ACKNOWLEDGMENT
Table 111.
Determination of Corrosion Products and Additives in Synthetic Homogeneous Reactor Fuel Composition of Synthetic Fuel. U(VI), 40 g.,liter; Al(TII), 50 mg./liter; Si(II), 100
mg./liter; Fe(III), 100 mg./liter; Zr(IV), 100 mg./liter; Cu(II), 100 mg./liter; Cr(IIT), 50 mg./liter. Synthetic Rel. Ion Fuel Taken, ,111. Ion Found, y Diff., y Std. Dev., % AI( IIT) 1 0 49 5 -0 5 3 2 0 6 30 4 to 4 0 4 19 8 -0 2 0.2 9 4 -0 6 Si(I1) 1.0 100,2 +0.2 2.3 $1 0 101.0 0 2 21.1 $1.1 20.4
Fe(II1)
98.0 99.0 19.5 19.5 59.3 29.5 24.5 29.0 100.1 100.0 9.8 10.2 19.9 20.2 19.6
1.0
0 2 Zr(1V)
Cu(I1)
0.62 0.30 0.25 0.29 1.0 0.1
Cr(II1)
0.4
20.8
1-0.4
-2.0
-1.0
-0.5 -0.5 -2.7 -0.5 -0.5 ... +o. 1
...
-0.2 $0.2 -0.1 +0.2
0.7
1.8
1.6
2.5
-0.4 $0.8
The polarographic cells for use in the High Radiation Level Analytical Facility were designed by TV. L. Aladdox of this laboratory. LITERATURE CITED
(1) Horton, A. D., ANAL. CHEM. 25, 1331 (1953). (2) Horton, A. D., Thomason, P. F., Ibid., 28,1326 (1956). (3) Kraue, I
