CORNING Chromatography Products - Analytical Chemistry (ACS

May 29, 2012 - CORNING Chromatography Products. Anal. Chem. , 1969, 41 (2), pp 24A–25A. DOI: 10.1021/ac60271a721. Publication Date: February 1969...
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What makes Coming's new automatic preparative gas $ diromatograph worth 14,500? It works more efficiently

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CefRing's APG 402 is a preparative gas chromatograph with system efficiency equal to that of many analytical units—and better than most preparative units. Take the terpene separation often used to demonstrate chromafographs. West units easily separate the a and β pinene fractions. But many miss the four minor impurities normally present. Cefiwif's APG 402 cleanly resolves all six fractions, as shown in this chart of a typical run. Two of the five collected fractrans were at least 9 t % pure; the others at least 95% pure. And material balance snows an overall recovery of 98% of the injected sample. Seniftd this purity is a unique injection system that keeps the sample under inert carrier gas at all times—and a collection manifoid that uses a ceuntercurrent gas purge to positively prevent fraction cross-contamination—and the most flexible trapping system ever put in a preparative gas chromatograph, aHowing you to optimize trapping of each fraction. 24 A

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ANALYTICAL CHEMISTRY

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The APG 402's collection programmer offers you a virtually un­ limited range of fractionation possibilities—so you can do a wider range of separations. There are five collection traps and one waste trap. Electronic logic lets you open and close each one at any point on the chromatogram. Opening and closing of each trap is inde­ pendently adjustable for the same peak—and can be set to any point on the front or back slope. With this flexibility, you can (1) collect up to five individual peaks in the five traps; (2) divide large peaks into fractions; (3) accumulate up to nine peaks as a single fraction; (4) waste up to eight peaks before beginning collection—or combine any or all of these options into a single sequence. And for more flexibility in the compounds you can handle, Coming's APG 402 is the only preparative gas chromatograph that offers an optional glass system.

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