J. Am. Chem. SOC. 1986, 108, 7435-7436
7435
Scheme I
-rjs+-
'
I
-0H'
H
la
H '
IC
2
3
6 Figure 1.
plot of N-(S)-(-)-(4-methylcyclohexylidene)fluoroacetyl-L-(-)-ephedrine. ORTEP
Scheme I
4
ca. 10-20% of linalol is ~ b t a i n e d . ~ . ~ . ~ Compressed geraniol films are similarly unreactive, again giving