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Addition/Correction pubs.acs.org/joc
Correction to “Pd-Catalyzed Conversion of Aryl Iodides to Sulfonyl Fluorides Using SO2 Surrogate DABSO and Selectfluor” Ariana L. Tribby, Ismeraí Rodríguez, Shamira Shariffudin, and Nicholas D. Ball* J. Org. Chem. 2017, 82 (4), 2294−2299. DOI: 10.1021/acs.joc.7b00051 Page 2296: The following text should be added as a third paragraph in the Experimental Section. The authors apologize for any inconvenience to the scientific community that this omission may have caused. Fluorination Step. After 14 h, the tube was allowed to cool to room temperature. The tube was opened to air, and Selectfluor (638 mg, 1.8 mmol, 2 equiv) was added followed by acetonitrile (3 mL). The Schlenk tube was resealed, and the mixture was allowed to stir at room temperature for 2 h. After 2 h, the solvents were removed by rotary evaporation. The crude product was isolated using automated flash chromatography (SiO2) on a 100% hexane to 60:40 hexanes/ethyl acetate over 14 min unless otherwise noted.
© XXXX American Chemical Society
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DOI: 10.1021/acs.joc.7b01097 J. Org. Chem. XXXX, XXX, XXX−XXX
