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J. Org. Chem. 1985,50, 3649-3651 mishaps occurred in over 50 reactions with other alkenes. General Procedure for D a t a in Table I. 1-Decene (5.0 mmol), manganese(II1) acetate hydrate, and sodium azide were refluxed in glacial acetic acid at the concentrations specified until the dark brown color had disappeared (