Addition/Correction Cite This: J. Am. Chem. Soc. XXXX, XXX, XXX−XXX
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Correction to “An Alkyne−Aspirin Chemical Reporter for the Detection of Aspirin-Dependent Protein Modification in Living Cells” Leslie A. Bateman, Balyn W. Zaro, Stephanie M. Miller, and Matthew R. Pratt* J. Am. Chem. Soc. 2013, 135, 14568−14573. DOI: 10.1021/ja408322b S Supporting Information *
Page 14571. The following errors should be corrected in the Experimental Procedures section on Synthesis of AspAlk: • The incorrect IUPAC name for AspAlk was given. The correct name is 2-[(1-oxo-4-pentyn-1-yl)oxy]benzoic acid. • The deuterated solvent used to collect the 1H NMR was incorrect. The correct solvent is CD3OD. • The deuterated solvent used to collect the 13C NMR was incorrect. The correct solvent is (CD3)2CO. • The peak list for the 13C NMR was incorrect. The spectrum was taken in (CD3)2CO, but the spectrometer was set to CD3OD, causing the shifts to be inaccurate. The correct list is δ 169.92, 164.90, 150.97, 133.88, 131.76, 125.98, 123.87, 123.59, 82.32, 69.65, 33.23, 13.66. Supporting Information. The 13C NMR spectrum has been replaced.
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ASSOCIATED CONTENT
S Supporting Information *
The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/jacs.8b03225. Supporting figures, NMR characterization of AspAlk, and proteomic data (corrected) (PDF)
© XXXX American Chemical Society
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DOI: 10.1021/jacs.8b03225 J. Am. Chem. Soc. XXXX, XXX, XXX−XXX