Inorganic Chcnz istry
918 NOTES TABLE I1 OBSERVED A S D CALCULATED STRUCTURE FOR
FACTORS
[ s(C H S ) zB&e ~]
K&!
Fc
2
I?
L
0
0
2
92
-95
1
5
9
10
0
0
4
32
30
1
7
7
5
3
0
0
6
48
48
2
2
2
53
-54
5
KIEI 9
0
0
8
15
2
2
4
8
0
0
10
12
:2
2
2
6
io
9 -8
0
2
2
136
140
2
2
8
10
12
0
2
4
6
2 1 0
0
0
0
2
6
4
-3
2 2
4
4
47
-47
0
8
11
11
2
4
6
11
9
0
2 2
10
21
22
2
4
8
17
-17
0
4
4
12
11
2
4
IO
13
12
0
4
6
27
-26
2
6
6
33
-35
:5
0
4
8
20
21
2
6
8
16
15
0
4
10
5
-4
3
3
51
51
0
6
6
28
29
3
3 3
5
60
-58
0
6
8
20
3
3
7
8
-9
0
8
8
23
-20 22
3
3
9
12
12 -3
1
1
1
15
73
3
5
5
4
1
1
3
58
58
3
5
7
8
-8
1
1
5
0
1
3
5
9
10
-11
1
1
7
14
15
3
7
7
8
-11
1
1
9
IB
19
4
4
4
:
11
7
10
4
4
6
-38
1
1 3
8 38
3
48
-46
4
4
8
0
1
1
3
5
:6
15
4
6
6
5
-5
1
3
7
0
-2
4
6
8
11
-10
1
3
9
0
4
5
5
5
29
-28 -16
6
1
5
5
20
-19
5
5
7
17
1
5
7
6
-5
5
7
7
7
-4
8
6
6
11
-11
B-B B-H C-N C- H
TABLE I11 BONDDISTANCES IN [S(CH3)a]zB6Hs 169i00lA 1 11 A 0 0 7 A 148+0 0lA 0 99 f 0 04