APPENDIX A Chromatographic Techniques for the Separation of Polymethoxyflavones from Citrus (Chapter 1) Ram M. Uckoo, G. K. Jayaprakasha, and Bhimanagouda S. Patil*
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Vegetable and Fruit Improvement Center, Department of Horticultural Sciences, 1500 Research Parkway Ste A120, Texas A&M University, College Station, TX 77845 *E-mail:
[email protected] © 2012 American Chemical Society Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
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572 Figure 1. Structures of polymethoxyflavones isolated from citrus.
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
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573 Figure 2. Structures of hydroxylated polymethoxyflavones isolated from citrus.
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
574
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Table 2. 1H NMR of polymethoxyflavones isolated from citrus species
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
575
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Table 2. (Continued) 1H NMR of polymethoxyflavones isolated from citrus species
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
13C
NMR of polymethoxyflavones isolated from citrus species
576
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Table 3.
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.
577
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Table 3. (Continued) 13C NMR of polymethoxyflavones isolated from citrus species
Patil et al.; Emerging Trends in Dietary Components for Preventing and Combating Disease ACS Symposium Series; American Chemical Society: Washington, DC, 2012.