ANALYTICAL CHEMISTRY
554
Partial -Powder X-Ray Diffraction Pattern of Zr(SO&.4H20 d , A., Calcd. 6.527 5.308 4,025 4.346 3.617 3.483 3.264 3.155 2.993 2.985) 2.905
hkl 400 220 111 311 51 1 620 800 131 71 1 331 040 202 53 1 440 911 022 222 73 1 10.2.0 a b
2.664
d , A.; Obsd. 6.49 5.30 4.90 4.32
...
3.47 3.24 3.15 2.98 2.91 2.71
...
2.50 2.463 2.419 2.382
2: 408 2,373
1/11b 45 5
25 100
...
30 5 5
75 15 5 10
... 20
10
hkl 602 422 12.0.0 622 840 11.1.1 931 151 351 822 242 551 442 200 10.0.2 11.3.1 13.1.1 751 113 642
d, A., Calcd.,
d, A.& Obsd.
I/Iib
2,341 2.176' 2.173. 2.170 2.146 2.143. 2.137,
2.332
36
2.164
5
2.134
30
2.080
5
1,980
25
1.910
