Cooling of Gases through Packed Tubes - Industrial & Engineering

Max Leva, Murray Weintraub, Milton Grummer, and E. L. Clark. Ind. Eng. Chem. , 1948, 40 (4), pp 747–752. DOI: 10.1021/ie50460a042. Publication Date:...
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Cooling of Gases through Packed Tubes MAX LEVA, MURRAY WEINTRAUB, MILTON GRUMMER, AND E. L. CLARK Central Experiment Station,

U. S . Bureau

of Mines, Pittsburgh, Pa.

The coefficient h of the first equation was differentir with respect to D, a t Dt and G = constant, and a m mum heat transfer coefficient was predicted for a -ti DP - = 0.153. This was verified experimentally.

H e a t transfer coefficients were determined for the flow of heat from hot air and carbon dioxide to cooling water. Tests were made with a 2-inch and a S/d-inch standard packed pipe. The packing material was of low thermal conductivity, spherical, and smooth. The ratio of particle to tube diameter varied from about 0.08 to 0.27. The gas flow range was characterized by the modified Reynolds number interval 250-3000. Two dimensionally homogeneous equations were proposed correlating film coefficient h w i t h the physical properties of the system. Thus:

Dt

second equation is not quite so precise as the first fc but for most engineering work it is accurate enough, on account of its greater simplicity should be prefe to Equation 1. Both equations state that h is pro tional to

($).

This was proved by determining

transfer coefficients for carbon dioxide. The value of group is 229’0 smaller for carbon dioxide than for air. check between the air data and carbon dioxide data excellent. The possible inclusion of the Prandtl nul is discussed as well as the application of the equatioi tube sizes larger than 2 inches.

and, by an approximation of Equation 1,

E

ARLIER work (1) in this field revealed t h a t heat transfer

ture. The air outlet of the small tube was open, and then two copper-advance thermocouples which, for all the experir were approximately l / 4 inch below the adjustable screen a inch apart from each other. The temperature gradieni served were negligible in all cases. The water jacket me2 36 inches on the large and 14 inches on the small tube.

coefficients of gases passing through packed tubes could be correlated by the equation:

The validity of this expression for a wide range of gas. heating operations was stressed a t that time. There was, however, no experimental evidence to show whether this equation could also be used to estimate heat transfer coefficients for gas cooling operations. A few orienting experiments with a 2-inch tube were sufficient t o indicate t h a t the above equation did not apply t o cooling operations. The experimental findings were about 15y0 higher than the calculated values. It appeared, therefore, that typical data were required if a correlation was to be achieved which would permit the prediction of gas cooling coefficients.

f

valve I

,

va

\0

Thermometer Thermocouple

UNIT AND OPERATION

Figure 1 shows essential details of the experimental equipment. Two tubes served as test units. Measured quantities of air could be admitted to either the 2-inch or a/*-inch tube. By proper manipulation of valves 1 and 2, the temperature of t h e air arriving a t the tubes.could be controlled satisfactorily. To induce good mixing and thereby avoid temperature grtdients, the air entered the tubes sidewise through tees. At this point the inlet air temperature was measured by mercury thermometers. The air left the large tube through a reducer and throttle valve. Horizontal temperature explorations revealed t h a t this device was well suited for equalizing the air tempera-

\Thennometar Blower

Water inlet

Figure 1. Unit for Determination of Cooling Coeffi

747

INDUSTRIAL AND ENGINEERING CHEMISTRY

748 TABLE I.

5;; -. _.

ZU

COLLECTED WITH

DATA

G

Re

ti

575

498 426 349 328 268 215 160

327.5 330,b 324 324 5 337.0 330.3 331

tz

tw

%INCH

TUBE

At

Q

78.6 77.5 74.0 73.0 65.9 61.6 33.4

2370 2058 1648 1557 1348

h

hDt k

D p = 0.169 1n.b 41.6 35.6 29.2 27.4 22.4 17.95 13.40

1-a b

8 7 ,5 86.5 86.0 85 83 82 80.5

Dp 2-a b c d e f g

39.2 30.1 25.6 21.5 18.18 15.01 11.37

1681 1291 1098 905 765 632 479

478 367 312 258 218 180 137

324 337 337 338 335.5 327.5 333

3-a b

51.4 44.5 37.0 29.06 25.8.5 20.9 17.28

2205 1910 1588 1248 1110 896 740

841 730 606 476 420 339 280

331.5 331.5 338.5 336.5 326 329 328.5

48.5 43.1 40.0 34.9 29.8

2078 1840 1720 1498 1277

780 695 643 561 480

335 339.5 330.5 337 329.5

57.7 49.8 42.4 30.2 30.2 25.4 19.61

2480 2140 1819 1295 1295 1090 841

1583 1367 1161 827 827 697 537

325.5 335.5 336 333.5 330 331 333.5

1690 1556 1465 1230 912 1551 1386 1260

382 397.5 397.5 398.5 398.5 394 361 366.5 363.5

2230 2080 1745 1360 985 852 691 561

1430 1330 1120 870 631 546 443 360

329 337 333.5 334 330.5 321 5 328.5 335

3158 2836 2432 2105 1767 1470 1215 1063 923 785 654 543

265.5 2384 2045 1770 1485 1284 1020 895 776 660 550 457

331.5 336 335 325 325 339 329.5 330 324.5 325 329 335

2690 2450 1982 1561 1287 1055 857 679 513

2258 2058 1663 1312 1086 886 720 570 430

323.5 333.5 336 337,5 332,5 331.5 330 330 328

75.5 75.5 76 76 77.5 77.5

77

795

20.2 18.0 15.0 14.3 13.7 11.5 8.90

192 170 142 135 130 109 84.0

71.9 71.9 70.0 69.1 65.8 62.8 60.8

2210 1802 1535 1300 1091 874 679

20.6 16.7 14.8 12.6 11.0 9.0 7.50

195 158 140 119 104 85 71

84.8 82.9 81.8 75.4 72.0 70 4 67.7

2978 2590 2223 1684 1493 1230 1019

24.0 21.0 18.3 15.0 14.0 11.7 10.0

227 199 173 142 133 111 95

87.8 87.4 83.5 82 1 76.9

2830 2468 2310 2076 1735

21.6 19.0 18.6 17.1 15.2

205 180 176 162 144

80.3 79.8 78.9 73.9 71.4 70.5 66.7

3240 2932 2510 1786 1768 1497 1174

27.6 25.0 21.5 16.1 16.7 14.1 11.9

262 238 204 153 159 134 113

105 105 103 104 100.3 88 93.5 93.2 93.0

4358 4294 4045 3392 2530 1832 3724 3400 3070

28.3 27.2 27.0 22.0 17.0 14.0 27.2 25.0 22.5

271 260 258 210 162 134 2 52 231 208

81

72.5 64.3 64 62.2 60

2980 2790 2400 1880 1360 1140 950 795

25.0 22.5 21.4 17.5 14.1 11.9 10.0 8.50

237 213 203 166 134 113

97.6 93.2 88.1 83.3 78.9 78.2 73.0 70.8 68.5 66.0 64.0 63.6

4180 3850 3116 2765 2342 2085 1668 1470 1250 1061 911 779

29.8 28.3 24.0 22.5 20.0 18.0 15.2 14.0 11.7 10.7 9.50 8.00

280 a67 226 212 188 170 143 132 110 101 90 75

30.0 28.5 23.5 18.3 17.2 14.6 12.5 10.2 7.70

285 271 223 174 164 139 119 97 73

1057

= 0.169 I n .

86.0 84.5 84.0 83.0 82.5 82.0 81.0

77.0 77.0

77.0 76.5

77.0 77.0

77.0

D p = 0.228 In.

c

d e f g

87

86 85 82 81.5 80.5 79.5

72.5 72.5 73 73 73 73 73

D p = 0.228 In. 4-a b c d

e

89 88 87 86 84

73 73 73 73.5 73.5

a

D p = 0.388 In. 5-a b c d e f g

88.5 87 86.5 84 83 82.5 81

75.5 75.5

75.5 75 75 75 75

D p = 0.388 In.

e f

i?

i

63.3 58.4 54.9 46.1 34.2 24.6 57.1 51.0 46.3

657

71.5

io

71 71.5 71.5 71 71.5 70.5 69.5

D p = 0.388 I n . 7-a b c d e f

51.7 48.1 40.4 31.4 22.8 19.8 16.0 13.0

Dp 8-2

b

: e

f

85 83.5 82 81

78

77.5

77

76.5

72.5 73 72.5 73 73 72 72.5 73

84 76

95 80

= 0.5075 I n .

92

00 .~

88 86.5 84.5 82 80.5 79.5 78 ’ 78 77 76

70 71 72 72 72.5 72 72 72 72 72 72 72.5

D p = 0 . SO75 In. 9-a b

ki

62.7 57.1 46.2 36.4 30.0 24.6 19.98 15.83 11.96

a Runs

75 7.5

82 81 80 79 79

74.5 74.5 85 75 75 75 75

79.8 80.2 80.1 74.1 69.5 66.7 63.6 60.4

60.0

1 to 7, inelwive, were made with glass beads of diameters as indicated: runs 8 and

9 were made with porcelain balls. b Packing height in all cases was 36 inches; air was used f o r eYery run.

Vol. 40, No. 4

the pipes were assembled, they were cleaned of all dirt, but the surfaces were not etched or polished. The circulation rate of the cooling water was kept at. t,he fairly high ve1ocit.y of 3 feet per second through the large, and 9 feet per second t,hrough the small annulus. -4s ,the temperature rise of the water a t these rates was negligible, it was sufficient to record only the inlet, water temperat,ure. For each of the various paclrings investigated, the following readings were made: air rate through tube; inlet and exit air temperatures; and wat,er temperature. On the basis of the inside packed-hibe diameter, the height, of the pacliing in the tube, and the assumpt,ion that a logarithmic temperat,ure difference prevailed betn-cen air and water, heat-transfer coefficients were calculated. All physical properties of the fluids were evaluated at, the average bulk temperatures. PACKISGMATERIALS.Low thermal conductivity [