ARTHUR H. THOMAS COMPANY - Analytical Chemistry (ACS

ARTHUR H. THOMAS COMPANY. Anal. Chem. , 1959, 31 (2), pp 98A–98A. DOI: 10.1021/ac60146a797. Publication Date: February 1959. ACS Legacy Archive...
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7ΑΟΜ04. HIGH TEMPERATURE

COMBUSTION FURNACE • A new furnace for general use in micro and semimicro combustions at temperatures up to 1150°C (2100°F) • Dual thermocouples for determination of both element and tube temperatures • Long-life heating element of new design, and Pyroceram end plates

For milligram and centigram procedures. Designed specifically t o provide a temperature of 1150°C (2100°F) as required for t h e direct determination of oxygen by the Unterzaucher procedure, b u t suitable for all microchemical combustion techniques requiring elevated temperatures. Accommodates combustion tubes u p t o 18 m m outside meter. A built-in Platinum-Platinum 1 3 % Rhodium thermocouple is supplied with t h e Furnace. An external removable thermocouple of identical characteristics is offered for direct determination of temperatures existing within the combustion tube. A switch permits reading of temperatures of either thermocouple on the pyrometer. ^J The replaceable heating element is of new design,

tor switch for the two thermocouples, mounted pyrometer, pilot light and adjustment knob for the built-in variable input transformer, Housing· is of sheet metal finished in two tone * T r t h v e n t i l a t e d t o n o f anodized aluminum ^ t w o \ i r c u l a r e î d pVtes a?e of l o n g S n g p y r o C e r a m and are held in position by two aluminum rings. Overall dimensions of the Furnace, 1334 X 1234 X 8Vs inches; height t o combustion tube 9 inches. Use of the 1 KW constant voltage transformer is recommended to protect the heating element and to provide a temperature at center of heating chamber constant within 5°C olts irrespective of line fluctuations in t h e r n e 9 t o 130 , ^ § .° , ,Y - Without transformer, a change ot 5% m input voltage results in changes up to lo C at H50°C.

providing a heating c h a m b e r approximately 280

5675-B.

mm long X 19 mm inside diameter, with a groove

as above described, with built-in Platinum-Platinum 13% Rhodium

On b o t t o m t o a c c o m m o d a t e t h e i n t e r n a l t h e r m o COUple. Special K a n t h a l r e s i s t a n c e w i r e is WOUnd

in coils, arranged t o provide a zone approximately 100 m m long with uniform temperature when operating a t 1150°C. A l t h o u g h t h e construction

Furnace, High Temperature Combustion, Thomas,

Thermocouple for determining temperature at the element, but without External Thermocouple or Constant Voltage Transformer.

Power

consumption 650 watts. For use on 115 volts, 50 or 60 cycles, a.c 425.00

5675-C.3 0 Ditto, but with 1 KW Constant Voltage Transformer. volts 6 0 c cle a c on,

insures a long element life, it can be conveniently

For 9 5

r e p l a c e d in t h e e v e n t of a b u r n o u t .

5675-D.

"'

-

v *· - ·

y

External Thermocouple f o r determining

Control panel contains on-off power switch, selecMore detailed QUALITY AND SERVICE

A.H.T.CO. LABORATORY

APPARATUS

information

596.00

Ditto, but with 1 KW Constant Voltage Transformer and temperatures within the

tube. For 95-130 volts, 60 cycles, a.c only sent upon

636.00

request

ARTHUR H. THOMAS COMPANY More and more laboratories rely on Thomas/ tas f

Laboratory

Apparatus

and

Reagents

/ VII VINE ST. AT 3 R D · PHILADELPHIA S, PA. Circle No. 117 on Readers' Service Card 98 A

·

ANALYTICAL CHEMISTRY