Asymmetric Reduction of a 1,5-Benzothiazepine Derivative with Sodium Borohydride−(S)-α-Amino Acids: An Efficient Synthesis of a Key ...
irradiation. However, the rate of the photoreduction of 4-cholesten-3-one (I) was enhanced by a factor of 22.5. The photoreduction of I with sodium borohydride ...
Total synthesis of dl-dihydrocallitrisin, dl-7,8-epialantolactone, dl-7,8-epiisoalantolactone, and dl-atractylon. Arthur G. Schultz , Jollie D. Godfrey. Journal of the ...
WITH SODIUM BOROHYDRIDE. 2273 to a mixture of a mercaptan (5-20 mole equivalents) and triethylamine (1.5-5 mole equivalents) at â20° (if methane-.
The reduction of conjugated aldehydes and ketonos by sodium borohydride leads, in general, to substantial amounts of fully saturated alcohol products.
1-butanethiol are used). The reactionmixture is allowed to warm to room temperature upon stirring. The precipitated triethylamine hydrochloride is filtered off ...
Reduction of Nitroaromatic Compounds with Sodium Borohydride. Lloyd A. Kaplan. J. Am. Chem. Soc. , 1964, 86 (4), pp 740â741. DOI: 10.1021/ja01058a046.
Sodium borohydride reduction of steroidal ketones with and without irradiation. James A. Waters, Bernhard Witkop. J. Am. Chem. Soc. , 1968, 90 (3), pp 758â ...
Different examples of alkyl diphenylphosphinates were studied but results were similar to ours. Reduction of Alkylidenecyanoacetates with Sodium Borohydride.
Nov 13, 1978 - (12) J. W. Timberlake and J. C. Martin, Rev. Sci. Instrum., 44, 151 (1973). (13) B. K. Bandlish, A. W. Garner, M. L. Hodges, and J. W. Timberlake, ...
1720 J . Org. Chem., Vol. 44, No. 10, 1979
Notes
Table I. S(l3C) Values (in ppm, Relative to Mersi) of Reduced AzanaphthalenesO
