreactor for Ethanol Production Using In-Situ Extraction of Ethanol. M. L. Shuler, D. E. Steinmeyer, A. P. Togna, S. Gordon, P. Cheng, S. J. Letai 11:35—28. Nondispersive Extraction for Recovering Lactic Acid from Fermentation Broth. C. J. Wang, R. K. Bajpai
Special Topic Discussion Groups 2:00-4:00 PM—Biotechnology and Specialty Chemicals. M. L. Shuler —In-Situ Bioremediation: Why Is It So Difficult? M. E. Reeves
Pearl Room Thermal, Chemical, and Biological Processing B. H. Davison, A. A. Antonopoulos, Cochalrmen 7:00 PM—29. Fermentation Studies on Sugars Recovered from Waste Cellulosics via Acid Hydrolysis. M. J. Beck, R. D. Johnson, C. S. Baker —30. Active Protein and Substrate Flow Effects in a Tubular Immobilized Invertase Reactor. F. N. Onyezlll — 3 1 . Evaluation of Dilute Sulfuric Acid Hydrolysis and Autohydrolysis for Sugar Production from Hardwood Hemicellulose. R. C. Strickland, D. S. Tuten, M. D. Hardy —32. Conversion of Newsprint and MSW-Cellulosics to Sugar by Dilute Sulfuric Acid Hydrolysis. R. C. Strickland, D. S. Tuten, M. D. Hardy —33. Effect of Medium Composition and Growth Intervals on Growth, Total Lipids, and the Fatty Acid Composition of Fusarium solani. M. K. Tahoun, Z. El-Merheb, A. E. Salem —34. Delignification of Nonwoody Biomass. G. J. Tyson —35. Study of Treating Pharmaceutical Wastewater in the Upflow Anaerobic Sludge Blanket (UASB) Reactor. G. Datlan, F. Zihua, H. Xiaogang —36. Single-Cell Protein Production from Acid-Hydrolyzed Lignocellulosics. T. A. McCaskey, A. H. Stephenson, R. C. Strickland —37. Dilute Acid Pretreatment of Corn Residues and Short Rotation Crops. R. Torget, P. Werdene, M. E. Himmel, K. Grohmann —38. Technical and Economic Analysis of Ethanol Production from Wheat Straw or Aspen Wood Chips Using Steam Explosion or Dilute Acid Pretreatments. R. Torget, A. Power, D. J. Schell, P. J. Walter, K. Grohmann, N. Hinman —39. Effect of Pretreatment on SSF of Hardwood into Acetone/Butanol. M. Shah, Y. Y. Lee, R. Torget —40. Continuous Production of Biogas from Cheese Whey Using a pH-Controlled Two-Stage Mesophelic Reactor. A. E. Ghaly, J. Pyke — 4 1 . Thermal Degradation of Cereal Straws in Air and . Nitrogen. A. E. Ghaly, A. Ergudenler Applied Biological Research 7:00 PM—42. Influence of Macronutrients, Auxins, and Biosynthetic Precursors on Rosmarinic Acid Synthesis in Cell Suspension Cultures of Salvia officinalis. K. Shetty, D. L. Crawford, R. Korus —43. Isolation and Characteristics of Plasmids from Clostridium thermosaccharolyticum. S. Kalyuzhnyy, N. Belogurova, T. Mosolova, S. Varfolomeyer —44. Kinetic Investigation and Mathematical Modeling of Methanogenesis. S. Kalyuzhnyy, S. Varfolomeyer, V. Gachok, V. Sklyar —45. Biodegradation of Mixtures of Hazardous Organic Compounds. G. W. Strandberg, D. J. Larson, T. L. Donaldson —46. Induction of Mutation in Trichoderma viride and on Laboratory-Scale Conversion of Natural Cellulose into Fuel. M. K. Tahoun, A. Khalil, S. Helmi, A. H. Khairy —47. Induction of Mutation in Aspergillus nigertor Conversion of Cellulose into Fuel Precursor. S. Helmi, A. Khalil, M. K. Tahoun, A. H. Khairy —48. Characterization of a Photosynthetic Shear-Resistant Glycine Max Cell Line. J. Castillon, V. N. Coleman, F. Kong, V. Piriyapan, W. J. Treat, C. R. Engler, E. J. Sottes —49. Immobilization of Enzyme to Platinum Electrode and Its Use as Enzyme Electrode. S. Gondo, M. Kawakami, H. Koya
Advance Registration —50. Ethanol Production by Recombinant Escherichia coli Carrying Genes from Zymomonas mobilis. H. G. Lawford, J. D. Rousseau — 5 1 . Degradation of Organic Sulfur Compounds by a CoalSnhihilizinn Furious. B. D. Fateon. C. A. Woodward. Τ Μ Clark, D. M. Sharkey —52. Physiological Aspects of the Regulation of Extracellu lar Enzymes of Phanerochaete chrysosporium. C. G. Dosoretz, A. H. C. Chen, H. Ε. Grethlein —53. Biochemical Oxidation of D-Sorbitol to L-Sorbose by Immobilized Gluconobacter oxydans Cells. S. Stefanova, A. Triphonov, I. Tepavicharova, Chr. Konstantinov —54. Microbial Desulfurization of Fossil Fuels. T. Omorl, L. Monna, T. Koana, T. Kodama, A. Hiratsuka, κ. Hon-nami, Ν. Nishikawa —55. Butanol Production from Carbon Monoxide by Butyrl· bacterium nwthylotrophicum. A. J. Grethlein, R. M. Worden. Μ. Κ. Jain, R. Datta —56. Kinetics of Growth and Catechol Production by Bacil lus stearothermophilus BR 219. R. M. Worden, R. Subramanian, M. J. Bly, S. Winter, C. L. Aronson —57. Characterization of Four Purified Extracellular Ligninases from the Lignin-Solubilizing Actinomycete, Streptomyces viridosporous T7A. T. S. Magnuson, M. A. Roberts, D. L. Crawford, G. Hertel —58. Microbes as Biocatalysts for Oil Well Stimulation and Foam Placement. F. M. Cusack, J. W. Costerton —59. Studies on Cellulase Production Using Spent Sulfite Liquor and Paper Mill Waste. Z. Xin, Q. Yinbo, G. PeIJi, W. Zunong —60. Hydrolysis of Cellobiose by Immobilized-Glucosidase Entrapped in Maintenance-Free Gel Spheres. J. Wood ward, Κ. Μ. Clarke — 6 1 . Lignite Solubilization by an Extracellular Product of Pénicillium. R. Beyerinck, M. N. Karim, L. Henk —62. Anaerobic Degradation or Furfural (2-Furaidenyde) to Methane and Carbon Dioxide. C. J. Rlvard, K. Grohmann —63. Isolation and Characterization of Two Chromatographic Forms of 0-o-Glucosidase from Aspergillus niger. M. E. Himmel, D. J. Mitchell, J. O. Baker, W. S. Adney, K. Tatsumoto. K. Grohmann. J. W. Fox —64. Toxic Effects of Selected Industrial Solvents in Batch and Continuous Anaerobic Reactors. L. J. Schwartz —65. Genetic Transformation of Xylose-Fermenting Yeast P. stipitis. N. W. Y. Ho, D. Petros, X. X. Deng —66. Selection of Thermotolerant Yeasts for Simultaneous Sacchariflcation and Fermentation of Cellulose. I. Ballesteros, M. Ballesteros, A. Cabanas, J. Carrasco, C. Martin, M. j . negro, r. oaez, π. oavz —67. Dual Inoculation with VA Mycorrhiza and Rhizobium is Beneficial to Leucaena Growth. R. P. Gupta, V. Punj —68. Effects of Nutrients and Temperature on Biomass, Growth, Lipid Production, and Fatty Acid Composition of Cyclotella cryptica. S. Srlharan, D. Bagga, M. Nawaz —69. Entrapped Thermoalkalophilic Bacillus and Endoglucanase Production. K. Bala Krishna, A. Varma —70. Purification of Trichoderma reeseiCellobiohydrolase I by Preparative Native Gel Electrophoresis. N. E. Lee, J. Woodward — 7 1 . Strain Development for Alcohol Production from Hemicellulose Hydrolyzate. T. Sekl, N. Nakashima, W.-Z. Xu, C.-X. Pan, I. Urabe, T. Yoshida, H. Okada —72. Use of Cyanobacterial Diazotrophic Technology in Rice Agriculture. D. N. Tlwarl —73. Plant Extract Estimulation of Biofilm Production by the "Tea Fungus," Acetobacter xylinum. J. D. Fontana, A. M. deSouza —74. Seed Gum of Stiphnodendron barbatiman. F. Reciher, S. C. S. Leitner, M. R. Sierakowski, J. D. Fontana, J. B. C. Correa Bloenglneering Research 7:00 PM—75. Extractive Fermentation of Acetic Acid: Eco nomic Trade-off between Yield of Clostridium and Con centration of Acetobacter. R. M. Busche —76. Production of Ethanol and Coproducts from MSWDerived Cellulosics Using Dilute Sulfuric Acid Hydrolysis. J. W. Barrier, M. M. Bulls, R. O. Lambert, J. D. Broder —77. New Kinetic Approach to the Fermentation of Multisubstrate Complex Media. A. Converti, M. Del Borghi —78. Modeling of D-Sorbitol to L-Sorbose Biotransformation by Immobilized Cells Gluconobacter Suboxydans in a Bubble Column. V. Beschov, M. Kosseva —79. Microbial Removal of Sulfur Dioxide (S02) and Nitric Oxide (NO) from a Gas. K. L. Sublette, K. H. Lee —80. Economic Analysis of the Microbial Reduction of Sul fur Dioxide (S0 2 ) as a Means of By-Product Recovery from Regenerable Processes for Flue Gas Desulfurization. K. L. Sublette, K. Gwozdz — 8 1 . Determination of the Partition Coefficient for Protein Separation in an Air-Fluidized Bioreactor. P. B. Kokitkar, R. D. Tanner —82. Effect of pH and Gas Composition on the Bubble Fractionation of Proteins. A. H. G. DeSouza, W. T. Effler Jr., R. D. Tanner —83. Bioreactor Design Considerations in the Production of High-Quality Microbial Exopolysaccharide. H. G. Lawford, J.Rousseau —84. Modeling of an Immobilized Cell, Three-Phase Fluidized-Bed Bioreactor. J. N. Petersen, Β. Η. Davison —85. MSW Volume Reduction, Value Recovery, and Value Addition. M. Eley, J. Watson, M. J. Beck, R. D. Johnson, T. McCaskey —86. Structured Model for Vegetative Growth and Sporula tion in Bacillus thuringiensis. M. Starzak, R. Bajpai —87. Prediction of Bed Height in a Self-Aggregating Yeast Ethanol Tower Fermenter. C. S. Chen, E. C. Chang, C. S. Gong, L. F. Chen
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Catalysis Letters A new monthly journal for the rapid publication of short communications Articles are published within three months of acceptance First-class airmail delivery to the USA, Canada, Japan, Australia, etc. EDITORS-IN-CHIEF: Professor Gabor A, Somoriai. Department of Chemistry, University of California, Berkeley, CA 94720, USA Professor John M Thomas, F.R.S., Director of the Royal Institution of Great Britain and the Davy Faraday Research Laboratory, 21, Albemarle Street, London, WIX 4BS, United Kingdom Volumes 4-5, 1990, $ 204.80 each inch postage; volumes. 1-3, 1988-1989, $ 221.50 each incl. postage 400 pages per vol. ISSN 1011-322 X Abstracted/indexed in Current Contents, Science Citation Index, Scisearch and Automatic Subject Citation Alert.
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—88. Theoretical and Experimental Investigation of an Upflow Solids-Retaining Bioreactor for Cellulose Conversion. D. A. Hogsett, G. Spieles, L. R. Lynd —89. Simultaneous Saccharification and Fermentation of Pretreated Woody Crops to Ethanol. D. D. Spindler, C. E. Wyman, K. Grohmann —90. COS Degradation by Selected CO-Utilizing Bacteria. K. D. Smith, K. T. Klasson, M. D. Ackerson, E. C. Clausen, J. L. Gaddy — 9 1 . Parameters Affecting the Kinetics of Ethanol Production from CO, C0 2 , and H2 by Clostridium ljungdahlii. K. M. 0. Lundback, B. B. Elmore, S. B. Baker, T. K. Klasson, E. C. Clausen, J. L. Gaddy —92. Comparison of Inhibitory Effects on S. cerevisiae and Z. mobilis in Batch and Continuous Culture. J. J. Wu, E. C. Clausen, J. L. Gaddy —93. Use of an Aqueous Two-Phase System for ABE Fermentation. Y. J. Kim, W. A. Weigand, J. Hong —94. Continuous Fermentation of D-Xylose by Immobilized Pichia stipitis: Comparison between CSTR and CPFR. M. J. Nunez, R. Chamy, A. Sanroman, J. M. Lema —95. Use of a Novel Immobilized 0-Galactosidase Reactor To Hydrolyze the Lactose Constituent of Skim Milk. A. P. Bakken, C. G. Hill Jr., C. H. Amundson —96. Simple Structured Model for the Growth of Wild Carrot Cells. G. C. Frazler, D. K. Dougall —97. Enzyme Adsorption/Desorption during the Hydrolysis of Pretreated Poplar. J. R. K. Nutor, A. O. Converse —98. Studies on Whole-Cell Immobilization of Yeast Saocharomyces cerevisiae NSI 113 on a Packed-Bed Calcium Alginate Support on Cane Molasses. K. Pande, P. K. Agrawal —99. Comparative Evaluation of Catalase Immobilization Methods on Different Supports. V. G. Artenie, D. C. Cojocaru —100. Bioconversion of By-Products of Sugar Industry (Molasses and Sugarbeet Pulp) for SCP Production. P. Nkjam, M.Vogel — 1 0 1 . Enzymatic Saccharification and Fermentation of Sugar Beet Pulp for SCP Production. P. Nlgam, M. Vogel —102. New Methods for Growing Plant and Mammalian Cells and for Dissociation of Methanol. R. Clyde Biotechnology, Bloenglneerlng, and the Solution of Environmental Problems 7:00 PM—103. Study on BOD Microbial Sensor for Wastewater Treatment Control. L. Yourong, C. Ju —104. Comparative Microbial Degradation of Organic Cyanide. M. S. Nawaz, J. H. Davis, K. D. Chapatwala —105. Bioprocess for C02-Elimination from Power Plant Flue Gas: the Possible Use of Microalgae and Seawater. M. Negoro, N. Shioji, K. Miyamoto, Y. Miura —108. Production of Oil-Degrading Bacteria and Their Use in Microbial Remediation of Contaminated Soils. H.-P. Rohns, S. Schalenbach, L. E. Webb —107. Methanol Suppression of Trichloroethylene Degradation by M. trichosporium. A. V. Palumbo, W. Eng —108. Iron Oxidation by Thiobacillus ferrooxidans. S. K. Kang, R. D. Sproull —109. Isolation of Amoebic-Bacterial Consortia Capable of Degrading Trichloroethylene. R. L. Tyndall, K. Ironside, C. D. Little, S. Katz, J. Kennedy —110. Biological Pretreatment of Water Hyacinth for Improved Biogas Production. D. Madamwar, V. Patel, A. Patel —111. Fiber-Optic-Based Apparatus for the Nondestructive, In-Vivo Measurement of Photosynthesis: Application to Environmental Monitoring. J. E. Coffleld, D. A. Graves, E. Greenbaum
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Whaley Hall Session 5 Biotechnology, Bloenglneerlng, and the Solution of Environmental Problems J. R. Geiger, D. A. Graves, Cochairmen
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8:40 AM—Introduction 8:45—112. Risk Assessment of Microorganisms Used in Pollution Control. H. S. Strauss 9:10—113. Anaerobic Dechlorination of Chlorinated Biphenyls by Mixed Bacterial Cultures from PCB-Contaminated Sediments. M. E. Reeves, C.-C. Chang, T. L. Donaldson 9:35—114. In-Situ Soil Aeration for Enhanced Blodegradation of Hydrocarbons. R. E. Hlnchee, D. C. Downey, R. Miller 10:20—115. Biological Oxygen Consumption as a Measure of Biodegradation of Mixed Organic Wastes. D. A. Graves 10:45—116. Land Farming of Oily Sludge in Kuwait—Effect on Soil Properties and Plant Growth. A. S. El-Nawawy, I. H. El-Bagouri, M. Abdal, S. M. Khalafawi, R. M. Al-Daher, F. Khalil 11:10—117. Novel Biotreatment Process for Glycol Waters. L. M. V. Raja, G. Elamvaluthy, R. Palaniappan, R. M. Krishnan 11:35—118. Gas Hydrate Formation in Reversed M i c e l l e s Applications to Bioseparations and Biocatalysis. V. T. John, H. Nguyen, M. Rao. J. B. Phillips
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MOLECULAR MODELING: METHODSAND TECHNIQUES A 4-day hands-on lecturelaboratory short course
Tuesday-Friday, June 5-8, 1990 University of North Carolina at Chapel Hill An invaluable opportunity for R&D scientists in the organic, medicinal, and biochemical fields What You'll Learn: • The ways molecular modeling can be applied to your work and experiments • How to work with MM2, SYBYL, MODEL, AMPAC, GAUSSIAN86, and ALCHEMY II • Tested methods for conducting energy optimizations, conformational searches, and molecular mechanics • How to work with six types of hardware-Apple, Digital, Evans & Sutherland, IBM, Silicon Graphics, and Tektronix • The limitations, precautions, and advantages of quantum and molecular mechanics • AND MUCH MORE!
•REGISTER T0DAY!« Enrollment is strictly limited to 25 participants. Call (800) 227-5558 and ask for ext. 6050. Or, use the coupon below to request a free descriptive brochure on this new, state-ofthe-art course. American Chemical Society Dept. of Continuing Education Meeting Code MOL90060 1155 Sixteenth Street, N.W. Washington, DC 20036 Please send me a free brochure on the ACS Short Course, Molecular Modeling: Methods and Techniques, to be held June 5-8,1990, at Chapel Hill, NC Name Title Organization Address City, State, Zip _ MOL90060
