AUTOCLAVE ENGINEERS INCORPORATED - ACS Publications

May 3, 2012 - AUTOCLAVE ENGINEERS INCORPORATED. Anal. Chem. , 1948, 20 (7), pp 15A– ... View: PDF | PDF w/ Links. Article Options. PDF (263 KB)...
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15A VOLUME

20,

NO.

7,

JULY

1948

NOW I

HIGH PRESSURE

IS WITHIN REACH OF tfM LABORATORY A BRAND NEW RESEARCH TOOL Virtually a c o m p l e t e laboratory in itself, this new, one liter autoclave was designed by Autoclave Engineers, Inc. to make High Pressure Research available to every laboratory. COMPLETELY SELF C O N T A I N E D A l t h o u g h this unit is extremely low in price it incorporates all of the major improvements, pioneered by Autoclave Engineers, I n c . and generally found only in their m u c h higher priced, custom built equipment. This one liter autoclave is self-contained and consists primarily of a one-liter stirred reactor designed for working pressures up to 5,000 p.s.i., working temperatures to 6 5 0 F with agitator speeds variable from 3 0 0 to 1000 R.P.M. Since this unit offers positive agitation at known rates of speed it enables the chemist to carry out reactions involving suspended catalyst in quantities as small as 1 5 0 cc. POSITIVE PATENTED SEAL T h e cover on this unit incorporates t h e improved, leak-proof, quick-seal feature developed by Autoclave Engineers, I n c . T h e agitator shaft is sealed and protected by a special packing assembly which allows operation w.th either light or heavy gases, at high pressures, and high temperatures without leaking and without galling the shaft—a feature of real importance t o the chemist whose range of working gases may vary from heavy ammonia t o light hydrogen. T h e autoclave stirring shaft is equipped with an internal water cooling system. Specially designed fittings enable t h e chemist to make gas tight joints without the use of large tools, in a minimum of time, ONLY without fear of burring t h e closure or set screws. $ 9 75.00 Complete autoclave with stirrer, heating jacket, floor stand, COMPLETE oil system, pressure gauge, blow out assembly and motor, UNIT ready t o operate.

ANNOUNCINGHERE ARE THE They sfiow the careful engineering which results in exceptionally efficient operation, a feature of all autoclaves developed by a u t o c l a v e Engineers, Inc. Capacity—one liter Diameter—3" inside diameter Inside Depth—9" . Working Pressures—0 to 5,000 p.s.i. 8,000 p.s.i. test pressure Working Temperature—650°F. Body and Cover—Type 316 Stainless Steel Forging. Internal Parts—Type 304 Stainless Steel Essential Parts—Type 410 Stainless Steel

SPECIFICATIONS Closure—Set screws type closure with hardened thrust ring and confined gasket Agitator and Drive—Paddle type agitator—300 to 1000 R.P.M., 1/4 H. P. motor Heating—Electric heating or Steam jacket for 250 lb. p.s.i. working pressure Stuffing Box—Bottom packing, latern ring and top packing. Packing is aluminum foil Accessories — O i l cylinder complete with fittings and valves, necessary support and pressure gauge, rupture disc and thermo-couple well Support—Welded steel stand—Motor mounting attached

NEW CONING AND THREADING TOOL Accepted by leading industrial high pressure laboratories. Sure, fast and accurate .. saves many hours of tedious hand work over a period of time. Write for detailed bulletin CT-1.

STAINLESS STEEL VALVES &FITTINGS A complete line carried in stock for immediate shipment. Features exclusive self-sealing packing ring.

AUTOCLAVE ENGINEERS 3737

WEST

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