Contributed Articles - Analytical Chemistry (ACS Publications)

Chem. , 1971, 43 (1), pp 3A–4A. DOI: 10.1021/ac60296a703. Publication Date: January 1971. ACS Legacy Archive. Cite this:Anal. Chem. 1971, 43, 1, 3A-...
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Contributed Articles

General Analysis of Potentiostatic Current-Time Curves for Cylindrical Electrodes. Sidney Barnartt and C. A. Johnson Simultaneous Determination of Silicate and Phosphate by an Automated Differential Kinetic Procedure. J. D. Ingle, Jr., and S. R. Crouch Radioisotopic X-Ray Analysis of Silver Ores Using Compton Scatter for Matrix Compensation. P. G. Burkhalter Application of Field Ionization to Gas-Liquid Chromatography-Mass Spectrometry (GLC-MS) Studies. J. N. Damico and R. P. Barron Machine Intelligence Applied to Chemical Systems. Prediction and Reliability Improvement in Classification of Low Resolution Mass Spectrometry Data. P. C. Jurs Double Beam Photon Counting Photometer with Dead Time Compensation. K. C. Ash and Ε. Η. Piepmeier Chlorine-35 Nuclear Quadrupole Resonance Studies of Trichloromethyl Compounds. E. G. Brame, Jr.

Time-Lapse Spectrometry in Organic Photochemistry. N/co/ae Filipescu, F. L. Minn, and J. W. Pavlik

83

The Question of Instrumental Artifact in Linear Sweep Voltammetry with Positive Feedback Ohmic Drop Com­ pensation. E. E. Wells, Jr.

87

Photon Activation Analysis—A Review.

93

2

7

10

17

22

26

G. J. Lutz

Use of Static Argon Atmosphere in Emission Spectrochemical Determination of Chromium in Biological Materials. Κ. M. Hambidge

103

Mixed Carrier Gases in Chromatography—A Source of Error. Raymond Annino, Joseph Franko, and Harry Keller

107

Micro and Ultramicro Analyses by Null Point Pressuremetry and Coulometry: Hydrogénation and Hydrogenolysis. D. J. Curran and J. E. Curley

118

Analysis for Impurities by Nuclear Scattering. Cohen and R. A. Moyer

123

B. L.

35

Notes Cryoscopic Determination of Number-Average Molecu­ lar Weight by Quartz Crystal Thermometry. J. S. Fok, J. W. Robson, and F. C. Youngken Accuracy of Analysis by Electrical Detection in Spark Source Mass Spectrometry. R. A. Bingham and R. M. Elliott Radioactive Tracer Technique for Molecular Diffusion Coefficients in Granular Media. E. R. Bennett and W. E. Bolch Spectrophotometric Analysis of Carbonyl Compounds in the Presence of Carbohydrates without Prior Separa­ tion. Ε. Β. Sanders and Jack Schubert Polarographic Determination of Traces of Nitrilotriacetate in Water Samples. J. P. Haberman Selectivity in Liquid-Liquid Chromatography. Marine and D. C. Locke

38

Potentiometric Study of Copper(l) Complexes with Uni­ valent Anions in Acetonitrile. J. K. Senne and Byron Kratochvil

129

Solvent Effects in Gel Permeation Chromatography. G. Bergmann, L. J. Duffy, and R. B. Stevenson

131

J.

43 Interference of Lithium in Atomic Absorption Spectrometry. A. M. Bond and D. R. Canterford

134

Spectrofluorometric Determination of Traces of Fluoride Ion by Ternary Complex Formation with Zirconium and Calcein Blue. T. L. Har and T. S. West

136

Fluorometric Methods for Determination of Europium and Terbium. D. E. Williams and J. C. Guyon

139

Spectrophotometric Determination of Sulfide Ion with Organic Disulfides. R. E. Humphrey, Willie Hinze, and W. M. Jenkines III

140

74

Determination of Nitrite by Controlled-Potential Coulometry. J. E. Harrar

143

79

Spectrophotometric Determination of Rhodium with Nitroso R. Formula for the Rh(lll)-Nitroso R Complex. O. W. Rollins and M. M. Oldham

146

55

59

63

D. £.

Pyrolysis Gas Chromatography of Phenyl Polymers and Phenyl Ether. M. T. Jackson, Jr., and J. Q. Walker

Sodium Removal as an Aid to Neutron Activation Analysis. H. R. Ralston and E. S. Sato

68

ANALYTICAL CHEMISTRY, VOL. 43, NO. 1, JANUARY 1971

·

3A

Contributed Articles

AP 100

APIEZON

Determination of Polymeric Isocyanate in the Presence of Reactive Halides.

P. M. Beaz/ey

Evaluation of Methods for Iron in Reduced Iron Ores.

AP 101

LU U>

4 Ul

APIEZON

Ε (3

Amperometric

Titration

of

148

Determination

of

Metallic

S. C. Blum and T. D. Searl

Calcium

and

Using the Lead Dioxide Electrode.

150

Magnesium

C. O. Huber, K.

Dahnke, and F. Hinz

152

NEW APIEZON anti-seize greases stop costly laboratory glassware breakage A P - 1 0 0 is a h i g h v a c u u m C o m p l e t e l y effective in tests grease for use down to against a wide range of a g ­ 5 x 1 0 - 1 1 torr at 1 5 ° C , with a gressive solvents over peri­ s o f t e n i n g point of 3 0 ° C . ods of 72 hours a n d more. A P - 1 0 1 is a n a l l - p u r p o s e Also—Apiezon Oils—low va­ stop-cock grease for moder­ por pressures—very s t a b l e — ate v a c u u m use d o w n t o 1 0 1 ideal as v a p o r - d i f f u s i o n p u m p torr a n d a s o f t e n i n g point of fluids. 185°C. Apiezon Compound Q a T h e s e greases a r e resist­ putty-like, versatile, low cost ant to o r g a n i c solvents a n d sealant. will not leach o u t of g r o u n d Apiezon Waxes for more glass joints or stop-cocks. permanent vacuum joints. Write tor Bulletin 43-AC. Oil

Determination of Nitrogen in Vanadium Nitrides and Uranium Nitride (UN).

D. H. Bollman and D. M. Morti-

more

154

Correspondence Re:

"Criteria for Judging Acceptability of Analytical

Methods."

T. J. Farrell

156

Aids for Analytical Chemists Nonaqueous Electrochemical Cell Capable of Rigorous

JAMES G. BIDDLE CO.

Exclusion of Water and Oxygen.

BIDDLE Electrical and Speed Measuring Instruments PLYMOUTH MEETING. PENNSYLVANIA 19462

J. L. Mills,

Roger

Nelson, S. G. Shore, and L. B. Anderson

157

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Device t o O v e r c o m e S p i n n i n g Difficulties w i t h Magnetic perature.

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ANALYTICAL CHEMISTRY, VOL. 43, NO. 1, JANUARY 1971

© Copyright 1971 by the American Chemical Society

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