Analytical Techniques - American Chemical Society

Mawr College and her PhD in chemis try from Stanford University. Her current research interests include the synthetic and analytical chemistry of gluc...
7 downloads 0 Views 1MB Size
SURFACE AREA ANALYZERS SUPERIOR QUALITY A N D SERVICE — OFF THE SHELF DELIVERY

MODERN, RELIABLE DYNAMIC FLOW used by both instruments, with any non-corrosive M adsorbate. No ideal gas Β corrections or void volume measurements required. Extreme sensitivity for a wide range of applications.

MONOSORB By far the world's fastest and most versatile single point B.E.T. surface area analyzer. Direct digital readout of surface area with extreme simplicity and accuracy. Ideal for process monitoring and other quality control applications.

QUANTASORB A very fast, accurate and versatile instrument for surface area, pore size distributions, adsorption and desorption isotherms. Ideal for measuring chemisorption uptake.

QUANTACHROME CORPORATION

POWDER INSTRUMENTATION

Six Aerial Way, Syosset, NY 11791 TWX: 510 221 2239 · TEL: 516 935-2240

CIRCLE 180 ON READER SERVICE CARD

Analytical Tech­ niques in Occupa­ tional Health Chemistry Analytical Technique in Occupational Heaim Chemistry

Based on a symposium sponsored by the Division of Chemical Health and Safety of the American Chemical Society. An excellent state-of-the-art review of new and improved instrumental methods for analyzing potentially hazardous chemicals in the workplace. General methods of air sampling as well as specific measurement techniques for as­ bestos, silica, organics. and metals are ex­ amined in this sixteen-chapter volume. This handy volume will serve as a valuable introductory text for those entering industrial/occupational health chemistry and as a ready reference for the experi­ enced industrial hygiene chemist who wishes to keep abreast of current de­ velopments. CONTENTS Generation of Test Atmospheres • Analysis of Asbestos and Quartz · Quantitation Using X-Ray Powder Diffrac­ tion · Determination of Respirable Quartz by Infrared Analysis · High Performance Liquid Chromatography · Analysis of Aromatic Amines · Determination of Methyl Isocyanate · Analysis of Polynuclear Aromatic Hydro­ carbons Using Ternary Solvent Systems · Vinyl Ace­ tate in Air · Airborne Contaminants · Organic Solvent Vapors · Monitoring Airborne Contaminants in Chemical Laboratories · Sampling for Mercaptans · Atomic Ab­ sorption Spectroscopy · Metals in the Workplace Envi­ ronment · Protein-Bearing Particles in Grain Elevator Air

ACS Symposium Series No. 120 Donald D. Dollberg, Editor National Institute for Occupational Safety and Health Allen W. Verstuyft, Editor Chevron Research Company

Commun. 1981, 325-27; Surman, D. J.; Vickerman, J. C. J. Chem. Soc. Chem. Commun. 1981,324-25. (38) Williams, D. H.; Bradley, C ; Bojesen, G.; Santikarn, S.; Taylor, L. C. E. J. Am. Chem. Soc. 1981, 103, 5700-5704. (39) Barber, M.; Bordoli, R. S.; Sedgwick, R. D.; Tyler, A. N.; Whalley, Ε. Τ. Biomed. Mass Spectrom. 1981,8,33742. (40) Morris, H. R.; Panico, M.; Barber, M.; Bordoli, R. S.; Sedgwick, R. D.; Tyler, A. N. Biochem. Biophys. Res. Commun. 1981.101. 623-31. (41) Fenselau, C ; Cotter, R. J.; Hansen, G. E.; Chen, T.; Heller, D. N. J. Chromatogr. November 1981. (42) Fenselau, C; Cotter, R. J. Pure Appl. Chem., in press. (43) Rinehart, K. L.; Gaudioso, Ζ. Α.; Moore, M. L.; Pandey. R. C; Cook, J. C; Barber, M.; Sedgwick, R. D., Bordoli, R. S.; Tyler A. N. J. Am. Chem. Soc. 1981, 103, 6517-20. (44) Barber, M.; Bordoli, R. S.; Sedgwick, R. D.; Tyler, A. N. "Proceedings of the 8th International Symposium on Mass Spectrometry in Biochemistry, Medi­ cine, and Environmental Research," Venice, Italy, 1981. (45) Burlingame, A. L.; Ballou, C. E.; Dell, A. "Proceedings of the 29th Annual Con­ ference on Mass Spectrometry and Al­ lied Topics," Minneapolis, Minn., 1981; pp 528-29. (46) Matsuo, T.; Matsuda, H.; Katakuse, I.; Wada, Y.; Fuiita, T.; Hayashi, A. Biomed. Mass Spectrom. 1981,8, 25-30. (47) MacFarlane, R. D.; McNeal, C. J.; Hunt, J. E. Adv. Mass Spectrom. 1979, 8, 349-54. (48) McNeal, C. J.; Ogilvie, Κ. Κ.; Theriault, N. Y.; Nemer, M. J. J. Am. Chem. Soc, in press. (49) McNeal, C. J.; Ogilvie, Κ. Κ.; Theriault, N. Y.; Nemer, M. J. J. Am. Chem. Soc, in press. (50) Chait, B. T.; Shpungin, J.; Gisin, B. F.; Field, F. H. "Proceedings of the 29th Annual Conference on Mass Spec­ trometry and Allied Topics," Minneapo­ lis, Minn., 1981, ρ 734. (51) Schueler, B.; Krueger, F. R. Org. Mass Spectrom. 1979,14, 439-41. (52) Kamensky, I.; Hakansson, P.; Sundqvist, B. Nucl. Inst rum. Methods, in press, 1981. (53) McNeal, C. J. Anal. Chem. 1982,54, 43 A.

318 pages (1980) Cbthbound $28.00 LC 79-28460 ISBN 0-8412-0539-6

Order from: SIS/American Chemical Society 1155 16th St.. N.W./Wash., D.C. 20036

116 A · ANALYTICAL CHEMISTRY, VOL. 54, NO. 1, JANUARY 1982

Catherine Clarke Fenselau is asso­ ciate professor in the Department of Pharmacology at the Johns Hopkins School of Medicine in Baltimore and director of the NSF Regional Instru­ mentation Laboratory there. She re­ ceived her AB degree from Bryn Mawr College and her PhD in chemis­ try from Stanford University. Her current research interests include the synthetic and analytical chemistry of glucuronides, chemical mechanisms for the biological activities of alkylat­ ing agents, and mass spectrometry.