NEWS
ABSORPTION CELLS MADE OF
GLASS—SPECIAL GLASS QUARTZ GLASS ACID RESISTANT FUSED
9:25 The Performance of the Interrupted Discharge in Argon. H. T. Dryer, F . Borile, Applied Research Labora tories, Detroit, Mich. 9:50 Spark Excitation in Controlled Atmospheres. Arno Arrak, Grumman Aircraft Engineering Corp., Bethpage, L. I., Ν. Υ. 10:35 Experimental Studies of the Molecular Emission Spectra of the Monoxides of Rhenium and the Metals of the Platinum Group. Victor Raziunas, Sidney Katz, I I T Research Institute, Chicago, 111. 10:55 Spectroscopy of Divalent Rare E a r t h Ions in Crystals. D. S. McClure, University of Chicago, Chicago, 111. 11:20 Crystal Mapping by Emission Spectroscopy. Jack F . Massengale, Texas Instruments, Inc., Dallas, Texas. 11:40 Transformation Functions for Photographic Response D a t a in Spectrography. J. M . McCrea, Applied Research Laboratory, United States Steel Corp., Monroeville, Pa. GAS CHROMATOGRAPHY Friday Morning—East Room Brian Andreen, Institute of Gas Technology, Chicago, III., Presiding
9:00 A New Method of Pyrolysis. Theron Johns, R. A. Morris, Beckman Instruments, Inc., Fullerton, Calif. 9:30 Refinement of Pyrolysis Techniques for Gas Chro matography. W. M . Barbour, Barber-Colman Co., Rockford, 111. 10:20 Polymer Analysis by Pyrolysis Gas Chromatography. B. Grotent, Esso Research and Engineering Co., Linden, N.J. 10:50 Gas Chromatographic Determination of Total Oxygen in Organic Materials. F . L. Boys and D . D . Dworak, Sin clair Research, Inc., Harvey, 111. 11:20 Gas Chromatographic Methods for the Detailed Study of Controlled Temperature Polymer Degradation. Robert T. Conley, Seton Hall University, South Orange, N . J., and Martin Co., Baltimore, Md.
PRECISION CELLS, INC. 401 BROADWAY NEW YORK, Ν. Υ. 10013 Write for Cafalog
No. 6 2 / 3 0
NMR SPECTROSCOPY
Circle No. 73 on Readers' Service Card
Separate Alkali Metals & Alkaline Earths Rapidly On Short Columns Use BIO-RAD Ion Exchange Crystals Bio-Rad 2 M (zirconium tungstate) 0.13 cm1 χ 12.3 cm column, 0.75 cm/min. flow rate, trace loading.
Illustrated is an alkali metals separation which can be effected on any one of these new in organic exchangers. Adsorption usually takes place from acidic solutions. Increasing con centrations of ammonium chloride or nitrate are used for elution. Bio-Rad Ion Exchange Crystals are inorganic microcrystalline aggregates with ion exchange capacities and properties similar to those of conventional ion exchange resins, but whose deferences oiler special advantages including the ability to perform separations at temperatures up to 300° C and to withstand high level radiation without breakdown. High selectivity for specific ions allows chromatographic analysis of trace materials in concentrated solutions. Separations of precious metals, cesium from brines, polyvalent anion;, and reactor fission products are described in "Ion Exchange Crystals"—check below.
BIO-RAD Laboratories 3 2 N D & GRIFFIN AVE., RICHMOND 1, CALIF. Gentlemen: I would appreciate further information o n : Π
Ion exchange resins
Π Adsorbents for chromatography
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Ion exchange celluloses
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Labeled compounds ( C u , C' 4 , N 5 , H : )
Ion exchange crystals
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Stable isotopes
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_] " C h e m t a m " standard solutions NAME
TITLE
ORGANIZATION ADDRESS CITY
STATE
Circle No. 23 on Readers' Service Card
52 A
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ANALYTICAL CHEMISTRY
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Friday Afternoon—San Juan Room 2:00 Determination of 3-(p-Chlorophenoxy)-l,2-Propanediol, 2-Carbamate in 3-(p-Chlorophenoxy)-l,2-Propanediol, 1-Carbamate by NMR. G. Slomp, R. H. Baker, Jr., F . A. MacKellar, The Upjohn Co., Kalamazoo, Mich. 2:25 Signal-to-Noise Determinations. G. Slomp, The Up john Co., Kalamazoo, Mich. 2:40 Further Considerations of Instrumentation and Tech niques. Eugene A. Pier, Varian Associates, Palo Alto, Calif. 3:30 Panel and Problem Solving Session Herman A. Sssymanski, Canisius College, Moderator. Charles Bell, University of Illinois. Speakers of the N M R Symposium. EMISSION—FLAME—ATOMIC ABSORPTION SPECTROSCOPY Friday Afternoon—Tally-Ho Room John A. Norris, Jarrell-Ash Co., Newtonville, Mass., Presiding
1:45 S p e c t r o g r a p h s Determination of Rhenium in Molyb denite with the D.C. Arc. W. G. Schrenk, Show-jy Ho, Department of Chemistry, Kansas State University, Man hattan, Kan. 2:05 The Determination of Boron in Metal Particles Using the Copper Fluoride Evolution Technique. K. W. Guardipee, J. E. Paterson, M . E. Waitlevertch, Jr., A. L. Wolfe, Westinghouse Electric Corp., Research and Development Center, Pittsburgh 35, Pa. 2:25 The Influence of Thermal Conductivity of Electrodes upon the Spectrochemical Analysis of Small Samples and Trace Concentrations. F. J. Haftka, Union Carbide Euro pean Research Associates, Brussels 18, Belgium. 2:45 Application of a Digital Computer Quantometer to the Analysis of Aluminum Alloys and the Advantages Obtained. T. J. Hudson, W. L. Lee, Aluminum Co. of Canada. 3:30 Panel Discussion Panelists: Sabina Sprague, Atomic Absorption John A. Dean, Flame Alan Goldblatt, Arc-Spark Emission E m m e t t Kaelble, X-Ray