APPENDIX A - ACS Symposium Series (ACS Publications)

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APPENDIX A Chromatographic Techniques for the Separation of Polymethoxyflavones from Citrus (Chapter 1) Ram M. Uckoo, G. K. Jayaprakasha, and Bhimanagouda S. Patil*

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Vegetable and Fruit Improvement Center, Department of Horticultural Sciences, 1500 Research Parkway Ste A120, Texas A&M University, College Station, TX 77845 *E-mail: [email protected]

© 2012 American Chemical Society Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

Downloaded by UNIV LAVAL on July 10, 2016 | http://pubs.acs.org Publication Date (Web): May 25, 2012 | doi: 10.1021/bk-2012-1093.ot002

572 Figure 1. Structures of polymethoxyflavones isolated from citrus.

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

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573 Figure 2. Structures of hydroxylated polymethoxyflavones isolated from citrus.

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

574

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Table 2. 1H NMR of polymethoxyflavones isolated from citrus species

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

575

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Table 2. (Continued) 1H NMR of polymethoxyflavones isolated from citrus species

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

13C

NMR of polymethoxyflavones isolated from citrus species

576

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Table 3.

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.

577

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Table 3. (Continued) 13C NMR of polymethoxyflavones isolated from citrus species

Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.