Correction to “Total Syntheses of Lyconadins A–C” - Journal of the

Apr 2, 2014 - ... solvent and other impurities. The stored samples of 13, 17, 4, and 21 were reanalyzed. The original FID of 30b was located, and the ...
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Correction to “Total Syntheses of Lyconadins A−C” Takuya Nishimura, Aditya K. Unni, Satoshi Yokoshima, and Tohru Fukuyama* J. Am. Chem. Soc. 2013, 135, 3243−3247. DOI: 10.1021/ja312065m S Supporting Information *

Supporting Information, pages S4 and S26. The 13C NMR spectrum of compound 9 was improperly manipulated in the originally published Supporting Information to obscure peaks corresponding to solvent and other impurities. The stored sample of 9 was reanalyzed, and the corrected list of the peaks and the unaltered spectrum are included in the revised Supporting Information. Supporting Information, pages S35, S37, S43, S45, and S55. The 1H NMR spectra of compounds 13, 17, 4, 21, and 30b, respectively, were improperly manipulated to obscure small peaks corresponding to solvent and other impurities. The stored samples of 13, 17, 4, and 21 were reanalyzed. The original FID of 30b was located, and the spectrum was reprocessed. The unaltered spectra are included in the revised Supporting Information. The changes do not affect any of the conclusions of the article.



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S Supporting Information *

Additional text with experimental details, characterization data, and NMR spectra (revised). This material is available free of charge via the Internet at http://pubs.acs.org.

Published: April 2, 2014 © 2014 American Chemical Society

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dx.doi.org/10.1021/ja5025386 | J. Am. Chem. Soc. 2014, 136, 5817−5817