Boron trifluoride-mediated reaction of 1,9-dihalopentacyclo[5.4.0.02

Boron trifluoride-mediated reaction of 1,9-dihalopentacyclo[5.4.0.02,6.03,10.05,9]undecane-8,11-diones with ethyl diazoacetate: a novel synthetic entr...
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J. Org. Chem. 1988,53, 5969-5971

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3. SbPh, 1,1,2,2-TetrachloroethaneSystem. The reaction of SbPh, (0.05 M) and 1,1,2,2-tetrachloroethane in the presence of aluminum chloride resulted in an EPR spectrum (Figure S6a12) identical with that of the dibenzo[a,c]triphenylene radical cation in SbC15-CH2C12 solution.16 Proton hyperfine coupling constants of 0.60, 2.00, 2.27, and