4000 3000
2000
CM"'
!
1W^
IO00
90O
80O
700
i ".' 1* RAW SAMPLE SURVEY -Total sampfe is charact e r î r e d by I R o p t i c a l analysis. Then . ί.
mâmmà WAVELeNGTH-tMANS)'
" "
*
*
«
ISAMfclfÊÏ
ANALYTICAL DOUBLE 5ΠΕ«
y'-^^^^^^B^-life^B^lfe^l ;W;:ttv
il^iiiilÉIÉi.
2. F R A C T I O N A T I O N " M i x t u r e pf dichloroethylene isomers is. sepa r a t e d ;by t h e ; F*-E 1 5 4 V a p o r Fracto£neter equipped with a hïgh- v capacity preparative column, "f rans-diçh ibroethy lene is coU lected by low^tëmperature con- densationas it is eluted. ,
FRACTION OF SAMPLE
2000
-4000 3OO0
5Γ"ΐτΐ~
(f~ L Λ
τ«4 •
1
*cJ ' ,'
sS?1 ! 1
Infrared
f"
....
I
• • ] " " • •
$
! 1 1 β
;
I0OO 90O
;
j—L_#i
!
A/ If 1i
!f jI
800
~"1T ' ' ' ; ! ι 1
~m « 1/ ip 1
il 1:
~*
ι
....
À f
SPSS!* I4~
CM* 1
I5O0 •ri-r,
II
Γ
τ
-t tej
I
!
T^-
; 1 i m ;ψ >V
π
; ' t •
si \ /}*«'*%.
ι
' v%i >;-. j β] ; γ &""
j
j ί
f
| s~~ Γ
I
|\
iy ô ?(MICRONS) J *ο I I WAVELENGTH
700
i " " - ^*fr 1 ' , !
I2
'—l
13
and Gas Chromatography . . · Y(mr Mosi Poîverful Analytical
An analytical system that enlarges the specific capabilities of two basic analytical methods now provides f a s t and positive answers to difficult analytical problems. Here's how i t works : The Perkin-Elmer Model 154-C Vapor Fractome t e r — a new gas chromatographic instrument —first separates the sample into relatively pure fractions, recorded fractograms providing the quantitative information. Trie fractions are collected, and then run through the P-E Inf racord,® a new low-cost ($3,850), compact, double-beam, bench spectrophotometer. Here, infrared analysis supplies the detailed qualitative data difficult to
1A
t5
WMMwmmm ^analysed A&I0H$4ESÇU^ "fra