Contributed Articles - ACS Publications - American Chemical Society

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Contributed Articles Submicromolar Concentration Measurements with Tubular Electrodes. W. J. Blaedel and S. L. Boyer

Study of the Uncatalyzed Oxidation of Arsenic(lli) by Cerium(IV) in Perchloric Acid Medium. K. G. Everett and D. A. Skoog

Analysis of Vapor-Phase Pyrolysis Products of the Four Trimethylpentane Isomers. J. Q. Walker and J. B. Maynard

Application of the Carbon Rod Atomizer to Atomic Absorption Spectrometry of Petroleum Products. K. G. Brodie and J. P. Matousek

Extractive Titration Technique for Kinetic Studies of Fast Bromination Reactions. R. K. Baker and Quintus Fernando

Spectorphotometric Determination of Xanthate and Total Sulfur in Viscose. Matiur Rahman

1614

Isolation and Analysis of Carbonyl Compounds as Oximes. J. W. Vogh

1618

1548

Computer-Assisted Ion Cyclotron Resonance Appearance Potential Measurements for C5HM Isomers. M. L. Gross and C. L. Wilkins

1624

1557

Analysis of 2-Substituted-2-Methyl-5-Norbornenes by Nuclear Magnetic Resonance Spectrometry. R. V. Moen and H. S. Makowski

1629

Gas-Solid Chromatography of Hydrogen Bonding Compounds. Antonio Di Corc/a and Fabrizio Bruner

1634

Electrooxidation of Iodine on Smooth Platinum in Acetic Acid Medium. Influence of Adsorption of Electrode Products upon Voltammetric Limiting Currents. Rolando Guidelli and Giovanni Piccardi

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Characterization and Quantitative Analysis of D-Glucose for Use in Clinical Analysis. Bruce Coxon and Robert Schaffer

1565

Voltammetric Behavior and Analytical Detection of Oxygen, Superoxide, Hydroxide, and Water Present Together in an Ionic Solvent. P. G. Zambon/n

1571

Analytical Evaluation of a Cyanide-Ion-Selective Membrane Electrode under Flow-Stream Conditions. Bernard Fleet and Henning von Storp

1575

Extraction-Derivatization-Gas Chromatographic Determination of Trace Phosphate in Aqueous Media. D. R. Matthews, VY. D. Shu/ts, M. R. Guerin, and J. A. Dean

1582

© Cepyrigit 1171 •y the American Ciemical Satiety

MANUSCRIPT REQUIREMENTS published in December 1970 issue, page 1879, outlines scope and copy requirements to be observed in preparing manuscripts for consideration. Manuscript (4 copies) should be submitted to ANALYTICAL CHEMISTRY, 1155 Sixteenth St., N.W., Washington, D. C. 20036. The American Chemical Society assumes no responsibility for the statements and opinions advanced by contributors to its publications. Views expressed in the editorials are those of the editors and do not necessarily represent the official position of the American Chemical Society. 1971 Subscription Rates

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Separation of Weak Organic Bases Such as Aniline, N-Heterocyclic, and Sulfonamide Derivatives on Cation Exchange Resin. T. C. Gilmer and D. J. Pietrzyk

1585

Specification of Gas Chromatographic Behavior Using Kovats Indices and Rohrschneider Constants. L. J. Lorenz and L. B. Rogers

1593

Applications of Paramagnetic Shift Reagents in Proton Magnetic Resonance Spectrometry. Analysis of Alcohol Mixtures. D. L. Rabenstein

1599

Small Computer, Magnetic Tape Oriented, Rapid Search System Applied to Mass Spectrometry. L. E. Wangen, W. S. Woodward, and T. L. /senhour

1605

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ANALYTICAL CHEMISTRY, VOL. 43, NO. 12, OCTOBER 1971 ·

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Contributed Articles Electrooxidation of Iodine on Smooth Platinum in Acetic Anhydride Medium. Giovanni Piccardi and Ro­ lando Guide///' Determination of Volatile Constituents of Human Blood and Tissue Specimens by Quantitative High Resolution Mass Spectrometry. Walter Snedden and R. B. Parker Interactions between Rock and Organic Matter. Esterjfication and Transesterification Induced in Sedi­ ments by Methanol and Ethanol. Patrick Arpino and Guy Ourisson Alternating Current Polarographic Determination of Electroactive Species More Negatively Reduced than the Major Component. A. M. Bond and J. H. Canterford Polarographic Evaluation of Formation Constants for a Partly-Reversible System and a New Systematic Pro­ cedure for All- as Well as Partly-Reversible Systems. Kozo Momoki and H/sao Ogawa Extension of the Microcoulometric Determination of Total Bound Nitrogen in Hydrocarbons and Water. F. A. Fabbro, L. A. Filachek, R. L. lannacone, R. T. Moore, R. J. Joyce, Y. Takahashi, and M. E. Riddle

1646

1651

Rapid Analysis of High Purity η-Heptane and Other Pure η-Paraffins for Trace Hydrocarbon Impurities by Gas Chromatography. R. N. Nigam and Rijhwani Moolchandra

1701

Computer Program to Draw Absorption Profiles in Atomic Absorption Spectrometry. C. L. Chakrabarti, Rajendra Pal, and Mohan Katyal

1704

Simplified Wet Ash Procedure for Total Phosphorus Analysis of Organophosphonates in Biological Sam­ ples. D. S. Kirkpatrick and S. H. Bishop

1707

Analysis of Insect Chemosterilants. Action of Phos­ phate Buffers on Aziridine. J. G. Pomonis, R. F. Severson, P. A. Hermes, R. G. Zaylskie, and A. C. Terranova

1709

Tape-Controlled Gradient Elution Chromatography System for Steroid Analysis. D. F. Johnson, N. S. Lamontagne, G. C. Riggle, and F. 0. Anderson

1712

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Correspondence 1671

Notes Influence of the Setchenow Salt Effect upon Analytical Results Involving Concentration by Solvent Extraction Techniques. Theo Groenewald

3',5'-Cyclic Adenosine Monophosphate Phosphodi­ esterase Assay Using High Speed Liquid Chromatog­ raphy. S. N. Pennington

1678

Some Considerations on Stepwise Electroreduction in Voltammetry and Chronopotentiometry. Rolando Guidelli

1715

A Digital Potentiostat. Clem

1718

W. W. Goldsworthy and R. G.

Alternate or Simultaneous Electron Impact-Chemical Ionization Mass Spectrometry of Gas Chromato­ graphic Effluent. G. P. Arsenault, J. J. Dolhun, and K. Biemann

1720

1683

Aids for Analytical Chemists Photometric Method for Microdetermination of Hydroxylipids. M. M. Chakrabarty and M. K. Kundu Determination of Gold in Solutions of Thiourea. Groenewald and B. M. Jones

1686

1723

Direct Sample Injection into a Helium Ionization Gas Chromatograph. H. C. Dodd

1724

Pseudo-Three-Dimensional Presentation of Reaction Rate Data. S. N. Deming

1726

Correction. Example of Flame Photometric Analysis for Methyl Parathion in Rat Whole Blood and Brain Tissue. Joe Gabica, Joe Wyllie, Michael Watson, and W. W. Benson

1633

Correction. Combined High Speed Liquid Chromatog­ raphy and Bioassay for the Evaluation and Analysis of an Organophosphorus Larvacide. R. A. Henry et al.

1633

Theo 1689

Direct Analysis of Metal Halides by Electron Impact Mass Spectrometry. Kozo Matsumoto, Nobutoshi Kiba, and Tsugio Takeuchi

1691

Laser-Excited Atomic Fluorescence Flame Spectrom­ etry. L. M. Fraser and J. D. Winefordner

1693

Trimethylsilyl Esters of Aromatic and Aliphatic Sul­ fonic Acids. Preparation and Mass Spectral Proper­ ties. John Eagles and M. E. Knowles Digitization and Processing of Nuclear Magnetic Reso­ nance Spectra. R. E. Rondeau and V. L. Donlan 6A ·

Solenoid Operated Switching Valve for Automatic Ti­ tra tors. J. A. Blay and L. J. Betz

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ANALYTICAL CHEMISTRY, VOL. 43, NO. 12, OCTOBER 1971