ARTHUR H. THOMAS CO

FIRST CLASS. PERMIT NO. 1538. NEW YORK, N. Y. BUSINESS REPLY CARD. NO POSTASE STAMP NECESSARY IF MAILED IN THE UNITED STATES...
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READERS' INFORMATION SERVICE Optical Equipment Ovens & Incubators Oxygen Bombs pH Indicators DH M te Photometers' . . . . . . Polarimeters

59 129 127 63 40 i « '. '. '. '. '. 58, 114 12

Polyamiaocarboxylic Acid Compounds. . Potentiometer Recorders Preaees

Pumps Radioactivity Safety Devices Radiochemicals Reagents Recorders Refrigerated Baths _ . Rotameters

5 13

32, 64 87, 133 124 66, 95 40, 44, 65 68,86,144,148 10 . 3

Spectra Spectrograph^ Equipment Spectrometers

85 24 71, 149

Spectrophotometers. . .2,22,69,108,112,151 Spencer Photomicrographic Cameras . . 20 SUrrer8

60

Syringes

47

Table Tops Taper Sleeves

27 90, 125 36 23 126

combustion apparatus

7 141

Testing Machines Thermistors Titrators Triethyl Phosphate

137 92 1, 34, 82 153

Valves Viscometers

71, 117 30

Ware, Alumina

70

Ware, Fused Quartz Safety Enclosures Sample Changers Sample Handling Systems Scalers Scales

oniaer

91

Ware_ GIaB8

39> 42> 122>

u 2

Ware> plastic Ware, Porcelain

38

X-Ray Spectrometry

45

s6

for determination of halogens, sulfur, traces of metals, etc., in organic materials

FIRST CLASS PERMIT NO. 1538 NEW YORK, Ν. Υ.

BUSINESS REPLY CARD NO POSTAGE STAMP NECESSARY IF MAILED IN THE UNITED STATES

READERS' INFORMATION SERVICE Analytical Chemistry 430 Park Avenue New York 22, Ν. Υ.

A simplified technique for catalytic com­ bustion of organic materials in oxygen. The procedure converts organic materials into soluble combustion products which are then analyzed by usual inorganic gravimetric or volumetric methods. Consisting of a heavy wall flask, of borosilicate glass, with ground glass stopper with attached platinum wire gauze sample carrier and specially cut low ash paper sheets which serve as sample holders. In use, sample is placed in the platinum carrier and the flask is charged with a small amount of absorbing liquid and with freeflowing oxygen. The paper is ignited; stopper with sample is seated in the flask and flask inverted at an angle. Combustion proceeds at high temperatures and combustion prod­ ucts are absorbed in the liquid. Titrations can then be made directly in the flask. Results compare favorably, i.e., within ± 0.3%, with conventional methods. Because of low cost, time and space saving features, the method is finding wide use for many sub­ stances which undergo complete combustion. See Wolfgang Schoniger, Mikrochimica Acta, 1956, Heft 1-6, pp. 869-876. 6470-E. C o m b u i t l o n A p p a r a t u s , T h o m a · SchSnlger (Schdnlger Fla»k), as above described, 300 ml capacity, for samples up to 10 mg 28.35 6 4 7 0 - G . Ditto, as above but with 500 ml flask, far iamples up to 100 mg 29.0Ό

ARTHUR H. THOMAS CO. Laboratory Apparatus and Reagents VINE ST. A T THIRD

PHILADELPHIA 5, PA. More and mora laborofories RELY ON THOMAS Circle No. 93 on Readers' Service Card

116C

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ANALYTICAL CHEMISTRY