BRUKER SCIENTIFIC, INC. - Analytical Chemistry (ACS Publications)

BRUKER SCIENTIFIC, INC. Anal. Chem. , 1969, 41 (2), pp 57A–57A. DOI: 10.1021/ac60271a737. Publication Date: February 1969. ACS Legacy Archive...
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be

conventional!

BRUKER’s newly developed HX-60 (60 MHz) NMR system opens many channels of research which have not been possible or practical with

conventional old-concept commercial spectrometers. Over the past decade while Proton High Resolution NMR has become the most widely accepted technique for organic structural determinations, researchers have strived to expand this highly sophisticated technique into other areas of research such as the Biomedical and Biochemical fields. With conventional instrumentation, this expansion became not only costly but also very impractical due to the time absorbed in performing instrument modito fications and exchanges. In practice, Multi-nuclei research had become many people theoretical instead of practical. BRUKER, seeing the frustrations of the researcher, combined many years of electronic and scientific know-how with a logical outlook and has come up with “THE SYSTEM” for Multi-nuclei research. Now BRUKER is proud to introduce the HX-60. —



Ci3 TIME AVERAGED 14.93 MHz Ci3 (Nat. Abun.) Spectrum. Carbon 13 NMR Spectrum Accumulation; 13 passages at normal sweep speed. 13 mm. at 20°C. Trimethylphosphate —

Completely solid state modular design. Push button operation. Proton stabilization for all nuclei by means of frequency synthesized techniques. for examination of up to eight nuclei without probe change. UNIVERSAL PROBE 5, 10, 13 and 15 mm spinning sample tube inserts. Variable temperature utilizing digital readout controller for temperatures from —150°C to +200°C. 3-4 kHz (high resolution). Dual frequency modulation Wide-Line 40 Hz modulation. Calibrated wide sweeps utilizing internal proton stabilization: 1H— 250 ppm proton stabilized 500 ppm proton stabilized 31P 1000 ppm proton stabilized 13c Homo- and Hetero-nuclear spin decoupling (selective and modulative). Independently swept f, and f2 channels allowing INDOR experiments to be performed. Pulsed Gates increased leakage suppression for critical applications.

Time Constant................................0.05 sec. Sweep Width ................................15 Hz/cm. Sweep Duration........................13 x 50 sec.













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Circle No. 25 on Readers' Service Card

HI/R3I HETERO-DECOUPLED 24.2 MHz P31 Spectrum. Triphenylphosphite 5 mm. at 19°C. in Acetone. Time Constant........................0.1 & 0.3 sec. Sweep Width ................................6.0 Hz/cm. Sweep Duration...............................100 sec.