Design and analysis of industrial experiments

Waco, Texas. WILLIAM B. COOK. •. CHEMISTRY OF THE PESTICIDES. Donald E. H. Frear, Professor of Agricultural and Biological. Chemistry, Pennsylvania ...
1 downloads 0 Views 1MB Size
654

JOURNAL OF CHEMICAL EDUCATION '

use more initative; more unknowns and experimental problems. New experiments included in this edition include those on elution and paper-strip chromatography, enzymatic and spontaneous resolution, formation of geometricalisomers, and cost cslculatiotions. In this reviewer's opinion, the text will serve admirably for the undergraduate organic chemistry lahoratory. It may be used also as a constant source of help for graduate students in research. The Instructor's Manual (23 pp., available for 406) will prove especially helpful in planning organic laboratory work as it has a rather complete list of chemicals needed, suppliers, and up-to-date prices. Also included are many helpful suggestions wit,h regard to the experiments included in the text.

is extremely well covered. But the principal value of the book lies in its particularly appropriate method and plan of presentation and in its lucid style. The reader soon feels that an attempt is made to help him solve his problems, rather than to force upon him artificial problems for which statistical solutions happen to exist. The introductory first chapter is followed by one entitled The Planning of Simple Comparative Experiments, which is an excellent, though brief, exposition of the main principles underlying the st.atisticd method. Chapter 3, entitled Sequentid Tests of Significance, while interesting and important, can be omitted in s. first study of the subject. Beginning with Chapter 4 the reader i8 gradually led into experimental designs of increasing complexity. Randomized blocks, Latin square designs, KO'' incomplete block designs, and factorial as well as fractional fmBArmn U ~ n l ~ n s r ~ ~ torial experiments arediscussed in great detail and illustrated by W I C O , TBXM mesns of numerical examples. In the factorial designs a clear dietinotion is made between qualitative and quantitative factors, and a. much neglected subject, the use of regression methods in CHEMISTRY OF THE PESTICIDES combination with analysis of varianoe, is adequately treated. to lstatistics, H, Frear, Professor A~~~~~~~~~ and ~ ~ The last ~ chapterl deal8 with ~ a recent ~ contribution ~ State University, Third edition, D, the sequential method developed by Box and his co-workers for Chemistrl, Ir, NDstrmd Co., New 1955, vi + 469 pp, 32 the determination of optimum conditions, the most important ~pplicationof which is the search for maximum yield conditions figs. 19 tables. 16 X 23 om. $8. in chemical manufacturing processes. This reviewer has only one major complaint in connection with T m k s t edition of this well known and vslushle text and reference hook appeared in 1942, with 300 pages; the second this excellent hook: the omission of an adequate discussio~of edition was published in 1948, with 417 pages; this third edition partially balanced incomplete block designs. Indeed, experihas 469 pages despite the deletion of detailed andytical pro- ments in the physical sciences are often characterized by relatively oedures for insecticides and fungicides (which occupied 68 pages small random errors but large systematic errors. Therefore, a in the first edition and 73 pages in the second edition). This amall number of replications is generally sufficient, and the necessary increase in pagination reflects very well the growth and presence of several levels of precision is n o t objectionable as long as the comparison of lowest precisian is still satisfactory. recognition accorded this field of endeavor. This book is highly recommended to experimental workers in In general, this third edition represents an extensive revision of the second edition, with the inclusion of many new insecticides, the physical sciences. fungicides, herbicides, and, for the first time, rodenticides of JOHN MANDEL NATIONAL oI. current interest. The seven parts of the book are: I, Synthetic Organic Insecticides (138 pp.); 11, Natural Organic Insecticides W ~ s n w a ~ o D. a . C. (94 pp.); 111, Inorganic Insecticides (45 pp.); IV, Fungicides (79 pp.); V, Herbicides (36 pp.); VI, Adjuvants (24 pp.); and 0 BASIC LUBRICATION PRACTICE VII, Rodenticides (15 pp.). This book will be even more valuable than its predecessors as an authoritative, surprisingly oomplete compendium of AIIen F. Brewer. Reinhold Publishing Corp., New York, 1955. 286 PP. Many figs. and tables. 15.5 X 23.5 cm. $6.75. information on origin, general chemistry, properties, methods of xiv preparation, featured applications, and some pertinent chemical an Opening on haw operating conditions affect reactions As withofthe the four major editions, classes of pesticides. has written this book lubrication and a second chapter on the significance of physical tests af lubricants, the book devotes 19 ~haptersto meehrtnical with skill and certainty. The index is commendahl~complete, and design features of md its for soccessful and very few typographical errors are apparent. There may be lubrication. Final chapters are on storage, reconditioning used some confusion among readers not familiar with organic chemistry oils, and nonpetroleum lubricants. as to which of the structural formulas containing carbocyclic rings are aromatic and which are saturated for many of the compounds represented. ALUMINUM PAINT AND POWDER "Chemistry of the Pesticides" is highly recommended for the teacher and student interested in pesticides, and for the research Junius David Edwards and Robert I. Wmy. Third worker looking for a convenient and very complete catalogue of Reinhold Publishins Corp.. New York, 1955. ai + 2219 pp. 76figs. 21tables. 15.5 x 23.5 cm. $4.50. basic facts about all currently important pesticidal chemicals.

''

*

=.

+

.

F. A. GUNTHER

Unmsssmr ar CA~rvonnc* Rrvensre~.CALIIORNI*

0

DESIGN AND ANALYSIS OF INDUSTRIAL EXPERIMENTS

How duminum powder is made and its use in metallurgy, plastics, and other industries. Aluminum paints are of various typesand have both generaland specific applications to wood and metale. 0

FABRICATED MATERIALS AND PARTS

Edited by Owen L. Davies. Hafner Publishing Company, New 636 pp. 16 tables. 16 X 2 5 em. $10. York, 1954. ziii

Theodore C. DuMond. Reinhold Publishing Corp., New York, 1955. v f 322 pp. 117 figs. 19 fables. 15 X 22 em. $6.50.

THISbook, which is the joint work of George E. P. Box, Lewis R. Connor, Wilfred R. Cousins, Owen L. Davies, Francis R. Himsworth, and George P. Sillitto, marks animportant milestone in the application of statistics to the phyeical sciences. With a single exception, noted helaw, the field of statistical design

SOMEproduction methods for producing small parts are discussed-e. g., castings, forgings, extrusion, powder metal parts, spinning, electrofonning, bonded, molded plastics, and formed, nonmetallic materials. Cost, production, and design factors are discussed.

+