Correction to Total Synthesis of (−)-Huperzine A - Organic Letters

Feb 3, 2014 - ... serrata (=Lycopodium serratum) in minuscule amounts. The most efficient total synthesis of huperzine A, the first asymmetric total s...
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Addition/Correction pubs.acs.org/OrgLett

Correction to Total Synthesis of (−)-Huperzine A Takahiro Koshiba, Satoshi Yokoshima, and Tohru Fukuyama* Org. Lett. 2009, 11(22), 5354−5356. DOI: 10.1021/ol9022408 S Supporting Information *

S

olvent peaks had been removed from the 1H NMR spectra reported for compounds 10 (S6) and 14 (S14). The revised Supporting Information now contains the full spectra for these compounds. Original FIDs were located, and the spectra were reprocessed and have been replaced for the above compounds in the revised Supporting Information submitted with this correction. The spectra editing did not affect any of the conclusions of the published paper. The purities calculated on the basis of the revised spectra and corrected yields are as follows: 10 (94% purity, 75% yield), 14 (97% purity, 86% yield).



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S Supporting Information *

Revised Supporting Information including reprocessed spectra. This material is available free of charge via the Internet at http://pubs.acs.org.

Published: February 3, 2014 © 2014 American Chemical Society

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dx.doi.org/10.1021/ol500160t | Org. Lett. 2014, 16, 1270−1270