C O N T R I B U T E D ARTICLES Scientific C o m m u n i c a t i o n s
Use of M a n g a n e s e ( l l l ) f o r the Spectrophotometric Determination of F e r r o c y a n i d e , Tin(ll), a n d Iron(ll). W. U. Malik and Mohammed Ajmal
Correlation of Microwave A b s o r p t i o n a n d Moisture in Polymers.
JACK MERRITT
Mass Spectra of A m i n o Acids U s i n g a Radio-Fre q u e n c y Spark Source. FISCHER
W . L. BAUN AND D .
W. 294
Spectrophotometric Determination o f Boron Using Barium Chloranilate. R. D. Srivastava, P. R. Van Buren, and Hyman Gesser 209
Spectrophotometric Determination o f Nickel with 1 , 2 , 3 - C y c l o h e x a n e t r i o n e Trioxime. w . J. Frierson and Nina Marable
A R a p i d M e t h o d for the Direct Determination of Ele mental O x y g e n b y Activation with Fast N e u trons. D. J. Veal and C. F. Cook
1 78
Determination o f O x y g e n b y Activation Analysis with Fast Neutrons Using a Low-Cost P o r t a b l e N e u t r o n G e n e r a t o r . E. L. Steele and W. W. Meinke
185
Nitrogen-13 Neutrons.
in H y d r o c a r b o n s I r r a d i a t e d J. T. Gilmoro and D. E. Hull
with
210
Voltammetric Determination of M e t a l s in Low Concen trations. W. W. Ullmann, B. H. Pfeil, J. D. Porter, and W. W. Sanderson 213
P o l a r o g r a p h i c Reduction of 1 , 2 , 4 - B e n z o t h i a d i a z i n e - l , 1 -Dioxides a n d R e l a t e d Compounds. A. I. Cohen, B. T. Keeler, N. H. Coy, and H. L. Yale
216
S q u a r e W a v e P o l a r o g r a p h Amperometric Titrations of Indium with EDTA. R. E. Hamm and C. T. Furse . . .
219
Analysis o f Cesium a n d Rubidium Salts a n d M e t a l s . M.C. FarquharandJ. A. Hill
222
N e w Indicator f o r Volumetric Determination of C o p p e r . Virginia Wills, O. F. Stambaugh, and Z. G. Proctor . .
224
The Determination o f M o n o e t h a n o l a m i n e a n d Ammonia in Air. D. D.Williams and R. R.Miller
225
Spectrophotometric Determination o f t r a t e in Propellants. George Norwitz
227
Fast
Estimation o f M a n g a n e s e in Biological M a t e r i a l b y Neutron Activation Analysis. Hamilton Smith. . . .
Drop Size o f Aerosols in Flame J. A. Dean and W. J. Carnes
207
293
187
190
Spectrophotometry.
Determination o f H y d r o x y l N u m b e r o f P o l y o x y a l k y l ene Ethers b y A c i d - C a t a l y z e d A c e t y l a t i o n . R. S. Stetzler and C. F. Smullin
Spectrophotometric Determination o f Glycine in G l y cine Potassium Trioxalatochromium(lll). H. C. Perrin and G. H. Spaulding
Ultraviolet Spectrophotometric Determination of Ben zoic Acid in Refined Phthalic A n h y d r i d e . Raita Murnieks and C. E. Gonter
The Spectrophotometric Determination of A b i e t i c - T y p e DienOIC Rosin Acids. R. L. Stephens and R. V. Lawrence.
Spectrophotometric Determination o f Furfural in the Presence o f Sulfur D i o x i d e . J. F. Harris and L. L. Zoch .
Solvent Extraction with Q u a t e r n a r y Ammonium H a l ides. A. M. Wilson, Lillian Churchill, Kenneth Kiluk, and Paul Hovsepian
192
1 94
1 96
1 97
Inorganic N i
A p p l i c a t i o n o f C a r r i e r Distillation to the Spectro g r a p h s Determination o f T r a m p Elements in Cast Irons a n d Low Alloy Steels, j . γ. Eiienburg . . . .
230
Effect o f Rate o f N i t r o g e n Adsorption a n d Desorption on the A u t o m a t e d Determination o f Pore Size Distributions. E. v . Ballou
233
Identification of M e r c a p t a n s a n d Disulfides b y X - R a y Diffraction o f Their Respective 2 , 4 - D i n i t r o p h e n y l Thioethers. Robert Rittner, George Tilley, Albert Mayer, Jr., and Sidney Siggia
237
199
201
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VOL. 34, NO. 2, FEBRUARY 1962
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3 A
CONTRIBUTED ARTICLES Precision in X-Ray Spectrochemical Analysis. FixedTime VS. Fixed-Count. L. S. Birks and D. M. Brown . .
Radiochemical Analysis of 240
Infrared Microspectrophotometry Using ReflectingType 6X Beam Condensing Optics in Reference a n d S a m p l e Beams.
Mario Sparagana and W. B. Mason
Direct Titration of Phenols by Bromination.
247
Structural Group Analysis of
Determination Oils.
Polyphenyls. 280
Radiochemical Determination of Yttrium and Promethium. A Precipitation Technique. M. E. Pruitt, R. R. Rickard, and E. I. Wyatt
283
c. o. Huber
and J. M. Gilbert
M i n e r a l Oils. E. Hanson
242
Irradiated
F. F. Felber, Jr., and R. C. Koch
High Sulfur
Far-Ultraviolet Spectroscopic Detection of Gas Chromatograph Effluent. Wilbur Kaye
287
Correction
212
Content
Clarence Karr, Jr., R. T. Wendland, and W. 249
of
N-Phenyl-1-naphthylamine
in
Nicholas Feldman
256
Gamma Ray Absorptiometer for Determination of Uranium in Aqueous and Organic Solvent
Automated End Point for the Determination of Labile Organic-Bound Iodine.
Correspondence
Bennie Zak and E. S. Baginski .
257
Simultaneous Determination of Tin and Indium Using Anodic Stripping Voltammetry. R. D. DeMars . . .
259
Application of Stripping Analysis to the Trace Determination of Tin. S. L. Phillips and Irving Shain . . .
262
Solutions.
S. J. Broderick
295
Purification of Pyridine for Nonaqueous Titrations. W. M. Banick, Jr
296
Spot Test Detection and Spectrophotometric Determination of Nitrite with p-Phenylazoaniline. Eugene Sawicki, T. W. Stanley, and W. C. Elbert
Polarography of Tin(lV)-Pyrogallol Complexes. Bard
.
.
.
297
A. J. 266 Inaccuracy of Dumas Nitrogen Determinations of C e r t a i n 1,2,4-Triazoles.
Polarographic Chloride.
Behavior of
E. J. Browne and J. B. Polya
298
Indium in Presence of
E. D. Moorhead and W. M. MacNevin
. . .
269
Aids for the A n a l y s t Separation of Isopropyl Alcohol from Aliphatic Sulfides and Thiols by Gas Chromatography, v. j . Farmgia and C. L. Jarreau
271
High-Precision Refill Pipet.
Liquid-Liquid Partition Chromatography of Steroids. Systematic Approach Relating Column to Paper Chromatography Using the RM Function. Peter Kabasakalian and J. M. Talmage
.
.
.
Microdetermination of Silver Using Ion Exchange Concentration. N. s. McNutt and R. H. Maier . . . .
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ANALYTICAL CHEMISTRY
Injection
and
Automatic .
.
299
Versatility of Dynamic Sorption Method for Routine Measurements on Solids. K. V. Wise and E. H. Lee .
301
273
Beilstein Flame Method of Detection of Organohalogen Compounds Emerging from a Gas 276
Gas Chromatographic Identification of Major Constituents of Bubbles in Glass. F. R. Bryan and J. C. Neerman
Rapid
H. V. Malmstadt and H. L. Pardue .
278
Chromatograph.
F. A. Gunther, R. C. Blinn, and D. E.
ott
Use of Sample Rotators for Fluorescence Analysis of Light Elements in Cement Raw Mix. A. A. Tabikh
302
303