AUTHOR INDEX ANALYTICAL CHEMISTRY VOLUME 35-1963
.................... ................... ..................... ..................... ...................... ......................
January.. February.. March.. April.. May.. June..
.................... .................. ............... ................. ............... ................
1-1 20 121-264
July.. August.. September.. October.. November.. December.
265-424 425-600 601-776 777-936
.....
Annual Review (April).
ABUOTT, J . c.. A N D COLL.4'T J. W. Indirect POhrORraDhiC dete :mination of . - _ acids .............................. 8n9 ABDELRAHMAN,>I. M. A . See El Khad e~~~. n . H. S. Asri.. KENNETH.A S D I ) . % I J N E \V. ~ . B. An automatic, continuoi.ely ~nririble a:sanuator for gas chroinllrogrur,l.y ~ . . (aid). .............................. AND DESCHIIERTZISG, H A N N I I L ~ L . bual-chamber micro cross-section eas analysis detector for Dertnanent . . . ~... " (corresp.) . . . . . . . . . , . . . . , . . . . . . . . ., . . l i s 4 ABERNETHY R. F A N D ~ H h I S I . O S THEODORE. Solid a n d gaseous fuels ( k v . ) , , 78K ABR-~MS, JOAN.See Kesner, Leo. ABRIMS, S. T. See Merritt, Jack. ACKI~AN,R. G.. A N D BDROHER,F. D. T h e effect of detector bloiik foulinr on observed separations in ga.3 liquid clironiatography (corresp.) 413 __ Quantitative gas graphic estimation of 1 in aqueous media. . . . . . . . . . . . . . . . . . . 647 ADArde M. L. See Swann, M . H. ADAMS: R. N. See Kitagawa Toyokiclii. ADLER, NORMAN. A partial condensation variable reflux stillhead f x the distillation of trace components. , . , . , , . . , . . i?4 AFFSPRUNP,H. E., AND AIICHER,V. S. Determination of hexafluoropliosphate by amperometric titration with tetraphenylarsonium chloride. . . . . . . . . . . . . 976 - Gravimetric determination of hexafluorouhosphate a s tetra~~lienylarsonium hexafluorophosphate . . . . . . . . . . . . . . . . 1fJ1? Aoazzr, E. J., BURTNER,I). C CRITTESD E N , D. J., A N D PATTEI
B I ~ Q S. , P, F E R U S U O , QuIxrus. A N D FREISER, ~ I E N H P .A spectroIhototuetric a n d notentiometric studv of certain metal cliilates of pyridine-2,tf-dialdoxiiiie BAILEY It. F AID Ross D. A. Determination oi'oxygen in kalliurn arsenide by neutron activation analysis. . . . . . . . . BALOGA,MICHAEL,AND EARLEY, J . 1;. Evaluation of reaction rates froin transmittance-time traces (corres .) 1 % . 4 > I m x c Kw E See Innes, B. ' ' ' ' ' ' B.4NICK,
2
6. i.,' ~ A R O T H E R S , G.
A,.
ill) i!lI
I1 li
.ilIj
UONALDSOS, \%.T. Determination of americium-243 in curium-244 (oorresp.) . 1312 w. M., JR., AND. HOLZER,R. I\. Titration of acids in nonaqupous solvents. Potentiometric titration of Iithium(1) and sodium(1) in pyridine.. . . 1 4 1 3 BANKS, C. V. See Kaniin. (;. J., and Onishi, Hiroshi D A X T A , H. E. See Volbortli, Alesis. B.'See I. Kepr.er, B. L., a n d King, R. M. H E R X A NH. , B., AND BARD,4 . J . Cyclic chronopotentiometry. E'iffusion controlled electrode reaction o ' a single com1121 ponent s y s t e m . . ..................... -, TATWAWADI! S. V,., A N T BARD,A. J. Chronopotentiometric measurement of adsorption b y current reversal (sci. 2210 commun.) . . . . . . . . . . . . . . . . . . . . . . . . . . HERMANS, bl. E . A. See Altinann, C. J. G. HERNANDEZ, R.%YMOFD,JR.,.\ND ALEXROD, I,. R. Chromatographic separation of the steroids from total lipide extracts. . . 80 H E R N D O N J. , F., TOUCHSrONE. J. c,., WHITE,G. R., A K D DAVIS C. N. Horizontal chromatography accelerating apparatus. Separation of dyes and indica238 tors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . HERRERO-LANCIN.4, h1 ANOLITA, A N D WEST. T. S. -4new sensitive and selective spectrophotometric reaction fo' the determination of trace amounts of calcium. . . . . 2131 HERRINGTON, JOHN. See Ei.ans, Clayton. RUDOLF. HERSCH,P A U L ,AND DEURIKQER, Galvanic monitoring of oxsine in a i r . , . , 897 HEUSER,9. G . Volumetric jetermination of concentrations of sulfuvyl fluoride in 1476 air. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . HILL,H. I. See Golay, hl. J. E. HISHTA,CHARLES, AND BOMSTEIN, JOSEPH. Determination of benzyl :hloroformate b y gas chromatography 3f its amide. Extension of the principle t o other acid chlorides.. .......................... 65 . Gas chromatography (If polar compounds of low volatility (ccrresp.) . . . . . . 924 HITCHCOCK, R. B.. D E A N ,J. A., H A N D L E Y , T. H. Tri-n-butylphosphine sulfide as 254 a n organic extractant (sci. commun.) . . . HIVELY,R. A. Assignment of cis-trans configuration to mono-olefin pairs b y gas chromatography. . . . . . . . 1921 HOBART, E . W. See Jaworo H. D. See Lewis, C . P. HOBERECHT. HODQSON,F. N., DESJARDNS, M I C H E L , A N D BAUN, W. L. -4 convenient mass reference d a t e for use in m a r k source mass specirography (aid). .. . . 1112 HOELKE,C. W. K. See Mathers. W: G.' ' ' HOFF, J. E., AND FEIT,E . D. Functional group analysis in gas chromatography. Treatment of vapors with selective reagents (sei. commun.) . . . . . . . . . . . . . . . 1298 HOFYANN, J. E . See Pobiner, Harvey. HOLBROOK, W. B. See Booman, G. L. HOLLIS,D. P. Quantitative analysis of aspirin, phenacetin, a n d caffeine mix-
tures b y nuclear magnetic resonance spectrometry.. . . . . . . . . . . . . . . . . . . . . . . HOLT,B. D., AND GOODSPEED, H. T. Determination of nitrogen, oxygen, and hydrogen in metals b y inert gas fusion. A manometric method. . . . . . . . . . . . . . . . . . HOLZER, R. A. See Banick, W. M., Jr. HOPKINSP A See Shepherd G. R. HO, P. P. L.* AND MARSH, hi. nI. Some applications of ion exchange membranes in automatic coulometric aqueous acidbase titrations.. ..................... HORNINQ, E . C. See VandenHeuvel, W . J. 9. -, hiADDOCK, K. c.,ANTHONY, K. v., A N D VANDENH E U V E LW. , J. -4. Quantitative aspects t o gas chromatographic separations in biological studies (symp.) . . . . . . HOROWITZ, H. H., AND M E T Z Q E R GER, SHON. .I new analysis of thermogravimetric traces.. ...................... HORTON,-4. D., &{EYER! .A. s., JR., A N D BOTTS,J. L. Adaptation of a pas chromatograph for analysis of radioactive gas samples (aid) . . . . . . . . . . . . . . . . . . . . HORYATH, CSARA. See Halasz, Istvan. HOWARD, H. E . See Snyder, L. R. H. 0. HOWARD,J. M., AND SPAUSCHUS, Comparison of two colorimetric methods for determination of copper in mineral
1682
1510
618
526 1464
1988
...........................
-
1016
.IICHIRO. H. See Weber, C. W. Decimilligram
determination of nitrogen with simple sealed tube combustion m e t h o d . . . . . . . . . . . . . . 666 AND KIRSTEN,W. J. Simultaneous deiermination of carbon, hydrogen, 1522 nitrogen a t the decimilligram level. HSIETH,C.-C. See Lai. T.-T. HUANQ, T. C., WEFLER. VERNA, AND RAFTERY,ALAN. A simplified spectrophotometric method for determination of total and esterified cholesterol with tomatine (corresp.) . . . . . . . . . . . . . . . . . . 1757 HUDSON, R. L. See Parker, W. W. H U L L ,D . E. See Gilmore. .J. T. H U X E .D. M. The analysis for a profession (rept. for anal. chemists). . . . . . . .29A ( N'0.13) HUMPHREYS, W. G. See Armstrong, W. A. HUNEMORDER, E. J. See Mansell, R. E. HUKT,R. H. See Dorsey, J. A. H U K T E RI. , R.. AND WALDEN,31. I. C D. Russell. , ACETYLATIOS acid-catalyzed. determination of alkoxy groups in alkoxysilnnes. J. A. Magnuson . . . . . . . . . . . . . . . . . . . . . . s t u d y of steroids using l-’Zlcitcetic an-
1295 915
1978
1 I98 1253 93
189 184
532 1357 1243
1095 2081
159 1887
1291
1487
hydride. 0. V. Dominguez et 0 1 . . . . . ACETYLENE determination of compounds containing. Sidney Siggia a n d C. R. Stahl. . . . . . . oxy-, burner, for flame emission a n d absorption spectrometry (sci. commun.). R. N. Kniseley et ol... . . . . . . . . . . . . . . -oxygen flame for determination of tellurium. J. A. Dean and J. C. Simms. . -oxygen flames, strongly reducing, for atomic absorption s ectrometry (sci. commun.). Walter 8lavin a n d D. C . Manning . . . . . . . . . . . . . . . . . . . . . . . . . oxy- rerersed dame for analysis of calcium, in serum a n d urine. H . F. Loken et al.. . . . . . . . . . . . . . . . . . . . . . . total, in hydrocarbons, determination of trace amounts of. M. W. Scoggins a n d H. A. P r i c e . . . . . . . . . . Acetic acid. See Acids ACID Acetic diethyl-, isotope dilution analysis for determination of iron using. I n a r a Mencis a n d T. R. Swee$. . . . . . . . . . (ethylenedinitri1o)tetra-, complex with niobium, polarography o f . Robert Kirby and Henry Freiser. . . (ethy1enedinitrilo)tetra-, effect of gamma radiation on aqueous solutions of. H . E. Z i t t e l . . . . . . . . . . . . (ethylenedinitri1o)teti-a-, in urine, determination of (corresp.). R. E. Mosher et a l . . . . . . . . . . . . . . . . . . . . (ethylenedinitri1o)tetra-, or Tiron used a s masking agent in deterinination of boron in nitride, graphite rods, and titanium and zirconium borides. J. W. Tereshko . . . . . . . . (ethylenedinitri1o)tetra-. titration for determination of plutonium. W. B. Brown et a l . . . . . . . . . . . . . . . . . . . . . . ethylene(dinitri1o) tetra- used for indirect determination of thorium. D. R . Roeers and W. B. Brown. . . . . . .
1243 1740
910 699
253 875 48
1904 122 1528 403
J . S. D w y e r . . . . . . . . . . . . . . . . . . . equilibria in tertiary butyl alcohol. Leland Marple and J. S,F r i t z . . . . . spectropolarimetric titration of metal ions using asynimetric indicators. Stanlev Kirschner a n d D . C. Bbatnagar . . . . . . . . . . . . . . . . . . . . . . titration use of ion exchange membranes’ in automatic coulometric. P. P. L. KO and M. XI. M a r s h . . . . . dia!kyphosphorodithioic. complexes with zinc. T. H. Handley et 01.. . . . . . . . . . effect of strength on electro-oxidation of phenylenediamines and related compounds a t platinum electrode. H . B. l l a r k , Jr., and F. C. Anson. . . . . . . . fatty esters, argentation in countercurrent distribution t o separate isologues and geometric isomers of. C. R. Scholfirld et al.. . . . . . . . . . . . . . . . . . 2-niethylalkanoic, as internal standards in gas-liquid chromatographic assay of (sci. commun.). E. A. Kapier, J r . . . . . . . . . . . . . . . . . . . . . . performance of instrument for nimultaneous gas chromatographic and radioactivity analysis. D. C . Selson et al.. . . . . . . . . . . . . . . . . . . . . . . free, titrated in iron(II1) solutions and determination of basic iron(II1) compounds (corresp.). K u r t S t a r k e . . . . . indirect polarographic determination of. J. C. Ahhott and J. W. C‘ollat . . . . . . Krebs cycle, methyl esters of, qualitative a:a!yeis by .gas chromatography. €I.
161 1223
1069 618
1163 722
1588
1294
1575 1310 859 1916
157
1487
1000
Zucal i t al.. . . . . . . . . . . . . . . . 988 phosphorotLioic, di-n-butyl, as % n extractant for metal ions. T. H. Hand991 ley. . . . . . . . . . . . . . . . . . . . . . . . polyunsaturated, inadvertent isoinerieation durjng ester preparation (sei. commun.). H.J. Ast . . . . . 1539 potentiometric titration o f , inan Y, .+-dimethyl f a t t y amide. C et 01.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 973 preparation of methyl esters for gasliquid chromatography of. by DYrolysis of tetramethylammonium salts. E. W. R o b b and J. J. Westbrook, 111. 1F44 pyridine as reagent for detection of, on paper chromatograms (corresp.). J. Cerbulis and 11. W . Taylor. . . . . . . . . 114 ribonucleic deoxy-, Folin-Lon r y method t o determine protein contaminittion in (corresp.). G. R. Shepherd a n d 1’.
1261
17 -toluene solution, measurement of surface areas in. R. E. Mesmer and 1067 R. R . Irani tlase components of process gas streams, continuous electrolytic analyzer for, R. L. Burnett and R . F. K e a v e r . . . . . 1709 conductometric titrations in sulfuric acid system. D . E. Leyden . . . . . 307 equilibria in concentrated salt solutions, titration and measurements of p H and Ho. Donald Rosenthal and
Abbreviation used: cot., column; corr., conectlon; corresp., correspondence; rev., review; sci. commun., scientific communication; symp., syrnposlum. Numbers followed by the lotter “A” refer to pages In the advertising section; those followed by the letfer “R” refer to pages in the April review Issue.
VO1. 35, NO. 13, DECEMBER 1963
2237
A. Hopkins.. . . . . . . . . . . . . . . . . . . . . . . 1548 separated b y steam distillation and analyzed by gas chromatography. V. M. Riddle. . . . . . . . . . . . . . . . . . . . . . . . . . . 853 solutions, polarographic a n d chronopotentiometric behavior of o-phthalic acidin. R. P. B u c k . . . . . . . . . . . . . . . . 1853 titrated in nonaqueous solvents. potentiometric titration of lithi& a n d sodium perchlorate in pyridine. W. M. Banick Jr et al.. . . . . . . . . . . . . . 1413 very weak, enha&ement of acidity of, i n tertiary butyl alcohol. L. W. Marple and J. S. F r i t z . . . . . . . . . . . . . . . . . . . . . 1431 ACIDITY distributions in cracking catalysts (aid). R. J. Bertolacini. . . . . . . . . . . . . . . . . . . 599 enhancement of, of very weak acids in tertiary butyl alcohol. L. W. Marple 1431 a n d J. S. Fritz. .................... Actinide metals, microactivation analysis for oxygen in. A. C. Demildt. . . . . 1228 ACTIVATION ANALYSI~ determination of molybdenum, chromium, a n d iron content of individual stainless steel microspheres. P. A. Benson a n d C. E. Gleit. . . . . . . . . . . . . 1029 microL. &r oxygen i n actinide metals. A. U. Uemildt.. . . . . . . . . . . . . . . . . . . . 1228 applied t o determination of submicrogram quantities of manganese, sodium a n d copper in natural dirtmonds. E. C. Lightowlers. . . . . . . 1285 determination of micro amounts of calcium i n potassium chloride. F. W. E. ,3trelow a n d H. S t a r k . . . . . . . . 1154 determination of oxygen i n gallium grsenide. R. F. Bailey a n d D. A. 791 HOSS . . . . . . . . . . . . . . . . . . . determination of phosphorus in hypereutectic silicon-aluminum alloys. Robert Blackburn a n d B. F. G. Peters.. ........................ 10 determjnation of trace quantities of uranium. Dirk Decat et al.. . . . . . . 845 estimation of mercury in biological material. Hamilton Smith. . . . . . . 635 estimation of strontium-84 in biological material by. Hamilton Smith. . 749 fast, determination of total oxygen content of organic materials by. R. A. Stallwood et al.. . . . . . . . . . . . . 6 for oxygen determination in rocks, minerals. a n d water. Alexis Volborth and H.,E. Bant,a.. . . . . . . . . . . 2203 for sodium in sodium tungsten bronzes. R. J. Reuland and A. F. Voigt. ......................... 1263 lithium and lithium-6 analysis b y counting delayed neutrons. Saadia A m i d and Yehuda Welwart. 566 of aluminum; determination of yemitting impurities Kith long halflife. Francesco Girardi a n d Romano Yietra . . . . . . . . . . . . . . . . . . . . . . . . . . 173 of dilute detergent solutions (sci. commun.). C . H . W a y m a n . . . . . . 768 of oxygen, neutron flux monitoring for. J. T. Gilmore a n d D. E . Hull. , . . , . 1623 simplified method for determining sensitivities in (aid). B. T. Kenna and L. A. K e n n a . . . . . . . . . . . . 1766 using niobium-94m and tantalum182m and rapid radiochemical separations for simultaneous determination of niobium and tantalum. C. K. Kim a n d W. W. Meinke . . 2135 radio-, of sodium b y counting photoneutrons. Saadia Aniiel a n d Max Piesach 1072 safe, simple method of o eninr irradiated silica amooules (aidf. R a v Porritt and M . Thackray:. ........ .". . . . . . . . 1111 Actinium in uranium mill effluents, determined by radiochemistry. H . G. Petrow a n d R. J. Allen.. . . . . . . . . . . . . . . . . . . . . 747 Acoustical Spectrometry, instrumentation oolumn, R . H . Muller.. . . . . . . . . l l 5 A (P;io. 7) ADDITIVE0 a n d adulteration of food. lenal control in ~~~
~
......
application of 3-methyl-2-benzothiazolone hydrazone method t o atmospheric analysis of aliphatic aldehydes (corresp.). A. P. Altschuller a n d L. J. Leng.. . . . . . . . . . . . . . . . . . 1541 determination of atmospheric pollut a n t s in nart-per-hillion ran e by gas chromatography. T. A. s e l l a r et al.. . . . . . . . . . . . . . . . . . . . . . . . . 1924 1476 1934
determination of toxic organic compounds in admixture in t h e atmosphere by gas chromatography. 73 3 F. R. Cropper and Simon Kaminsky five methods for spectrophotometric determination of alkylating agents including some extremely sensitive autocatalytic methods. Eugene Sawickiet al.. . . . . . . . . . . . . . . . . . 1479 galvanic monitoring of ozone. Paul 897 Hersch a n d Rudolf Deuringer, . . . . gas chromatographic analysis of exhauat gas using temperature programmed capillary columns. D. J. McEwen.. . . . . . . . . . . . . . . . . . . . . . . 1636 hydrocarbon gas analysis using differential chemical absorption and flame ionization detectors. W. B. 1198 Innes e t al.. . . . . . . . . . . . . . . . . . . . . identification of carbonyl compounds a s their 2,4-dinitropbenylhydrazones in automobile exhaust b y paper chromato raphy. E. D. Barber a n d J. P. kodge, J r . . . . . . . . 348 modification of phenolphthalin method for determination of total oxidants (corresp.). D. F. Bender a n d A. W. Breidenbach., . . . . . . . . . 417 (rev.) A. P. Altschuller. . . . . . . . . . . . . 3R stabilized diazonium salts a s analytical reagents for determination of air-borne Dhenois a n d amines. G. 899
eta2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . r1546 peak, plate height measurements on gas columns. Richard Kieselbach. . . . . . 1342 ALCOHOLS a n d borane compounds, microanalysis of. gas chromatographic technique for de: termination of hydridic and active hydrogen in organic materials. Ihor Lysyj and R. C. Greenough.. . . . . . . . 1657 and paraffins, high molecular weight, etudy of flame response i n quantitative determination of. Gerald Perkins et a2 . . . . . . . . . . . . . . . . . . . . . . . . . . . 360
223 Fritz . . . . . . . . . . . . . . . . . . . . . . . . . . . ethyl, absolute, complexation of indium ion with 2-methyl-8-quinolinol in. W. E. Ohnesorge., . . . . . . . . . . . . . . . . . gas chromatographic determination of traces of ethanol in methanol. K. J. Bombaugh and W. E. Thomason. . . . . isopropyl-chloroform solvent mixture, spectrophotometric titration of some divalent metals in. R . K. Behm and R. J. R o b i n s o n . . . . . . . . . . . . . . . . . . . . -nitric acid, anion exchange separation of magnesium and calcium using. J. S. Fritz and Hirohiko W a k i . . . . . . . . . . . saturated, Ci-C4. gas chromatographic behavior of water and, on polyethylene glycol substrate: effect of solid support. Paul Urone a n d R. L. Pecsok.. terpene, analyzed by paper chromatograp h y a s their o-nitrophenyl- a n d p phenylazophenylurethane derivatives. J. A. Attaway et al.. . . . . . . . . . . . . . . . ALDEHYDE ..~ acet-, colorimetric analysis of. (corresp.) D. J. Clancy and D. E. Kramm . . . . . aliphatic application of 3-methyl-2benzothiazolone method t o atniospheric analysis of (corresp.). A. P. Altshuller and L . J. L e n g . . . . . . . . . . . aliphatic, color reaction of anthrone with T.-W. malonaldeh de and other. K F o n and Ll. W a t t s . . . . . . . . . . . . aromatic, a n d their acetals, spectrofluorescence of. E. P. Croivell and
305 137 452
1010 1079
837
234
~
ADSORPTION and electrode ouidation, effect on oxidation of oxalic acid a t platinum electrodes. F. C. Anson and F. A. Schultz measurement by current reversal in chrononotentiometrv isci. oommiin.). H.
1114 2210
t i n ............................... Aerodynamic forces in thermogravimetrx,. Lee Cahn and Harold Schultz.. . . . AIR a n d vaporizedliquid oxygen, gas chromatographic analysis of Ci t o C1 hydrocarbons in p.p.m. range in. C. J. Kuley ............................ borne particles, commercial instrument for continuous measurement of condensation nuclei. G. F. S k a l a . . . . . . .
POLLUTION
analysis of peroxyacyl nitrates b y gas chromatography with electron capture detection (sci. commun.). E . F. Darley et al.. . . . . . . . . . . . . . . . . .
2238
ANALYTICAL CHEMISTRY
8,
1987
1541 733 189
116 1724
1472 702
589
184
1616 phenylhydrazones b y infrared spectrometry. H. C . Lento a n d J . A. 1418 Ford . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Aldine, spectrophotometric determination of. H. 0.Friestad. . . . . . . . . . . . . . . . . 1012
Aliphatic molecules, study of integrates area of methylene rocking band of. H . F. Smith a n d A. S. Rosenberg.. . . . . . 1182 ALKALIMETALS determination of water and alkali metal oxide in alkali metal salts of selenium a n d tellurium by Karl Fischer titration P. T-I. Chiang and W. C. 1693 Rechnitz et al.. . . . . . . . . . . . . . . . . . . . 1322 ALKALINE EARTHS E D T A titration of lead(I1) in the presence of orthophos hate and (corresp.) F. H. Blood a n f W. H. Nebergall loss in micromolar concentrations, utility of 2,4 bis [ N , N ' - di - (carboxymethyl) aminomethyl] fluorescein in fluorometric estimation of metals in biologic materials. D. F. H. Wallach and 103.5 T . L . S t e c k. . . . . . . . . . . . . . . . . . . . . . . Alkalinity of sea water, determined conductometrically (corresp.) Kilho Park 1549 et al.. ................................. ALKALOIDS barbiturates, sympathomimetic amines, and tranquilizers, rapid gas chromatographic method utilizing solid injector in examination of toxicological 356 extracts. K. D. Parker et al.. . . . . . . steroids, a n d synthetic compounds separated by thin layer chromatography. B. P. Korzun et al.. . . . . . . . . . . . . . . . . 950 Alkanoic acids, %methyl-, a s internal standards in gas-liquid chromatographic assav of f a t t v acids (sei. commun.). E. 1294 A. flapier, ........................ Alkoxy groups determined in alkouysilanes b y catalyzed acetylation. J. A. 1Iagnuaon . . . . . . . . . . . . . . . . . . 1457 Alkyl and aryl halides, c 2.4-dinitrophenylhydrazones of aldehydes from reaction of their Grignard reagents with dimethylformamide. J. G. Sharefkin a n d Alex Forschirm.. . . . . 1616 Alkylating agents, five methods for spectrophotometric determination of, including autocatalytic, application t o air pollution. Eugene Sawicki et al., . . . . . . 1479 ALKYLBENZENES rearrangement technique for analysis b y mass spectrometry. E. W. Boyer et al. 1108 sulfonate concentrations in aqueous solution determined b y infrared spec9. D. trometry (sei. commun.). Kullbom a n d H. F. S m i t h . . . . . . . . . . . 912 sulfonate, neutron activation analysis of dilute detergent solutions (sci. com768 mun.). C. H . Wayman . . . . . . . . . . . Alloys, niobium base, evaluation of analytical procedures for. J. P. McKaveney. . 2139 ALUMINU.\I alkyls, colorimetric reagents and analysis 814 of. D. F. Hagen a n d W. D. Leslie.. . analyst in the automobile industry, M. L. Moss et el. (rept. for anal. chem.25A ( so. 7) ists). ....................... a n d zirconium and zirconium plus thorium in fluoride-bearing materials; vanadyl ion a s back-titrant for indirect amperometric titrations with EDTA. Gerald Goldstein et a l . . . . . . . 17 aspirin, near infrared method for determination of water in. H. H. Stein and J. I f . Ambrose.. . . . . . . . . . . . . . . . 550 determined in industrial water b y fluorometry and s ectrometry 1914 No11 and L. J. Stegnelli.. . . . . flame photometric dctermina lithium i n ; organic solven milligram amounts. W. 1736 and W. R . F o r d . . . . . . . . . . high purity, spectrophotometric determination of vanadium in. D. F. Biechler et al.. . . . . . . . . . . . . . . . . . . . 1G8A i n micromolar concentrations. utility of 2,4-bis- [N,N'-di-(c a r b o x y m e t h y 1) aminomethyl] fluorescein in fluorometric estimation of metals in biologic materials. D. F. H. Wallach and T. L. S t e c k . . . . . . . . . . . . . . . . . . . 1035 in oreano-aluminum comoounds. deter-
-
-
Jc.
1098
long half-life. Francesco Girardi and Romano P e i t r a . . . . . . . . . . . . . . . . . . 173 oxide, column chromatographic method for separation of furan derivatives on. 1.535 (sci. commun.). R . de la Rurde et al. plates for thin-layer chromatography. (aid). Fred Snyder.. . . . . . . . . . . . . . . . ,599 samples limited in quantity, "melt in rod" technique for spectrochemical 773 analysis of (aid). Nicholas Christ. . . . -silicon alloys, hypereutectic, neutron activation method for determination of phosphorus in. Robert Blackhurn a n d 10 B. F. G. P e t e r s . . . . . . . . . . . . . . . . . . . . . Amalgam eschange separation of hismuth, radiochemical. F. E. Orbe et a l.. . . . . 1436 AMERICIUM determined in curium (corresp.). C. J. 1312 Banick et al.. . . . . . . . . . . . . . . . . . . . . separated from other elements: application t o purification and radiochemical determination of. E. I.. M o o r e . , . . . . 715 Amide, N,.V-dimethyI, f a t t y , potentio-
metric titration of acids in. C. .I. Reynolds et al.. . . . . . . . . . . . . . . . . . . . . . AMINES aliphatic, lower, separation by gas chromatography. Y . L. Sze et al. . . . . . . . . aliphatic, priniary a n d secondary determined b y near-infrariid spectrophotornetrv. F. H. Lohn.an a n d W . E.
973 240
i07 899
tives of, and of amino acids and pep83 tides. Leo Kesner et al.. . . . . . . . . . . . diethyl- -ninhydrin, use'l in color t e s t aid i; identification cf amino acids (aid). Richard Circ3 a n d B. A. 262 Freeman. ......................... f a t t y , spectrophotometr c, determination in aqueous solution (corresp.). R. 1760 A.Larrick ........................ mono-, di-, a n d triethanol-, polarographic s t u d y of coppei (11) complexes 1092 of (corresp.). P. E. S t l polarographic current of I plexes of, applied t o a1 195 M a r k , Jr., and C. N. Reilley.. . . . . . . secondary, a n d tertiary spect r o p otometric determ nation of. R. 154 1LI. Silverstein. . . . . . . . . . . . . . . . . . . . primary, used for solvent extraction of plutonium; some applications t o plutonium extraction from 1671 terial. F. W. Bruenger sympathomimetic, a n d t r kaloids a n d barbiturates, rapid, gas chromatographic method utilizing solid injector in exami.iation of toxi356 cological extracts. K. 11. Parker et al. sympathomimetic, sodiur borate used in amperon 58 of. Edward Smith e t ai triethyl-, anodic oxidatir 677 Dapo a n d C. K. M a n n . . . . . . . . . . . . triethyl-, reaction at platinum anodes in acetonitrile solution; solvent background with perchlorate supporting electrolyte (sei. conirrun.). C. D. 1291 Russell. ......................... AMINOACIDS alpha-, automatic spectrophotometric reaction r a t e method f o r specific enzymatic determination of. H. V. h'lalmstadt and T. P. Hadjiionannou. 14 a n d sugars, solvents for paper a n d thin l a y e r , chromatography of, without id). H. S. El Khadem e t
primarf?
......................
derivatives, performance of instrument for simultaneous gas chromiLtographic a n d radioactivity analysis. D. C. Nelson etal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . diethylamine-ninhydrin used in color test aid in identification of (aid). Richard Circo and B. 4. F r e e m a n . . ion exchange chromatography of. single column, high resolving:, full; automatic Drocedure. P. B. Hamilton, . . , peptides- a n d amines automatic column chromLtography ok ether and water Leo soluble DNP-derivatives of. Kesner et al.. . . . . . . . . . . . . . . . . . . . . . Aniinoethanethiol hydrochloride reagent for spectrophotometric determihation for rhodium. S.C. Grirastava , , . , , , , , , . , , Aminophenol, selective oxitiation of, by cerium for spectrophotometric determination of. G. G. Guilb:iult., . . . . . . . AMINOQUIXOLINE used f o r spectrophotomet1,ic determination of iron(II1). V. E:. Gustin and T. R. Sweet. . . . . . . . . . . . . . . . . . . . . . . used in spectrophotometric determination of palladium. V. li. Gustin and T. R. Sweet. . . . . . . . . . . . . . . . . . . . . . AI\I.VOKIA a n d hydrazine determined in nuclear reactor loop samples. 9. S. Yamamura and J. H. S i k e s . , , , , . , coulometrically titrated v mite using direct ampe point detection [correiip.). G. D. Christian et al.. . . . . . . . . . . . . . . . . . . . hypochlorite-phenol reaction with substances other than. J. ' I W . earne.. . . in uranium compounds, modified Conu-ay method for deteimination of. (corresp.). C. J. G . Altmann et a l . . . liquid, f o r dissolution of lithium a n d alkali metals, for determination of oxygen in. R. J. Jaworoski st a l . . . . . . . . . microgram amounts in biological material, application of phenol-hypochlorite reaction t o ; spectrophotometric determination of nit T. M a n n , J r . . , , , , , , . , , , , salts of molybdovanadophctsph analysis of. (correep.) W. a n d R. H. M a u r e r . . . . . . . . . . . . . . . . . AhrhioxnM chloride, methyltricaprylused for liquid-liquid extraction df p t a t e ion. G. B. S. Salarin. et a compounds, substituted tricaprylmethylthiocyanate, utilized a s selective extraction agent i n spectiophotomerric determination of cobalt. A . M. Wilson and 0 . K. M c F a r l a d . . . . . . . . . . .
1766
1575 262 2055
83 1165 828 1395 44
1958
2217 327 596 1275
2179 595
salts tetramethyl-, preparation of m l t h y l esters for gas-liquid chromatography of acids b y pyrolysis of. E. W. Robb and J. J . Westbrook, 111. . 1644 sulfate determination of chlorite' critical study of different methods ' M. H. Hashmi and A. 4 . Ayaz. 2194 sulphate estimation of hypobromite, bromiie, and bromate by. &I. H. Hashmi a n d A. A . A y a z . , . . . . . . . . . . 908
A MPEROMETRY automatic cupferron titration of zirconium in highly radioactive solutions. Hisashi Kubota a n d J. G. S u r a k . . . . . automatic measurement of reaction rates: enzvmatic determination of
1715 1240
et al.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58 determination of vanadium in vanadium metal. R. A. L a n n o y e . . . . . . . . . . . . . 558 direct end-point detection applied t o coulometric titration of ammonia with hypobromide. (corresp.). G. D . Christian e t a l . . . . . . . . . . . . . . . . . . . . . 2217 improvement in titration of thiols a t rotating platinum electrode (corresp.) H. C . Borresen.. . . . . . . . . . . . . . . . . . . . 1096 titration of plutonium(V1) with iron(I1). C. A. Seils et a l . . . . . . . . . . . . . . . . . . . . . 1673 titrations with dilute solutions of permannanate. H . P. Silrerman and D. A. Skoog.. . . . . . . . . . . . . . . . . . . . . . . . . 131 titration with tetraphenylarsonium chloride. determination of hexafluorophosphaie. H. E. Affsprung a n d V. S. Archer. . . . . . . . . . . . . . . . . . . . . . . . . . . 976 vanadyl ion a s back-titrant for indirect titrations with E D T A ; general method. Gerald Goldstein e t a ! . . . . . 17 4hfPLIFIER8
Heath analog computer a s versatile analytical tool (symp.). G. W. E a i n g and T. H. Brayden, J r . . . . . . . . . . . . . 1826 multipurpose operational instrument for analytical studies (syrup.). W . L. 1778 Underkofler and Irving Shain operational, high-gain, multi-purpose electrochemical instrument for control of potential or current (symp.). George Lauer et al.. . . . . . . . . . . . . . . . . 1789 practical instrument synthesizer (symp.). C. F. Morrison.. . . . . . . . . . . . . . . . . . . . 1820 stabilized difference, a n d digital readout unit (symn.). E. C . Toren, J r . , a n d C. P. Driscoll.. . . . . . . . . . . . . . . . . . . . . . . 1809 Animals, fluorometric determination of selenium in. W. B. D y e et nl.. . . . . . . . . 1687 Anodic stripping and coulostatic analysis with a mercury electrode. Akiko Aramata a n d Paul Delahay.. . . . . . . . . . . 1117 Anthrone, new color reaction of, with malonaldehyde and other aliphatic aldehydes. T.-W. Kwon and R. bl. Watts,, 733 Antibiotics, seDaration of mixed neomvcin sulfates b y thin layer chromatography. T. F. Brodasky. . . . . . . . . . . . . . . . . . . . 343 Antihistamines, gas chromatography of. (sci. commun.). C . R . Fontan et al.. . . . 59 1 ANTIMONY a n d arsenic, rapid radiochemical procedure for. A. E. Greendale a n d D. L. Love . . . . . . . . . . . . . . . . . . . . . 632 and mercury, paper chromat of different valence states of. Mohsin Qureshi and ?I. A. K h a n . , . . . . . . . . . . 2050 telluride and bismuth telluride mixture contaicin selenium and iodine, analyCheng and B. L. Goydish. 1965 sis of. K. Aquameter Beckman parameters of (c0rresp.j. D. R. Gere and C. E . bleloa; 597 AqnEons SOLUTIONS attenuated total reflectance infrared analysis of. Bernard Katlafsky a n d R. E. Keller.. . . . . . . . . . . . . . . . . . . . . . 1665 dilute, quantitative study of gas chromatographic analysis of head space gas of (corresp.). Suheyla Ozeris and Richard Bassette.. . . . . . . . . . . . . . . . . . . . . . 1091 gas chromatography of. E. S. J a c o b s . . 2035 rapid combustion method for determining organic substances in. C. E. Van 315 Hall et nl., . . . . . . . . . . . . . . . . . . . . . . . ARGEXTATION in countercurrent distribution to separate isologues and qeometric isomers of f a t t y acid esters. C . H . Scholfield et a l . , . . . . . . . . . . . . . . . . . . . . . . . . . . 1588 system used for countercurrent distribution in fractionation of isomeric esters: hydrogenation of linoleate. C. R . Scholfield et a l . . . . . . . . . . . . . . . . . . . . . . 386 titration of orthophosphate, coulometric. G. D . Christian et a ! . . . . . . . . . . . . . . . . 1869 Arc, carbon, D.C., and gas chromatographic technique f o r simultaneous determination of oxygen and nitrogen in steels. F. M . Evens and V. A . Fassel. . . . . . . . . . . . 1444
e.
ARGON 983
302
gas chromatographic determination of minute quantities of nitrogen in (corresp.). B.-M. Karlsson. . . . . . . . . metastable atoms in the ionization of organic molecules. Rf and S. R. Lipsky.. . . . . . . . ... ARO,\rATIC hydrocarbons analyzed b y gas and liquid
1311 1562
et al.. ............................. 952 reflectance fluorescence spectra i n potassium bromide pellets. B. L. Van Duuren and C . Bardi. . . . . . . . . . . . . . 2198 Arsenic and antimony, rapid radiochemical procedure for. A. E. Greendale and D. 632 L . L o v e . ........................... Arsenide gallium, neutron activation analysis for determination of oxygen in. R. F. Bailey and D. A. Ross. . . . . . . . . . . 79 1 .4rsonium chloride, tetraphenyl-, amperometric titration using in determination of hexafluorophosphate. H. E. Affsprung and V. S. Archer. . . . . . . . . . . . . . 976 -4ryl a n d alkyl halides, characterized b y 2,4-dinitrophenylhydrazones of aldehydes from reaction of their Grignard reagents with dimethylformamide. J. G. Sharefkin a n d 41ex Forschirm. . . . . . 1616 .4SPIRIN
aluminum, near infrared method for determination of water in. H. H. Stein and J. M. Ambrose.. . . . . . . . . . . . . . . 550 and phenacetin and caffeine mixtures quantitatively analyzed b y nuclear magnetic resonance. D . P. Hollis. . . . 1682 in blood serum and plasma, phosphorimetry applied t o analysis of. J. D . Winefordner and H. W. Latz. . . . . 1517 Assay, analytical aspects of the chemical and biological, in U. S. Army C B R Agency (rept. for anal. chemists). Samuel S a s s . , . . . . . . . . . . . . . . . . . ,254 (No. 6 ) ?ITO.MIC
absorption spectrometry, physical basis of in relation t o Beer-Lambert Law. Dkiichiro Fuwa a n d B. L. Tallee. . . . . 942 weights, evaluation of (rept. for anal. chemists). Edward Wichers. . .23.4 (NO. 3) aeights, determination of by mass spectrometry (rept. for anal. chemists). -4. E. C a m e r o n . , . . . . . . . . . . . . ."A (NO. 2) Attrition, quantitative, characterization of granular solids by. D. E. Kramm and I. C. S t o n e , , . . . . . . . . . . . . . . . . . . . . . . . . . . 313 Automatic weighing, instrumentation column, R . H. Muller. . . . . . . . . . . . .,127.4 (No. 31 Automotive Industry analytical chemists in, Paul Winter kt al. (rept. for anal. 7) chemists). , . . , , , , , , , , . . , . . , . , , , 2 5 A (KO. Automobile exhaust, paper chromatographic identification of carbonyl compounds a s their 2,4-dinitrophenylhydrazones in. E. D. Barber a n d J. P. Lodge, Jr . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 348
Azo compounds, reagents for fluorometric determination of magnesium. Rodney Olsen and Harvey D i e h l . , . . . . . . . . . . . 1142 Azoniethines, C = N stretching frequency in. F. H. S u y d a m . . . . . . . . . . . . . . . . . . . 193
B BALANCE recording null-type, adaptation of a conventional, for controlled pressure, controlled atmosphere thermogravimetry. E. G. Hurd . . . . . . . . . . . . . . . . . thermogravimetric, modification of, for pyrol sis experiments in controlled a t mospgere (corresp.). D. A . S m i t h . . . BARBITURATES and alkaloids and sympathominietic and tranquilizers, rapid gas chromatographic method utilizing solid injector in examination of toxicological extracts for. K . D. Parker et a l . . . . . . . . gas chromatographic direct analysis of (corres.). E. W. Cieplinski.. . . . . . . . improved gas chromatographic column for faid). K. D. Parker et al. . . . . . . Base or'acid components of process gas streams, continuous electrolytic anal>zer for. R . L. Burnett and R . F. Klaver . . . . . . . . . . . . . . . . . . . . . . . . . . . . Beer's Law, dependence on; physical basis of analytical atomic absorption spectrometry. Keiichiro Fuwa a n d B. L. Vallee BEXZENE alkyl- and its sulfonic acid, determinatiod of minor components in, b y differential infrared spectrometry. J. M. Blakeway and N. A. P u t t n a m . . .... alkyl-, rearrangement technique f o r analysis b y mass spectromety. E. W. Boyer et al.. . . . . . . . . . . . . . . . . . . . . . . and related solvents, coulometrically generated iodine used t o determine waterbelow 10 p.p.m. in. R.F. Swensen a n d D. A. Keyworth. . . . . . . . . . . . . diethyl-, separated-by gas chromatography using packed columns (corresp.). C. -4. Blake, J r . . . . . . . . . . . . . . . . . . . . .
VOL. 35, NO. 13, DECEMBER 1963
0
1468 1300
356 250 418 1709 912
630 1168 863 1759
2239
disulfonic acid 4 5-dihydroxy- disodium salt of, or 'EDTA used a; maskiqg agent in determination of boron in nitrides, graphite rods, a n d titanium a n d zirconium borides. J. W. columns (corresp.). S. F. Spencer. .. halonitro- anion radicals, voltammetry a n d E P R spectra of (sci. commun.). Toyokichi Kitagawa et 01.. . . . . . . . . . . iodine-substituted, characterization b y formation of polyvalent derivatives. J. G. Sharefkin a n d Harold Saltsman. trinitro-, substituted, paper chromatography of. D.-M. Colmap.. . . . . . . . . . Bsnzoguanamine. S e e s-Triazine, 2,4-diamine-6-phenyl-. Benzoic acids, hydroxy-, and brominated aalicylanilides ion exchange separation of. N. E. Skeily and W. B. C r u m m e t t . . Benzothiazoline hydrazone method, 3methyl-2-, aqplied to atmospheric analysis of aliphatic aldeh des (corresp.). A . P. Altschuller and J. Leng. Benzyl chloroformate, determined b y gas chromatography of its amide. Charles Hishta and Joseph Bomstein ... BERYLLIUM
E.
............
157 592 1086
652
1680
1541 65 1620
311 spectrophotometric titration of. T. M. Florence and Y . J. Farrar. . . . . . . . . . . 712 spot test for based on color reaction EriochroAe Cyanine R. (corresp.) 1103 R. Mohilner.. . . . . . . . . . . . . . . . . . Binary mixtures, rapid determination b y pseudo-first-order differential reaction rates: conductometric determination of carbonyl compounds. L. J. P a p a et 61.. . 1889 Biochemical and chemical assay in the U. 9. Army CBR Agency (rept. for anal. chemists). Samuel Sass. . . . . . . . ..25A (.No.6) BIOLOQICAL ~IATERIALS determination of urinary ketosteroids b y gas chromatography. Mario Spara1231 gana et al.. ....................... enzymatic determination of glucose in serum, plasma, and blood, automatic amperometric measurement of reaction rates. H. L. P a r d u e . . . . . . . . . . . . . . . 1240 estimation of ammonium in, by hypoJ. T. chlorite-phenol reaction. 327 Wearne . . . . . . . . . . . . . . . . . . . . . . . . . . . estimation of strontium-84 in, b y neut_rop.activation analysis. Hamilton 749 Ymith ............................ fluids and tissues, determination of true chloride content in by I. Isotope dilutioh method. Ernest 95 Cotlove, ........................ 11. Non-isotopic method. Ernest 101 Cotlove.. ....................... fluorometric determination of calcium in blood serum. B. L. Kepner and D. 1238 M. Hercules.. .....................
D. Parker at al.. .................... human a n d bovine gamma globulins, immunofiuorescein titration of. (sci. commun.). R.,P. T a n g e r d y , . . . . . . . . in aqueous solution, liquid scintillation counting of. (corresp.). Hajime Takahashi et al.. ........................ manganese in human serum, determination of submicrogram quantities of. A. A. Fernandez e t al.. . . . . . . . . . . . . . . neutron activation analysis for estimation of mercury in. Hamilton Smith. phenol-hypochlorite reaction to microam amounts of ammonia in total igest of. spectrophotometric determination'of nitrogen. L. T. Mann, Jr. radioisotopic assay for neomycins B, C, and neamine. D. G. Kaiser., . . , . . , , separation of mixed neomycin sulfates b y thin layer chromatography. T. F. Brodasky . . . . . . . . . . . . . . . . . . . . . . . . . separation of vitamin D2, ergosterol, a n d tachysterolr, by chromatography. A. W. Norman and H. F. D e L u c a . . . . . serum a n d urine analyzed by reversed oxyacetylene flame spectrophotometry for calcium. H. F. Loken, et al.. . . some applications to plutonium extraction from; solvent extraction of plutonium with primary amines. F. W. Bruenger et al.. .................... with large quantities of c?lcium, deter-, mination of total radiostrontlum In. A. L. B o N . ....................... Biphenyl radical anions, coulometric titration of reducible organic compounds using. D. L. Maricle.. ...............
F
2240
ANALYTICAL CHEMISTRY
BISMUTH
1599
radiochemically separated b y amalgam exchange. F. E. Orbe et al.. . . . . . . . . 1436 telluride and antimony telluride mixture containing selenium and iodine, analysis of. IlICM a n d zinc 8-quinoliiiates precipitated from homogeneous solution. F. H. Firsching and J . G . Brewer.. . . . . . . . . . . 1630 iodide-linear stilrcli reanent for colorimetric iodimetry, sinlplified preparation of (c0rresti.I. J. L. Lambert 405 1682 tris-7-(l-azo-8-hydroxy 3,6-di-).
naphthalene-
C:ALCIUM
[ A O . 13)
USSR Research Reports: A Report Bibliography. E., H. Hall, Armed Services Technical Information Agency. . . . . . . . . . . . . . . .,. .. .53A (No. 8 ) Vacuum Microbalance Techniques. Vol. 3. K. H. Behrndt, e d . . . . . . . .98A (No. 10) Borane compounds a n d alcohols, microanalysis of. gas chromatographic technique for dktermination of hydridic a n d active hydrogen in organic materials. Ihor Lysyj and R. C. Greenough:. . . . . 1657 Borate sodium tetraphenyl-, used in amgeroketric titration of amines. Edward mith et at.. ........................ 58 Boron in organoboron compound?, flamephotometric microdetermination of. Tamotsu Yoshizaki.. . . . . . . . . . . . . . . 2177 Borax disk, x-ray spectroscopy method for trace analysis of metals. (corresp.). C. 1881 L. Luke . . . . . . . . . . . . . . . . . . . . . . . . . . . . Borax glass, matrix method for x-ray fluorescence analysis of polyphase metals (corres.). Suren Sarian a n d H. W.Weart. . . . . . . . . . . . . . . . . . . . . . . . . . . 115 BORON elemental, carbon determination in. C.-W. Kuo et al.. . . . . . . . . . . . . . . . . . 1505 extraction and flame spectrophotometricdeterminationof. W. J. Illaeck
....................
. notentiometric deter. . lite
~~~
n-
0
1079 2069
1154
2131
1489
of gas Chromatography apparatus from ion chamber measurements. D. C. Nelson and D. L. P a u l i . . . . . . . . . . . . . 1571 of nuclear magnetic resonance chemical shift scale fcorresp.). J. L. Jung1985 751
mucopolysaccharides, effect of temperature and time of heating on (corresp.). B. Radliakrishnamurthy and G. S. Berenson., . . . . . . . . . . . . . . . . 1316 CARBOHYDRhTES degradation products of, column chromatographic method for separation of (sci. commun.). R . de l a Burde 1535 et al. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . fluorimetric microdetermination of. J. C. Towne and J. E. Spikner.. . . . . . . . 211 C.4RBOX -14-acetic anhydride used in studies of acetvlation of steroids. 0. V. Doniin1243
830
2015 C.G.Pope ........................ compounds, mono-, direct quantitative isolation from fats and oils. D . P. Schwartz et al.. . . decimilligram determination of. Keiichiro Hozumi and 1%'. J. Kirsten. determination in elemental boron. C.-W. Kuo, et al.. . . . . . . . . . . . . . . . . . . determination of ferrous metals b y gas chromatography. Chen-Win K u o and Joe M. Walker.. . . . . . . . . . . . . . . . . . . . determined in thin metal films b y means of flash discharge lamp (sci. commun.). W. G. G u l d n e r . , . . . . . . . . . . . . . . . . . . dioxide, high frequency oscillimeter used in determination of (aid$. E. H. Bruins. .....................
-
CARBOGLIC ACID
336 660
1348 2209
1315 315
1353 783
48
348 422
and hydrocarhcn in basic solutions, spectrophotometric determination of; methods for obtaining material balance d a t a in carbanion oxidation re680 actions. Harvey Pobiner et al.. . . . . chlorides, gas chromatographic separation of their amides for determination of. Charles Hishta and Joseph Bom65 stein. . . . . . . . . . . . . . . . . . . . . . . . . . . . . hydrazides. coulometric determination of. A. F. Krivis et al.. . . . . . . . . . . . . 1955 in biological materials, by esterification and gas chromatography. C. W. 76 Gehrke and D. F. Goerlitz.. . . . . . . . . long-chain quantitative microdeterminatioh method snecific for. 0. S. 370
875
CALIBRATION
m d ~ and . titanium
ANALYTICAL CHEMISTRY
744
OZ
137 reshko. ...... in organoboranes, simple method for microdetermination of, either alone or simultaneously with nitrogen and/or phosphorus. R. C. Rittner and Robe r t C u l m o . . ...................... 1268 sensitivities and other properties of reagents for colorimetric determination of (corresp.). G. W. Goward and V. R. Wiederkehr . . . . . . . . . . . . . . . . . 1542 trifluoride for esterification of long-chain carboxylic acids. 0. S. Duron a n d Alois N o w o t n y . . . . . . . . . . . . . . . . . . . . 370 Bromate, hypobromite a n d bromite, eatimated b y ammonium sulphate, iodometric method. M. H. Hashmi a n d A. 908 A. Ayraz.. ..........................
2242
alcohol-nitric acid used for anion cxchange separation of magnesium and. J. S. Fritz and Hirohiko W a k i . . . . . . . and strontium, separated b y liquid ion exchange; determination of total radiostrontium in milk. F. E. Butler determination of total radiostrontium in biological samples containing large quantities of. A. L. B o n i . . . . . . . . . flame photometry of. use of reversed oxyacetylene flame in Beckman direct sprayer burner. H. F. Loken, et al.. . in potassium chloride, neutron activation analysis for determination of micro amounts of. F. W. E. Strelow and H. Stark ......................... sensitive, selective spectrophotometric reaction for determination of trace amounts of. 11. Herrero-Lamina and T. 5. W e s t . . . . . . . . . . . . . . . . . . . . surface hydrates, internally standardized mineral oil mulls used for infrared spectrometric analysis of. R. J. Morris, Jr. . . . . . . . . . . . . . . . . . . . . . . .
-hydrogen ratios, neutron scattering for determination of. H. L. Finston a n d Emanuel Yellin.. . . . . . . . . . . . . . . . . . i n hydrogen peroxide, combustion-gas chromatography for determination of. F. M. Pielsen and Sigurd Groennings Carbon labeled compounds, application of continuous elemental analysis of gas chromatographic effluents to. Fulrio Cacace et al.. . . . . . . . . . . . . . . . modification of electron probe t o detect (sei. commun.). J. Rlerritt et al.. . . . monoxide deterniined in Orsat gas analysis apparatus Tvitli cuprous sulfate,&naphthol (corresp.). Ross Stewart and D. G. E v a n s . , . . . . . . . . . . . . . . . . rapid combustion method for deterniining organic Rubstances in aqueous solutions. C. E. T a n Hall et al.. . . . skeleton and other structural features of organic compounds. gas chroinatographic determination of. Morton Beroza a n d Rafael Sarmiento. . . . . . . -14 tritium a n d sulphur-35 labeled compou,nds, oxygen flask method for assaying. H . E. D o b b s . . . . . . . . . . . . . ClRBOSYLS by hydration of acetylenes i n hydrocarbons, ultraviolet determination of. 11. W. Scoggins and H. A. Price.. . . . identified a s their 2,4-dinitrophenylhydrazones in automobile exhaust b y paper chromatography. E. D. Barber and J. P. Lodge. J r . . . . trace, automated determination of (aid). 8. A. Bartkieuicz and L. C. Xenvon . . . . . . . . . . . . . . . . . . . . . . . . . .
654
2191 1522 1505 2017 1744 934
141 Tanaka.. ......................... Carotenes. separat-on of, activated cellulose for solution-adsorption chroma93 tography. C. K. Miller et al.. . . . . . . Catalysts, cracking, acidity distributions i n (aid)., R. J. Bertolacini.. . . . . . . . . . . . 5Q9 Catalytic methods and spectrophotometric for determining alkylating agents, a plied to air pollution. Eugene Sawicky 1479 et al.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . CELL electrolysis, and gas circulating pump; electrochemistry of gases (aid). 120 P . E . T o r e n ..................... electrolysis, for continuous external generation of reagents in reagentaddition analyzers. R. B. Kesler. . . . 963 electrolysis, for high speed controlled potential coulometry. A,. J. Bard.. ... 1125 infrared, gas, heated, simple, inexDensive (aid). . . E. A. B u r n s . . . . . . . . 1106 CELLULOBE activated, for solution-adsorption chro93 matography. C. K. Miller et al.. . . . adaptation of oxygen flask method for ashing of [aid). J. C. Paulson.. . . . 1558 Centrifugal, accelerated horizontal paper chromatography for separation of dyes 238 and indicators. J. F. Herndon et al.. . Ceramics, analyst in the automotive industry, Willard Hauth e t al. (rept. for anal. chemists). . . . . . . . . . . . . . . . ..25A ( No. 7) CERIUM radiochemically determined by solvent extraction method. M . A. A n w a l . . 2048 I 'L selective oxidation of p-aniinophenol for spectrophotometric determination. G. G. Guilbault.. . . . . . . . . . . . . . . . . . 828 thenoyltrifluoroacetone used in specof. trophotometric determination Hiroshi Onishi and C. V. B a n k s . . . . . 1887 use of cerous ion in rapid titration of orthophosphate. T. A. Taulli a n d 1060 R. R. I r a n i . . ...................... Cerous ion, fluorometric procedure for determination of (sci. commun.). W. A. Armstrong et 51.. . . . . . . . . . . . . . . . . . 1300 CESIUM and rubidium in oil field waters, flame spectrophotometric determination of. 1258 A. G. Collins. ..................... 137 and 134, half lives of. L. A. Dietz 797 etal.. . . . . . . . . . . . . . . . . . . . . . . . . . . . radio-, chlorostannate method for separation of. C. F. Goeking et al.. . . . . . 1434 2-theno ltrifluoroacetone used in liquidliquid' extraction of. Peter Crowther and F. L. Moore.. . . . . . . . . . . . . 2081 Channel ratio method. of measuring liquid scintillation counting efficiencies. E. 1024 T.Bush ............................
CHEL.4TES metal, detection of in gas chromatography b y electron capture. W. L).-Ross. . . . . . . . . . . . . . . metal, i n analytical cherr i the 16th annual sym Fernando et al.. . . . metal of p y r i d i n e 4 6 trophotometric and potentiometric study of. S. P. Bag e ! 01.. . . . . . . . . . Chelating agent, quinoline - 8 - selenol (corresp.). Liichi Sekido et al.. . . . . . . . CIiemiluniinescence, 1imiti.d area flanie spectrometry. B. E. Brell. . . . . . . . . . . Chloramphenicol, gns chromatography of trimethylsilyi derivativeti of related to. P. D. S h a w . . . . CHOLESTEROL reliable method Goodman et a1 ............ total a n d esterified, simplified method t o determine (corresp.). T. C. Huang et al.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . total, in blood serum, perchloric acidphosphoric acid-ferric chloride reagent used for rapid dctermination of (corresp.). Tsutomu hlomose et al. Chlorate, determination of chlorite; critical study of different methods. M . H. Haslinii a n d A. A. A y a z . . CHLORIDE s t ,silver electrodes, coulometric efficiencv of anodic ceposition a n d H. -4. Laitinen LF. L i n . . . . . . . . . . . . . . . . . . . . . sues. ,ion method. Ernest Cotlove.. . . . . . . . . . . . . . . . . 11. Non-isotopic mathod. Ernest Cotlove, . . . . . . . . . . . . . . . . . . . . . interference, eliminated in chemical oxygen demand test. R. A. Dobbs and R. T. Williams.. . . . . . . . . . . ion exchange and nonaqueous t i t for determination of potassium perE. &-. chlorate in presence of. Albaugh et al.. . . . . . . . . . . . . . . . . . . . metallic, solid, unstable, method for introduction on t o gas chromatog columns (aid). C. P. &llis.. . trace quantities of broinide sepa by distillation meth
