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Gas Chromatography to be held at the ... 3:00 Diffusion and Mass Transfer Co- efficients in Packed .... Inc. Dr. Cohn was born in San. Francisco,. Cal...
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ANALYTICAL CHEMISTRY International Symposium on Advances in Gas Chromatography The University of Houston is sponsoring a Symposium on Advances in Gas Chromatography to be held at the Sheraton-Lincoln Hotel in Houston, Tex., on J a n u a r y 21 to 24, 1963. T h e meeting consists of invited papers by outstanding scientists from the U . S. and Europe. Topics include recent developments in the theory and practice of ionization detectors, gas chromatogr a p h y of n a t u r a l products, and new column techniques. Informal discussion groups on special topics are also planned. Attendance is limited and preregistration is necessary. Details and registration forms are available from D r . A. Zlatkis, Chemistry D e p a r t ment, University of Houston, Houston, Tex.

PROGRAM

NEWS etry: the Continuous Analysis of Fractions from Capillary Gas Chromatography. J. A. Dorsey, Shell Oil Co., Houston, Tex. 10:40 Studies on the Efficiency of Packed Gas Chromatographic Columns. D. D . DeFord, Northwestern University, Evanston, 111. 11:20 Recirculated Column for P r e parative Scale Gas Chromatography M. J. E. Golay, Perkin-Elmer Corp., Norwalk, Conn. T u e s d a y A f t e r n o o n , J a n u a r y 22 J . C . Winters, Presiding

1:30 Special Informal Session on Preparative Gas Chromatography 3:00 Diffusion and Mass Transfer Coefficients in Packed Gas Chromatographic Columns. J. H. Purnell, Cambridge University, Cambridge, England 3:40 Advances in the Theory of Plate Heights in Gas Chromatography. J. C. Giddings, University of Utah, Salt Lake City, Utah 4:40 Storage and Complete Automatic Computation of Gas Chromatographic Data. H. W. Johnson, Jr., Shell Development Co., Emeryville, Calif.

M o n d a y M o r n i n g , J a n u a r y 21

W e d n e s d a y M o r n i n g , J a n u a r y 23

A . Zlatkis, Presiding

R. A. Dinerstein. Presiding

9:00 Opening Remarks J. C. Allred, Vice-President, University of Houston L. T. Hallett, Editor, ANALYTICAL CHEMISTRY

9:20 A Sensitive Ionization Cross-Section Detector for Gas Chromatography. J. E. Lovelock, Baylor University College of Medicine, Houston, Tex. 10:00 A New Quantitative Detector. O. F. Folmer, Continental Oil Co., Ponca City, Okla. 11:00: A New Radioactive Gas Chromatographic Detector for the Identification of Strong Oxidants. B. J. Gudzinowicz, Monsanto Research Corp., Everett, Mass. M o n d a y A f t e r n o o n , J a n u a r y 21 S. dal Nogare, Presiding

1:00 Special Informal Conference on Capillary Columns. D. H. Desty, British Petroleum Co., Sunbury-onThames, England 3:00 Gas Chromatography and Inorganic Chemistry. C. S. G. Phillips, Merton College, Oxford, England 3:40 A New Column System for Gas Chromatography. R. P . W. Scott, W. G. Pye and Co., Cambridge, England 4:40 A New Concept in Gas Chromatography. H. R. Felton, E. I. du Pont de Nemours and Co., Wilmington, Del. T u e s d a y M o r n i n g , J a n u a r y 22 W . W . Brandt, Presiding

9:00 Theoretical and Practical Considerations on Choice of Solvent and Filling of Analytical and Preparative Columns. E. Bayer, Technische Hochschnle Karlsruhe, Germany 9:40 Rapid Scanning Mass Spectrom-

9:00 The Spreading of "Air Peaks" in Capillary and Packed Gas Chromatographic Columns. J. H. Knox, University of Edinburgh, Edinburgh, Scotland 9:40 Capillary Adsorption Columns. R. D . Schwartz, Shell Development Co., Houston, Tex. 10:40 New Types of Columns in Gas Chromatography. I Halasz, Institut fiir physikalische Chemie der Universitat Frankfurt am Main, Germany W e d n e s d a y A f t e r n o o n , J a n u a r y 23 C . H . Orr, Presiding

3:00 A Simple Compact Gas-Radio Chromatogram. A. T. James, National Institute for Medical Research, London, England 3:40 Radio Assay of Gas Chromatographic Compounds Labelled with Tritium. A. Karmen, National Heart Institute, Bethesda, Md. 4:40 Quantitative Aspects of Gas Chromatographic Separations in Biological Studies. E. C. Horning, Baylor University College of Medicine, Houston, Tex. T h u r s d a y M o r n i n g , J a n u a r y 24 O . L. Hollis, Presiding

9:00 Analysis of Flavors by Gas Chromatographic Techniques. A. I. M. Keulemans, Technilogical University, Eindhoven, Netherlands 9:40 Electron Capture Spectrometry of Biological Compounds. S. R. Lipsky, Yale University College of Medicine, New Haven, Conn. 10:40 Determination of Lead Alkyls by Electron Capture. H . J. Dawson, American Oil Company, Whiting, Ind.

11:20 Applications of the Methylene Insertion Reaction to Component Analysis of Hydrocarbons. I. Dvoretsky, Shell Oil Company, Houston, Tex. 12:00 Summary of Symposium. C. S. G. Phillips, Merton College, Oxford, England

Fisher, Labline, Sargent Winners Announced T h e winners of the annual Fisher, Labline, and Sargent Awards were announced at the 142nd ACS National Meeting in Atlantic City just before ANALYTICAL C H E M I S T R Y went to press.

T h e recipients and their biographies a p pear below. D r . D a v i d N . H u m e , Massachusetts I n s t i t u t e of Technology, was given t h e Fisher Award , i n Analytical Chemistry, sponsored by the Fisher Scientific Co. D r . H u m e is Professor of Chemistry at MIT. H e was born in Vancouver, B . C , b u t grew u p and a t tended public schools in Los Angeles, California. D r . H u m e received his B.A. from the University of California in 1939 and his M.A. in 1940. H e earned his P h . D . in 1943 from the University of Minnesota where his doctoral r e search was in physical and analytical chemistry. D r . H u m e worked with t h e M a n h a t t a n Project at the University of Chicago, and at the Clinton Laboratories, Oak Ridge, Tennessee. B y the end of the war he was in charge of all analytical research and service work a t the Oak Ridge plutonium plant. After the war, D r . H u m e t a u g h t a t the U n i versity of Kansas until 1947 when he joined M I T . Twenty-four students have earned the P h . D . degree under his direction. D r . Hume's fields of technical specialization are analytical chemistry, instrumental methods, polarography, radiochemical analysis, statistical m e t h ods, and complex-ion equilibria. H e is the a u t h o r of more t h a n 70 technical papers. H e is a consultant for t h e D u P o n t C o m p a n y a n d the Brookhaven National Laboratory, a m e m b e r of t h e Advisory Committee for Analytical Chemistry of the Oak Ridge National Laboratory, and an editor for t h e McGraw-Hill Advanced Chemistry Series. Professor H u m e has served as a member of the advisory board of ANALYTICAL

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NEWS National Science F o u n d a t i o n - N a t i o n a l Research Council, International Union of P u r e and Applied Chemistry. He is a member of the ACS, Sigma Xi, Phi L a m b d a Upsilon, and a Fellow of the American Academy of Arts and Sci­ ences.

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ANALYTICAL CCEMISTRY

Dr. W a l d o E . Cohn, Oak Ridge N a ­ tional Laboratory, won the ACS Award in C h r o m a ­ tography and Electrophoresis, sponsored b y L a b line I n s t r u m e n t s , Inc. D r . Cohn was born in San Francisco, Cali­ fornia, and re­ ceived his B.S. from t h e Univer­ sity of California at Berkeley in 1931, M.S. in 1932, and his P h . D . in Biochem­ istry in 1938. After teaching at Berke­ ley and H a r v a r d from 1937 to 1942, D r . Cohn joined the M a n h a t t a n Project, first at Chicago, and later a t the Clinton Labs at Oak Ridge. T h e r e D r . Cohn worked with development of radioiso­ tope production and distribution meth­ ods which culminated in the general distribution of radioisotopes produced in the Oak Ridge reactor. H e also in­ vestigated the ion exchange chromatog­ raphy of fission products, which re­ sulted in the first separation of the rare earths b y this method, leading to the first isolation of element 61. Since 1948 D r . Cohn, as a Senior Biochemist with O R N L , has concentrated on in­ vestigations of nucleic acid structure, chemistry and enzymology. D r . Cohn pioneered in ion exchange c h r o m a t o ­ graphic methods for biochemistry. H e is a u t h o r or coauthor of more t h a n 60 publications. D r . Cohn is a member of the E d i ­ torial Board of the Journal of Biologi­ cal Chemistry, and a m e m b e r of the American Society of Biological C h e m ­ ist, Biochemical Society (London), ACS, and American Association for t h e Advancement of Science. • D r . H o w a r d V . Malmstadt, Univer­ sity of Illinois, has been named the winner of the 1963 ACS Award in Chemical I n s t r u ­ mentation spon­ sored b y Ε . Η . Sargent and Co. Dr. Malmstadt was b o r n in M a r i ­ nette, Wisconsin, and received his B.S. degree from the University of Wisconsin in 1943. After three years in the U. S. N a v y in electronics and radar, he r e t u r n e d t o t h e

NEWS University of Wisconsin and earned his M.S. in 1948 and his Ph.D. degree in 1950. Dr. Malmstadt joined the faculty at the University of Illinois in 1951, and he was promoted to Pro­ fessor of Analytical Chemistry in 1961. Dr. Malmstadt has contributed to analytical chemistry by the develop­ ment, in conjunction with the Ε. Η. Sargent Co., of automatic titrimeters. lie also developed a graduate course "Klectronics in Analytical Instrumen­ tation" which was described in ANA­ LYTICAL CHEMISTRY, Feb., 1961.

Professor Malmstadt was awarded a Guggenheim Fellowship in 1960, at which time he investigated spectro­ scopic laboratories in Europe. He has authored or eoauthored 58 technical papers, and has written a book "Elec­ tronics for Scientists" published in June of this year by W. A. Benjamin, Inc.

1962 Harvey W . W i l e y Award Milton S. Schechter of the Agricul­ tural Research Service, II. S. Dept. of Agriculture, has been selected to receive the 1962 Harvey W. Wiley Award of the Association of Official Agricultural Chemists. Mr. Schechter was chosen for his numerous brilliant contributions to the development of analytical methods for insecticides and their residues and for his outstanding accomplishments in the development of new insecticides during his 25 years of service with the Dept. of Agriculture. Many of his contribu­ tions have achieved world recognition, particularly the standard "SchechterHaller" colorimetric method for DDT residues, the colorimetric method for residues of benzene hexachloride, and the development of a general route for the synthesis of pyrethrin-like insecticidal esters such as allethrin. Mr. Schechter is in charge of the project on the development of analyti­ cal methods for insecticides and their residues for the Pesticide Chemicals Research Division, of the Agricultural Research Service. The Harvey W. Wiley Award was established in 1956 by the AOAC in honor of the founder of the original Food and Drug law and of the AOAC, and is given annually to a scientist who has made an outstanding contribution to the development of methods for the analysis of food, drugs, cosmetics, feeds, fertilizers, or pesticides, or for use in general analytical chemistry. The Award of $500 is presented at the Asso­ ciation's meeting in the fall.

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NMR/EPR Workshop The 6th Annual Varian N M R / E P E Workshop will be held at the Labora­ tories of the Instrument Division of Varian Associates, Palo Alto, Calif., November 5 to 9. The emphasis, academic in nature, will be on the basic principles and ap­ plication of N M R / E P R and the lab­ oratory operation of instrumentation. A nominal charge of S50 will be made for participation in the workshop. However, this charge will be waived for registered graduate students who ap­ ply for admission with the approval and support of their university or college and faculty advisor. Further details are available from Varian Associates, Palo Alto, Calif.

Symposium on instrumentation in Textile Dyeing and Finishing The American Association of Textile Chemists and Colorists will include a technical session on instrumentation in its program for the National Conven­ tion to be held in Atlanta, Ga., Novem­ ber 14-17, 1962. The program has been announced by Dr. Gertrude A. Lathrop, chief chemist, Old Fort Finish­ ing Plant, Old Fort, N. C , who is chairman of the symposium. Three papers to be presented are of interest to analytical chemists: Infrared Spectroscopy Applied to Some Dyehouse Problems. J. A. Rayburn, J. M. Fields, Nancy Moore, and J. W. Weaver, Cone Mills Research and Development Division. Microscopical Techniques in Finish­ ing Research. Mary L. Rollins, South­ ern Regional Research Laboratory. Infrared Spectra of Selected ResinTreated Cottons. V. W. Tripp, E. R. McCall, and R. T. O'Connor, Southern Regional Research Laboratory.

International Symposium on Humidity and Moisture The 1963 International Symposium on Humidity and Moisture-Measure­ ment and Control in Science and In­ dustry will be held May 20-23, 1963, in Washington, D. C , under the joint sponsorship of the National Bureau of Standards, the U. S. Weather Bureau, the American Society of Heating, Re­ frigerating, and Air Conditioning Engi­ neers, the Instrument Society of America, and the American Meteorolog­ ical Society. The Symposium will review the state of the art, and present the results of original research and development work

on the measurement and control of humidity and moisture in the physical, engineering, meteorological, agricul­ tural, and biological sciences. Because of the range and breadth of fields that will be covered, the sessions and pro­ ceedings will be definitive sources of information on hygrometry and mois­ ture. Individuals from many countries will attend and participate. Commer­ cial and scientific instruments and equipment will be exhibited. Sessions will be held on the follow­ ing subjects: fundamentals, standards, principles and methods of measuring humidity of gases, principles and meth­ ods of measuring moisture in liquids and solids, applications, and methods of control. Original papers and critical reviews on the above subjects will be con­ sidered for presentation. Titles and substantive abstracts of approximately 300 words must be submitted in tripli­ cate by Nov. 1, 1962. Papers will be accepted or declined by Dec. 1, 1962. Manuscripts of the papers must be sub­ mitted in triplicate by June 1, 1963. The language of the Symposium and the published Proceedings will be English. Abstracts and papers should be sent to: Arnold Wexler, Chairman, Program Committee, National Bureau of Stand­ ards, Washington 25, D. C.

Chemical Control Problems The Fifth Conference on Chemical Control Problems, sponsored annually by the National Plant Food Institute meets October 8 at the Sheraton-Gib­ son Hotel in Cincinnati, Ohio. Included in the program are discus­ sions of preparation and distribution of samples for collaborative analysis, fu­ ture instrumentation in the fertilizer laboratory, and statistics as a tool for analytical problems. An open forum will be held following the day's agenda of speakers for discussion from the floor. For details contact Dr. Vincent Sauchelli, conference chairman, Na­ tional Plant Food Institute, 1700 Κ St., N.W., Washington 6, D. C.

Fractional Factorial Experiments Course A two-day course on Fractional Fac­ torial Experiments, sponsored by the Chemical Division of the American Society for Quality Control will be held at the Downtowner Motor Inn, Kingsport, Tenn., November 9 to 10. For further details contact R. G. Nations, Tennessee Eastman Co., Kingsport, Tenn.

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National Conference on Air Pollution

Tenth Hot Laboratory and Equipment Conference

Surgeon General Luther L. Terry of the Public Health Service has called a conference on air pollution to be held in Washington, D. C , Dec. 10-12, 1962. Participants will include health officials, engineers, physicians, scientists, legislators, industry spokesmen, and representatives of labor and civic organizations. The conference will be open to the general public. For more information write: Executive Secretary, National Conference on Air Pollution, Public Health Service, IT. S. Dept. of Health, Education, and Welfare, Washington 25, D. C.

The Tenth Hot Laboratory and Equipment Conference will be held the week of November 26, 1962, in Washington, D. C , as part of the Joint Winter Meeting of the American Nuclear Society, The Atomic Industrial Forum, and the AtomFair nuclear industry exhibit. The conference studies the design, construction, operation, and management of Hot Laboratories, and the devices and materials, and research and process equipment. Further details are available from the American Nuclear Society, Hot Laboratory Division, 86 E. Randolph St., Chicago, 111.

Activation Analysis

Industry Items

Two regional scientific symposia on "New Developments in Activation Analysis," will be held in Pittsburgh and Chicago in October by General Atomic Division of General Dynamics Corp. and ten other co-sponsoring organizations. The Pittsburgh meeting is scheduled for Monday, October 15, at the Pittsburgh Hilton Hotel. The Chicago meeting will be held Wednesday, October 17, at the Congress Hotel. General Atomic is principal sponsor of the symposia. Co-sponsoring organizations are: Kaman Nuclear, Nuclear Data, Inc., Philips Electronic Instruments, Picker X-Ray Corp., Radiation Counter Laboratories, Inc., Radiation Instrument Development Laboratory, Inc., Sames USA, Inc., Technical Measurement Corp., Texas Nuclear Corp., and II. S. Radium Corp. Purpose of the symposia is to acquaint scientists in various fields with the nature and capabilities of activation analysis, and to review new developments and new areas of applications. Information regarding invitations to the symposia may be obtained from H. R. Zeitlin, General Atomic, P. 0 . Box 608, San Diego 12, Calif.

Angstrom, Inc. is the name of a new company of spectrographic consultants which specializes in optical emission and x-ray spectrochemistry. The new firm will service and install spectrochemical equipment, train and instruct technicians or professional personnel, evaluate control problems, and design special purpose accessories. The company's address is: 2454 W. 38th St., Chicago 32, 111.

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Mid-Atlantic States Section of Air Pollution Control Association will hold its fall technical meeting on October 24 at the Nemours Building in Wilmington, Del. Theme of the meeting is Air Quality Standards. Programs may be obtained from Mr. W. R. Chalker, E. I. du Pont de Nemours & Co., 13W8 Lonvicrs Bldg., Wilmington 98, Del.

Beckman Instruments, Inc., has started construction of a new $1,250,000 engineering wing at its Fullerton, Calif., headquarters plant. The company specializes in the development and manufacture of electronic instrumentation for scientific, industrial, medical, and space-defense applications. The new wing will increase the company's total plant space at Fullerton, headquarters for four of Beckman's seven domestic operating divisions, to some 500,000 square feet. Fisher Scientific announces changes in its laboratory instrument and appliance financing plan including a reduction in down payment from the original 20% to 10%. Two plans are available ; one designed for financing durable equipment costing $1000 or more, and the other is a leasing plan with purchase options for equipment costing $5000 or more. For more information write: Fisher Scientific Co., 711 Forbes Ave., Pittsburgh, Pa. General Atomic announces an Activation Analysis Research and Service Program. Routine analytical services are offered plus a Participant Program whereby the nuclear reactor and laboratory facilities of General Atomic can be used by individuals. For more in-

NEWS formation, write General Atomic, Box 608, San Diego 12, Calif. JKM Instrument Co., Inc., of Dur­ ham, Pa., has announced the establish­ ment of an export division to handle foreign sales of its line of laboratory equipment and glass products. The new division is located at 1510 Race St., Philadelphia. JKM also recently an­ nounced the acquisition of Central Glass Blowing Co., Lanark, Pa. Mine Safety Appliances Co., Pitts­ burgh, Pa., has acquired the process control instrument business of the Perkin-Elmer Corp. The line pri­ marily consists of gas chromatography instruments for chemical, petroleum, and similar plant processes. Mine Safety Appliances is primarily con­ cerned with process instrumentation, while Perkin-Elmer is mainly inter­ ested in analytical instrumentation. Research Specialties Co. has opened an instrument servicing center at 195 Nassau Street, Princeton, N . J. I t will offer sales and services to users of gas chromatography and other in­ strumental analytical methods. Later this year a demonstration laboratory for RSCo's gas chromatography instru­ ments will be opened; followed by ex­ pansion of facilities to demonstrate the company's other product lines—auto­ matic chemical analysis systems, paper and thin layer chromatography equip­ ment, and general biochemical labora­ tory instruments. Servonuclear Corp., manufacturers of electrophoresis tanks and high volt­ age power supplies, has changed its corporate name to Savant Instru­ ments, Inc. and moved to a new plant at 221 Park Ave., Hicksvillc, Ν . Υ. The new name reflects the company's major interest in the field of research laboratory instrumentation and sys­ tems. Tracerlab, a division of Laboratory for Electronics, Inc., has an improved Film Badge Service. The new "TwinFilm" Service offers greater accuracy at lowest possible dosage levels—at lower cost. Volk Radiochemical Co. h a s opened a new office at 2446 Reedie Dr., Silver Spring, Md., for the benefit of isotope users in Va., Md., and D. C The Volk product line includes stable and radioactive isotope labeled com­ pounds for chemical and biochemical use as well as radioactive pharmaceuti­ cals for clinical diagnosis and therapy.

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