Second Annual Meeting
^ACSS
Federation of Analytical Chemistry and Spectroscopy Societies October 6 - 1 0 , 1975 Indiana Convention-Exposition Center Indianapolis, Ind. The second meeting of the Federation of Analytical Chemistry and Spectroscopy Societies (FACSS) boasts a technical program of 4V2 days comprised of three plenary lectures, 47 sessions, and 282 scientific papers. FACSS was organized some time ago to foster multidisciplinary interchanges among the members of various organizations interested in analytical chemistry and spectroscopy. The sponsoring groups are the American Microchemical Society; Analysis Instrumentation Div., Instrument Society of America; Assoc, of Analytical Chemists (Anachem); Div. of Analytical Chemistry, American Chemical Society; Eastern Analytical Symposium; Chicago Section, Society for Applied
Spectroscopy (Mid-America Conference); and the Society for Applied Spectroscopy. The technical program features plenary lectures by Justus Kirchner, Anachem Award winner David F. Boltz, and Benedetti-Pichler Award winner Petr Zuman. I n addition to sessions in the usual areas of chromatography, spectroscopy, and electrochemistry, there are special sessions dealing with pharmaceutical analysis, analytical instrumentation, chemometrics, food and drug analysis, trace characterization and analysis, Fourier transform, biological probe, process chromatography, ligand assays and other radiometric techniques, S E M and electron probe applications, computerized data
analysis, air/water, polymer characterizations, process emission monitoring, and spectroscopy and the automobile. Of special interest are the two symposia mentioned above in process control, a field in need of interaction among various disciplines. An instrument exposition will be held Tuesday through Thursday from 10 a.m. to 6 p.m. Further information concerning the exhibits may be obtained from Edward Ruffing, J & R Assoc, 125 Westview Rd., Upper Montclair, N.J. 07043. Continuing Education. Three FACSS workshops will be held i n conjunction with the meeting. They are: liquid chromatography, Oct. 8, 10-12 a.m. and 1-5 p.m. (M. T. Jackson);
Justus G. Kirchner, Plenary Lecturer, is a senior scientist for Coca-Cola. His contributions to the development of thinlayer chromatography are many and include the introduction of standards in TLC, quantitation, thick layers, fluorescent thin layers, two-dimensional chromatography, equipment for coating of thin layers, larger plates, reactive locating agents, and the use of thin layers to select solvents for column chromatography
David F. Boltz, Anachem Award winner, is professor of chemistry at Wayne University and science advisor for the Detroit District of the Food and Drug Administration. He has many publications to his credit and has directed the graduate research of 24 PhD and 40 MS candidates. Dr. Boltz's research interests include heteropoly chemistry, spectrophotometry, atomic absorption spectrometry, liquid chromatography, and analytical separation methods
Petr Zuman, winner of the Benedetti-Pichler Award, is professor of chemistry at Clarkson College of Technology. Dr. Zuman was educated in Prague and was associated for many years with the J. Heyrovsky Institute of Polarography of the Czechoslovak Academy of Sciences. Dr. Zuman's research interests are in the field of organic polarography, organic electrode processes, and analytical applications in these areas
ANALYTICAL CHEMISTRY, VOL. 47, NO. 11, SEPTEMBER 1975 · 905 A
Ira J. Holcomb
Jerry W. Wallace
X-ray fluorescence spectroscopy, Oct. 7, evening (Isidore Adler, H . J. Rose, Jr.); and automated data analysis, Oct. 7, morning. These workshops cost $10 each and require preregistration. The American Chemical Society is holding short courses in Indianapolis before and after the FACSS meeting. These courses are listed in ANALYTI CAL C H E M I S T R Y this month, ρ 960 A. I n addition, the Society for Applied Spectroscopy is holding a course on modern emission spectroscopy, Oct. 5—6, with R. M . Barnes as instructor. Persons wishing to register for this course should contact Claude Veillon, Biophysics Research Laboratory, Har vard Medical School, Peter B. Brigham Hospital, Boston, Mass. 02115. Employment. A n employment bu reau will be i n operation at the Con vention-Exposition Center from 9 a.m. to 4 p.m., Monday through Thursday. Employers and job candidates should contact Gary V. Kaiser, Lilly Research Laboratories, P.O. Box 618, Indianap olis, Ind. 46206. Special Events. Interesting activi ties have been scheduled throughout the week. I n addition to the confer ence mixer on Wednesday evening, Oct. 8, and a dinner theater evening, Oct. 9, there will be tours of Eli Lilly and Co.; Detroit Diesel-Allison Div. GMC Powerama; Nashville, Ind., I n dianapolis Museum of Art; Motor Speedway; Conner Prairie Pioneer Settlement; and Museum of Indian Heritage. Registration and Housing. The deadline for preregistration is Sept. 15. Fees are: preregistration, $15; reg ular, $20; one day, $10; student and exhibit only, $1.00. Information and forms for both housing and registra tion are available from Jean E. Stoeckly, MC 20610, Cummins Engine Co., Columbus, Ind. 47201. 812-3795043 The complete technical program and list of exhibitors and their prod ucts are given in the following pages of ANALYTICAL CHEMISTRY.
Roby Hott
Richard B. Luers
1975 FACSS Meeting Officers Cochairmen: Ira J. Holcomb, ParkeDavis & Co.; Jerry W. Wallace, E l i Lilly & Co. Budget-Treasurer: Edwin R. Shepard, Eli Lilly & Co. Secretary: Rafik H. Bishara, Eli Lilly &Co. Arrangements: Roby Hott, U.S. Naval Avionics Continuing Education: Claude Wil son, Indiana-Purdue Universities at Indianapolis Employment: Gary V. Kaiser, E l i Lilly & Co. Exhibit Manager: Edward B. Ruff ing, J & R Associates Housing: Roby Hott, U.S. Naval Av ionics Legal: James L. Rowe, E l i Lilly & Co. Message Center: Paul Quinney, But ler University Printing: Edgar W. Day, Jr., E l i Lilly &Co. Program Cochairman: Richard B. Luers, Parke-Davis & Co. Publicity: Jean E. Stoeckly, Cum mins Engine Co. Registration: Paul Quinney, Butler University Special Events: Kay Koch, Eli Lilly &Co. Student Awards: Roger E. Schirmer, Eli Lilly & Co. Monday Morning, October 6
Pharmaceutical Analysis I Chairman: R. E. Schirmer, Eli Lilly and Co.
9:00 Simultaneous Semiautomatic Analysis of Pyrrobutamine Phos phate, Cyclopentamine Hydrochlo ride, and Metapyrilene Hydrochlo ride in Pharmaceutical Mixtures. J. L . Hale, Eli Lilly & Co. 9:20 Fast and Accurate Vitamin C Analysis Using ABA-100 Discrete Analyzer. J. G. Theivagt, K. J. Houser, Abbott Labs 9:40 Automated, Stepping Differ
906 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 11, SEPTEMBER
1975
Jean E. Stoeckly
ential Calorimeter for Analysis of Purity. J. Zynger, E l i Lilly & Co. 10:20 Detection of "Amphet amine-Like" Compounds from I l licit and Pharmaceutical Prepara tions by Thin-Layer and Gas Chro matography Via Derivatization •with JV-Succinimidyl p-Nitrophenylacetate (SNPA). L . S. Eichmeier, M . E. Caplis, Northwest Indiana Criminal Toxicology Lab 10:40 Electrochemical Methods of Analysis of Cefamandole Nafate. E. C. Rickard, G. G. Cooke, E l i Lilly & Co. 11:00 Chemical Degradation of Pharmaceuticals. A. Dinner, Eli Lilly & Co. 11:20 Thin-Layer and Gas Chro matographic Screening Programs for New Drug Substances. R. W. Souter, R. H . Bishara, Eli Lilly & Co. Symposium on X-ray Spectrometry I Chairman: D. E. Leyden, U of Georgia
9:00 Wavelength Dispersion X-ray Fluorescence Analysis. J. V. Gilfrich, Naval Research Lab 9:20 Energy-Dispersive X-ray Fluorescence: Pros and Cons. J. A. Cooper, Ortec, Inc. 9:40 Comparative Evaluation of Wavelength-Dispersive and E n ergy-Dispersive X-ray Spectrometric Analysis. R. L . Myklebust, NBS 10:20 Standard Reference Sam ples for Trace Multielement Analy sis. J. R. Rhodes, Columbia Scientific Instruments 10:40 Use of Ion Beams in X-ray Analysis. T. A. Cahill, U of California 11:00 Trace Element Studies in Bioenvironmental Samples Using 3-MeV Proton-Induced X-ray Emission Analysis. R. L . Walter, DukeU 11:20 X-ray Fluorescence M u l tispectrometer System for Rapid Elemental Analysis of Particulate Air Pollutants. J. Wagman, R. L . Bennett, Κ . Τ. Knapp, EPA, Research Triangle Park
11:40 Aerosol Analysis w i t h D i chotomous Sampler and EnergyDispersive X - r a y Fluorescence. A. R. Stiles, N o r t h r u p Services Inc.; T. G. Dzubay, EPA, Research Triangle Park
NMR Spectroscopy I Chairman:
J. W. Moyer, Desoto, Inc.
9:00 Methods of Peak Assignment in 1 3 C N M R Employing Decoupling. J. B . Grutzner, Purdue U 9:30 N a t u r a l Abundance 1 3 C N M R Studies of Proteins. R. S. Norton, D. Wilber, A. Alerhand, Indiana U 10:30 Application of 1 3 C Magnetic Resonance to the Study of Chlorophyll a Oligomers. T . R. Janson, H . Sheer, J. J. Katz, Argonne National Lab; G. J. Ray, Standard Oil of Indiana 11:00 Modes of Bond-Opening and Alternating Copolymerizations of Butadiene and 1,2-Dicarbomethoxyethylenes. G. A. Lindsay, H . J. Harwood, U of A k r o n 11:30 Determination of Monomer Sequence Distribution of Acrylonit r i l e - M e1t3h y l m e t h a c r y l a t e Copolymers by C N M R . T . Gerken, W. M . Ritchey, Case Western Reserve U 12:00 Sequence and Tacticity of A N / M M A13Copolymers as Determined by C N M R . J. R. Mooney, J. A. Young, Standard O i l Co. of Ohio
Analytical Instrumentation I Chairman:
J. A. Williamson, Du Pont
9:00 Considerations in Adaptation of Kinetic Methods to M i n a t u r e Centrifugal Fast Analyzer. S. Brunk, J. P. Avery, H . V. Malmstadt, U of Illinois 9:20 Multichannel Pipet for P a r allel Aliquoting and Delivery of Solutions into M i n i a t u r e Centrifugal Analyzer Discs. R. P. Gregory I V , J. D . Lowry, H . V. Malmstadt, U of I l l i nois 9:40 Computer-Controlled M u l t i channel Recording U V / V i s i b l e Absorption Spectrophotometer. J. P. Avery, H . V . Malmstadt, U of Illinois 10:20 H i e r a r c h i a l Computer System for Automated Stopped-Flow Studies. G. E. Mieling, R. W. Taylor, H . L . Pardue, Purdue U 10:40 Bipolar Pulse Conductance Detection for Stopped-Flow K i n e t ics. F. J. Holler, S. R. Crouch, C. G. Enke, Michigan State U 11:00 Simple, High-Speed Pulse Detector for Photon Counting. J. Hornshuh, C. G. Enke, Michigan State U ; B . K . Hahn, D u Pont 11:20 Electronic Circuit Considerations for Solid-State Diode A r r a y Analytical Spectrometer. D. Lovse, H . V . Malmstadt, U of Illinois 11:40 D u a l Wavelength Spectrom e t r y Measurements w i t h Split Beam Ratiometric System. J. D. Defreese, H . V. Malmstadt, U of Illinois
Spectrophotometry: General
Monday Afternoon
Chairman:
Pharmaceutical Analysis II
W. D. Shults, ORNL
9:00 Precision and Accuracy in D u a l Wavelength Spectrophotometric Measurement. K . L . Ratzlaff, D.F.S. Natusch, U of Illinois 9:20 Adherence to Beer's L a w of Tin-Catechol V i o l e t - C e t y l t r i m e t h ylammonium Bromide Complex and Its Applications. O. Menis, S. A. Wicks, R. K . Bell, A. J. Fatiadi, N B S 9:40 Spectrophotometric Method for Determination of Arsenic. G. Kellen, Krafco R N D ; B . Jaselskis, Loyola U 10:20 Rapid Spectrophotometric Method for Determination of Ascorbic Acid i n U r i n e . B. Jaselskis, J. Hseih, Loyola U 10:40 C r i t i c a l Comparison of Endpoint Detection Techniques in Computer-Controlled Spectrophotometric Titrations. S. R. Goode, J. Matthews, U of South Carolina 11:00 Difficult Problems in Reflectance Spectroscopic Measurements. J. V. Park, Beckman Instruments 11:20 Synthesis and Study of N e w Tetraarylborate Reagents Containing Nitrogen in a Heterocyclic A r omatic Ring. S. S. Chao, C. E. Moore, Loyola U
Chairman:
(Determination of Sulfur). G. M . Maciak, P. W. Landis, G. L . Kirschner, E l i L i l l y & Co.
Symposium on X-ray Spectrometry II Chairman: J. R. Rhodes, Columbia Scientific Instruments
2:00 European Trends in X - r a y Analysis of Pollutants. H . DeVries, N . V. Philip's Glocilampenfabriekum, The Netherlands 2:40 Preconcentration Methods Prior to X - r a y Fluorescence Determination. D. E. Leyden, U of Georgia 3:20 T r a c e Level Water Analysis by Energy-Dispersive X - r a y Fluorescence. D. T . Carlton, Magnavox Co.; J. C. Russ, E D A X International, Inc. 3:40 Application of X R F Techniques to Environmental Water Samples. T . M . Spittler, G. F. Martins, EPA, Needham Heights 4:00 Determination of Trace M e t als in Combustible Fraction of U r b a n Refuse—Advantages and Limitations of X - r a y Spectroscopy. W. J. Campbell, H . E. Marr, I I I , D . L . Neylan, S. L . Law, Bureau of Mines 4:20 Intercomparison of Trace E l ement Determinations in Simulated and Real A i r Particulate Samples. D. C. Camp, A. L . VanLehn, U of California; J. R. Rhodes, A. H Pradzynski, Columbia Scientific Instruments 4:40 Trace Phase Analysis w i t h Powder Diffractometer, EnergyDispersion Spectrometer Combination. R. Jenkins, Philips Electronic Instruments, Inc.
R. E. Schirmer, Eli Lilly & Co.
2:00 Quantitative T h i n - L a y e r Chromatographic Method for Determination of Serotonin and Its Derivatives in Biological Samples. N . Narasimhachari, R.-L. L i n , Galesburg State Research Hospital 2:20 Separation and Quantitation of V i t a m i n B12 in Various Types of Samples by Reverse Phase H i g h Resolution Liquid Chromatography. C. Y. W u , J. J. W i t t i c k , Merck & Co. Inc. 2:40 Application of Liquid Chromatography w i t h Electrochemical Detection ( L C E C ) to Pharmaceutical Analysis. R. M . Riggin, R. E. Shoup, P. T . Kissinger, Purdue U 3:20 Determination of Dihydroquinidine in Quinidine by H i g h Speed Liquid Chromatography. R. G. Achari, E. E. Theimer, Cooper Labs 3:40 H P L C Analysis of Vitamins. I I : Quantitation of V i t a m i n D and V i t a m i n A in Oils, D r y Concentrates, and M u l t i v i t a m i n Formulations. K . A. Tartivita, J. P. Sciarello, B . C. Rudy, Hoffmann-LaRoche Inc. 4:00 Computerized Technique in Organic Microelemental Analyses
908 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 1 1 , SEPTEMBER
1975
NMR Spectroscopy II Chairman:
J. W. Moyer, Desoto, Inc.
2:00 Carbon Magnetic Resonance of JV-Carboxyl Anhydrides and O l i gomers Derived from Them. S. P. Sawan, H . J. Harwood, U of Akron 2:30 Comparison and I n t e r p r e t a tion of 1 3 C Chemical Shifts in A l k enylidenecyclopropanes, Aliènes, and Methylenecyclopropanes. D. J. Pasto, J. K . Borchardt, U of Notre Dame 3:20 Synthesis, Properties, and Carbon-13 N M R Spectra of T e traarylborates. F. Jarzembowski, C. E. Moore, D. Netzel, Loyola U 3:40 lH and 1 3 C N M R of Small Samples: One-Microgram Ή and O n e - M i l l i g r a m 1 3 C N M R Studies. T. C. Farrar, Jeol 4:00 Trace Analysis of Organophosphorus Compounds Using 3 1 P F T N M R . T . Gurley, W . M . Ritchey, Case Western Reserve U 4:20 Quantitative Determination of Phosphorous Containing Pesti cide Mixtures by 3 1 P N M R . L. A.
Wilson, Varian Associates; R. Greenhalgh, Canadian Department of Agri culture 4:40 Computer-Controlled, Se quential Sample N M R D a t a Acqui sition and Control System. G. L. Kirschner, P. W. Landis, J. B. Deeter, Eli L i l l y & Co.
J. A. King, Κ . Η . Pearson, Cleveland State U 4:40 Understanding Surface Area Measurements. M . A. Kaiser, R. L . Grob, Villanova U ; M . J. O'Brien, Merck Sharpe & Dohme
Emission Spectroscopy I Chemometrics in Analytical Chemistry Chairman:
B. R. Kowalski, U of Washington
2:00 Introductory Remarks. B. R. Kowalski 2:10 Quantitative Measures of Chemical Similarity and T h e i r A p plication in Analytical Chemistry. S. Wold, Umea U , Sweden 2:40 Optimization i n Analytical Chemistry. S. N . Deming, U of Hous ton 3:30 Fourier Transform and Cor relation Methods for Measurement and Analysis of Chemical Data. G. Horlick, K . R. Betty, U of Alberta 4:00 Analysis of iV-Dimensional D a t a Structures. D. L . Duewar, B. R. Kowalski, U of Washington
Analytical Symposium: General Chairman:
R. B. Luers, Parke, Davis & Co.
2:00 Interpretation of Mass Spec t r u m of Ornithine-Containing Lipid. M . L . Gross, D . R. Hilker, H . W. Knoche, J. M . Shively, U of Ne braska 2:20 Determination of Constitu ents of M a r i j u a n a from Different Origins by High-Resolution Gas Chromatography-Mass Spectrome try. M . Novotny, M . L . Lee, C. E. Low, A. Raymond, Indiana U 2:40 Determination of Grafted Chain Lengths and Frequency of Grafting in Grafted Poly (butadi ene) Rubbers. P. Shapras, G. C. Claver, Monsanto Co. 3:20 Rapid Determination of CaO in Magnesia and Chrome Ore Con taining Refractory Materials by E D T A . S. Banerjee, J. B . Vizzini, General Refractories Co. 3:40 Practical Application of T a n nabe-Sugano Theory to Maximize E S R Signal Intensity of M e t a l I o n Complexes. D . C. Warren, Houston Baptist U ; J. M . Fitzgerald, U of Houston 4:00 Multitechnique Study of I n teraction of A l Layers w i t h Polycrystalline Si. R. J. Blattner, C. A. Evans, Jr., U of Illinois; K . Nakamura, Nippon Electric Co., L t d . , Japan; M . - A . Nicolet, J. W. Mayer, California Institute of Technology 4:20 Spectropolarimetric Back T i t r i m e t r y Methods for D e t e r m i nation of M i l l i g r a m Amounts of Rhodium ( I I I ) and Platinum ( I V ) .
Chairman:
J. P. Walters, U of Wisconsin
2:00 Interchangeable Apparatus for Research i n Optical Emission Spectroscopy. J. P. Walters, U of Wisconsin 2:20 Interactive, Computer-As sisted Method for Determination of Wavelength in Optical Emission Spectroscopy. J. S. Beaty, GlobeUnion, Inc.; J. P. Walters, U of Wis consin 2:40 N e w Look at Traditional Ap proach to Spectroscopic D a t a Ac quisition and Interpretation Using Abel Inversion. A. Scheeline, J. P. Walters, U of Wisconsin 3:20 Electronic Control and A p plication of Adjustable Waveform Spark Source. D. M . Coleman, J. P. Walters, U of Wisconsin 3:40 Design and Application of 323 M H z Quarter-Wave Spark Source for Production of Positionally Sta ble Discharges at H i g h Repetition Rate. J. Rentner, J. P. Walters, U of Wisconsin; T . Uchida, Osaka U , Japan 4:00 Design and Performance of Mechanically Time-Gated, Radial ly Resolved Spectrometers for Re search on Repetitive Spark Dis charges. R. J. Klueppel, J. P. Wal ters, U of Wisconsin; W. S. Eaton, North-American Rockwell Science Center; S. A. Goldstein, Sandia Labs; R. D. Sacks, U of Michigan 4:20 Time-Gated Schlieren Study of Stabilized Spark Discharge. R. L . Waiters, Jr., J. P. Walters, U of Wis consin; J. W. Hosch, Oregon State U
10:40 Photomicrographs of T h i n Layer Chromatographic Adsor bents. P. F. L o t t , U of Missouri 11:00 Two-Dimensional Charac terization of Amino Acids in A c t i nomycin Hydrolysates. F. Bodansky, Hoffmann-LaRoche 11:20 Photographic Documenta tion in the Research Laboratory. D. E. Heinz, R. K . Vitek, Camag, Inc. 11:40 Theoretical Correlation of Solute Solubility and Adsorbability ( T L C ) . V. S. Marino, FDA; G. H . Schenk, Wayne State U
Recent Developments in Food and Drug Analysis Chairman: District
S. M. Walters, FDA, Detroit
10:20 Microwave Induced Plasma Coupled to a H a r r i c k Detector for Simultaneous Multielement Trace Analysis—Carbon Cup Sample I n troduction. F. L . Fricke, O. Rose, Jr., J. A. Caruso, U of Cincinnati 10:40 Investigation of Feasibility of Low-Temperature Ashing of Foodstuffs Prior to Heavy Metals Determination. L . E. Habeger, F D A 11:00 Luminescence Characteris tics of Aflatoxins. A. Gillespie, FDA; G. H . Schenk, Wayne State U 11:20 Determination of Saccharin in Food Products by U V Spectros copy. M . M . Hussein, H . Jacin, F. Ro driguez, Life Savers, Inc. 11:40 Thin-Layer Chromatogra phy as a Rapid and Inexpensive Screening Test for Determining Adulterants in Capsicum Extracts and Related Products. M . Bensinger, Alcolac, Inc.; A. Allen, P. Todd, Jr., Kalamazoo Spice Extraction Co.
Emission Spectroscopy II Tuesday Morning, October 7
Thin-Layer Chromatography Symposium I Chairman:
9:00
R. K. Vitek, Camag, Inc.
Introductory Remarks. R. K.
Vitek 9:15 Plenary Lecture. Modern Techniques in T L C . J. Kirchner, Coca-Cola Co. 10:20 Reverse Phase T h i n - L a y e r Chromatographic Separation of Bromodiphenhydramine and D i phenhydramine. S. A. Fusari, M . Terhalle, I . J. Holcomb, E. C. Alix, Parke, Davis & Co. 10:30 T h i n - L a y e r Chromatogra phy—A Neglected Chromato graphic Method? P. F. L o t t , U of Missouri
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1975
Chairman: Lab
E. S. Peck, Lawrence Livermore
10:20 Inductively Coupled Plasma—The Answer to M a n y U n solved Spectrochemical Problems. P. D. Dalager, A. L . Davison, R. M . Ajhar, Applied Research Labs 10:40 Theoretical and Experimen tal Study of Temperature, Velocity, and Particle Decomposition in I C P Spectrochemical Source. R. G. Schleicher, R. M . Barnes, U of Massa chusetts 11:00 Simultaneous Multielement Analysis of Biological Fluids and Tissues: R F Inductively Coupled Plasma-Optical Emission Spec trometry. R. L . Dahlquist, J. W. Knoll, Applied Research Labs; A. A. Wilcox, R. S. Chen, Santa Barbara Cottage Hospital; R. D. Irons, U of Rochester
11:20 U l t r a t r a c e Determinations by Optical Emission Spectroscopy: Stray Light Problem. G. F. Larson, V. A. Fassel, R. K . Winge, R. N . K n i seley, Iowa State U 11:40 Diagnostics of 144-MHz Plasmas. P. E. Walters, T . L . Chester, J. D . Winefordner, U of Florida
of Aminochromes. M . D . Morris, U of Michigan 12:00 Optimal Least-Squares Smoothing of Spectroscopic Data. J. Deltour, Y. Termonia, Faculty of Agromony, Belgium 12:20 Evaluation of Least-Squares Smoothing for Digitally Recorded Spectra. T. A. Nieman, U of Illinois; C. G. Enke, Michigan State U
Symposium on Trace Characterization and Analysis I
Tuesday Afternoon
Chairman: R. K. Skogerboe, Colorado State U
Thin-Layer Chromatography Symposium II
10:20 Current Status of Flame Spectrophotometric Methods for Trace Analysis. S. R. Koirtyohann, F. E. Lichte, U of Missouri 10:50 Trace and U l t r a t r a c e Char acterization by Optical Emission Spectroscopy. V. A. Fassel, Iowa State U 11:20 Activation Analysis: Cur rent Status and Prospects for the Future. J. R. Vogt, U of Missouri 11:50 Adventures i n Pulse V o l tametry. R. A. Osteryoung, J. G. Osteryoung, Colorado State U
Application of X-ray Diffraction in Characterization of Materials I Chairman: R. J. Fredericks, Ethicon, Inc.
10:20 Introduction to Powder Dif fraction. B . Post, Polytechnic Insti tute of New York 10:50 Crystalline Phase Identifi cation Using Powder Diffraction File. G. J. McCarthy, Penn State U 11:20 Computer Applications in Powder Diffraction. R. L . Snyder, N Y S College of Ceramics at Alfred U
Infrared and Raman Spectroscopy: General Chairwoman: Co. (Ohio)
Chairman: R. K. Vitek, Camag, Inc.
2:00 Quantitative Thin-Layer Chromatography i n Pharmaceuti cal Analysis. S. Ahuja, Ciba-Geigy Corp. 2:20 Preparation of Superior T h i n - L a y e r Chromatograms for Quantitative I n Situ Densitometric Scanning Analysis. P. E. Flinn, F D A 2:40 Chemical Methodological As pects of I n Situ Quantitative E v a l uation of Thin-Layer Chromato grams. L . R. Treiber, Case Western Reserve U 3:20 Luminescence Analysis of Anti-inflammatory Agents in Blood or Plasma Following T h i n - L a y e r Chromatographic Separation. J. A. deSilva, N . Strojny, Hoffmann-LaRoche Inc. 3:40 Assay of Pharmaceuticals Using Quantitative T L C Elution Techniques. S. A. Fusari, I . J. H o l comb, R. B . Luers, Parke, Davis & Co. 4:00 T h i n - L a y e r Chromatograph ic Separation and Fluorometric Determination of 4-Aminobiphenyl in 2-Aminobiphenyl. I . J. Jakovljevic, J. Zynger, R. H . Bishara, E l i L i l l y & Co. 4:20 "Requisites for High-Preci sion I n Situ Quantitative T L C . G. E. Lightner, Lightner Instrument Co. 7:30 Tuesday Evening. Round Table Discussion on T L C . Cochairmen: R. K . Vitek, Camag, Inc.; J. K i r chner, Coca-Cola Co.
usch, Colorado State U ; T . M . Thorpe,
Miami U
4:20 Characterization V i a Atomic and Molecular Luminescence Spec trometry. J. D . Winefordner, U of Florida 4:50 Trace Analysis by Electron Spectroscopy. J. C. Carver, U of Georgia
Emission Spectroscopy III Chairman: E. Dunlop, Du Pont
2:00 Determination of Antimony, Barium, Lead, and Arsenic i n Sam ples of Interest to the Forensic Sci entist Using Argon Plasma Emis sion Spectrometry. R. W. Parian, E. T. Solomons, Georgia Crime Lab; C. P. Rutherford, Consultant 2:20 Recent Developments in Emission Spectrometry w i t h D C Plasma Arc. W. E. Rippetoe, T . J. Vickers, C. D . Keirs, Florida State U 2:40 Computerized Calculations of Quantitative Emission Spectregraphic Analysis Results. S. Lerman, Ε. Η . Eck, Con Edison 3:20 Computer-Controlled System for Plasma-Optical Emission Spec trometry. T . Karlinski, D . Missio, Spectrametrics, Inc. 3:40 Minicomputer-Based Emis sion Spectrographic Analysis Sys tem. C. P. Thomas, U.S. Geological Survey 4:00 Glow Discharge Optical Spectroscopy: Technique for M i crovolume Elemental Analysis and Depth Profiling. F. Sequeda-Osorio, J. E. Greene, U of Illinois 4:20 Optical Emission Analyses w i t h Spectrometer Designed for Automatic Background Correction. R. K . Skogerboe, G. N . Coleman, P. J. Lamothe, S. J. Freeland, F. T . Varcoe, Colorado State U 4:40 Applications of Plasma Emis sion-Echelle Spectrometer System to T r a c e Analysis of Solutions. R. K . Skogerboe, I . T . Urasa, Colorado State U
J. G. Grasselli, Standard Oil
10:20 Computer-Spectrometer I n teractive System for Raman and I n f r a r e d Spectroscopy. W . F. Edgell, E. Schmidlin, T . J. Kuriakose, Purdue U 10:40 I n f r a r e d Microsampling Re visited. R. J. Obremski, H . J. Sloane, Beckman Instruments, Inc. 11:00 I n f r a r e d Spectroscopy Study of Interaction of Silanes w i t h Antimony Oxide. G. A. Pasteur, H . Schonhorn, Bell Labs 11:20 T r i p l e - and Multiple-Beam Spectroscopy. T . B . Hirschfeld, Block Engineering, Inc. 11:40 Catecholamine Determina tion by Resonance Raman Spectra
Symposium on Trace Characterization and Analysis II Chairman: V. A. Fassel, Iowa State U
2:00 X - r a y Fluorescence Analysis and Microanalysis. C. O. Ruud, U of Denver 2:30 Advances i n I o n Beam Tech niques for Materials Characteriza tion. C. A. Evans, Jr., U of Illinois 3:20 Advances i n Inorganic Mass Spectrometry. R. K . Skogerboe, Col orado State U 3:50 Gas Evolution Analysis: A Potentially Powerful Tool for T r a c e M e t a l Speciation. D.F.S. Nat-
912 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 1 1 , SEPTEMBER 1975
Fourier Transform Spectroscopy Group Symposium on Applications of Fourier Transform Infrared Spectroscopy or Why FT-IR? Chairman: W. G. Fateley, Kansas State U
2:00 Advances in Polymer Analy sis Made Possible by F T - I R . H . T . White, J. J. Elliott, Exxon 2:30 Applications of F T - I R at the Upjohn Co. W. C. Krueger, P. A. Mealman, L . M . Pschigoda, B . L . Story, Upjohn Co. 3:20 National Technical Prob lems—Interferometry and F T S to
the Rescue. J. R. Ferraro, Argonne National Labs 3:50 Recent Advances in State of Analytical G C - I R Techniques. J. N . Willis, Spectrotherm Corp. 4:20 Getting the Most Out of the Least ( F T - I R for Surface Studies). R. Jakobsen, Battelle-Columbus Labs 4:50 Optimizing Sensitivity of Fourier Multiplex Spectrometers Through Variable Scan Velocity. D. Mattson, R. E. Gillespie, K . R. L i n delin, Eocom Corp.
11:00 Electrochemical Determi nation of Serum Cholesterol. C. Olson, Ohio State U 11:20 Bioelectrodes for Measure ment of Cerebral Metabolism and Blood Flow. V. D . Desmukh, Baylor Coll of Medicine 11:40 Evaluation of Automated Coulometric Back-Titration A n a l ysis of Bicarbonate. S. J. Meier, R. Stockmar, Bronson Methodist Hospi tal
Process Chromatography Application of X-Ray Diffraction in Characterization of Materials II Chairman:
R. J. Fredericks, Ethicon, Inc.
2:00 W h a t Can X - r a y Diffraction T e l l Us About Metals and Alloys? S. Weissman, Rutgers U 2:30 Polymer Characterization Using X - r a y Diffraction. R. J. Fred ericks, Ethicon, Inc. 3:30 Some Important Applications of X - r a y Powder Diffraction in Mineralogy and Ceramics. D . K . Smith, Penn State U
Chairman:
J. W. Lee, Bendix Corp.
10:20 Basic Theory of Process Chromatography. J. Clemons, Vir ginia Polytechnic Institute and State U 10:50 Justification, Consider ations, and Purchase of Process Chromatograph. A. Foundos, Birchall Assoc. 11:20 Design Criteria for Process Liquid Chromatograph. J. A. W i l liamson, D u Pont 11:50 Totally Pneumatic Gas Chromatographic Process Stream Analyzer. R. Annino, Canisius Coll; J. Curren, Jr., R. Kalinowski, E. Karas, R. Lindquist, R. Prescott, Foxboro Co.
Wednesday Morning, October 8
Anachem Award Symposium I Chairman: Corp.
J. Cramer, BASF Wyandotte
9:00 Presentation of Anachem Award to D. F. Boltz, Wayne State U 9:05 Award Address: Quest for Sen sitivity, Specificity, and Speed in Chemical Analysis. D . F. Boltz 10:20 Industrial Applications of Selective Ion Electrodes. R. Danchik, Alcoa Labs 10:50 Applications of Staircase Voltametry to Trace M e t a l Analy sis. J. Jasinski, FDA; D. Rubin, R. Schroeder, Wayne State U 11:20 Polarographic Determina tion of Erythromycin by Tensammetric Peak-Height Analysis. Ο. Κ . McFarland, Xerox Corp. 11:45 Indirect Voltametric Deter mination of Silicon Utilizing M o lybdoheteropoly Chemistry. A. Bazzi, D. F. Boltz, Wayne State U 12:00 Anachem Award Luncheon, Room 123. Speaker: M . G. Mellon, Purdue U
Analytical Applications of Vidicon Tube in Spectrometry Chairman: A. Davis, Hooker Chemicals and Plastics Corp.
10:20 Real Time Analytical Spec trometry. J. M . Marrs, Tektronix, Inc. 10:40 Derivative Spectroscopy w i t h a Vidicon Spectrometer. T . E. Cook, H . L . Pardue, Purdue U 11:00 Development and Charac terization of Computer-Controlled Vidicon Spectrometer. T . A. Nieman, U of Illinois; C. G. Enke, M i c h i gan State U 11:20 Applications of Vidicon Spectrometer to Clinical Analysis. H . L . Pardue, D . M . Fast, A. E. McDowell, Purdue U 11:40 Applications of Electronic Detection on Laser Microprobe. T . H . Briggs, Western Electric
Chairman:
J. C. White, ORNL
10:20 Bioanalysis w i t h Membrane Electrode Probes. G. A. Rechnitz, State University of New York
10:20 Some Observations on Use of Computer-Controlled Rapid Scanning Spectrometer for M e a surement of Transient Spectral Phenomena. P. N . Keliher, Villanova U ; T . A. Doris, W. J. Puchalski, Frankfort Arsenal
914 A · ANALYTICAL CHEMISTRY, VOL.
, NO. 11, SEPTEMBER 1975
Chairwoman: D. S. McCann, Wayne County General Hospital
Atomic Absorption Spectroscopy I: Instrumentation Chairman: Coll
J. J. Hazdra, Illinois Benedictine
10:20 Adaptive Computer Optimi zation of Isolated-Droplet Flame Spectrometer. T . W . Hunter, G. M . Hieftje, Indiana U 10:40 Diffusion of Atoms from I n dividual Solute Particles Vaporiz ing in Analytical Flame: M a t r i x Ef fects. C. B. Boss, G. M . Hieftje, Indi ana U 11:00 Production and Application of Stable Helium-Oxygen-Acety lene Laminar Flame for Use in Atomic Spectrometry. K . A. Satur day, G. M . Hieftje, Indiana U 11:20 N e w Method for Continuous Source A A Using Selective Reso nance Line Modulation. R. L . Coch ran, G. M . Hieftje, Indiana U 11:40 N e w Developments in Con stant Temperature Furnace Atom ic Absorption. R. Woodriff, Montana State U 12:00 Multielement MicrowaveExcited Electrodeless Discharge Lamps for Atomic Absorption and Atomic Fluorescence Spectrome try. S. R. Goode, D. C. Otto, U of South Carolina
Wednesday Afternoon
Anachem Award Symposium II Chairman: J. A. Howell, Western Michigan U
Analytical Instrumentation II Biological Probe Symposium
10:40 "Analog Shift Register": Economical Approach to Fast Transient Recording. T . A. Last, C. G. Enke, Michigan State U 11:00 Compact Nitrogen Laser w i t h Split-Beams Measurement System for Molecular Fluorescence Analytical Methods. M . J. Simmons, J. D . Freese, H . V. Malmstadt, U of I l linois 11:20 N e w Front-Surface Optical Design for Automated, Quantita tive, Stopped-Flow Fluorometry. M . Bryant, K . O'Keefe, H . V. M a l m stadt, U of Illinois 11:40 Converting an X - Y Record er into a T r u e Incremental Plotter. F. J. Holler, T . Kelly, T . V. Atkinson, Michigan State U
2:00 Atomic Spectroscopy Using Chlorine-Hydrogen Flame. J. How ell, G. Pizarro, Western Michigan U 2:20 Direct Microblood Lead Analysis by Atomic Absorption Using Double-Beam Background Correction. F. Armore, Illinois De partment of Public Health 2:40 Multicomponent Spectropho tometry w i t h Rapid Scan Spec trometers. S. Rose, C. E. Abrams, P.
Hanavan, W. McGarvey, American Cyanamid Corp.; Ν . Ε. Rigler, Havens & Emerson, L t d . 3:20 Trends in Kinetics of LigandLigand Exchange Reactions of Ethylenediaminetetraacetato M e t a l Complexes w i t h Stereospecific Ligands. K . Pearson, J. A. Boslett, Jr., Cleveland State U 3:40 Absorption Spectrophoto m e t r y Study of Determination of Traces of Diamines. C. Meyers, D. F. Boltz, Wayne State U 4:00 Coulometric-Spectropolarimetric Analysis. R. J. Palma, Sr., R. A. Gibbs, Midwestern U 4:20 Comparison of Spectrophoto m e t r y Methods for Determination of Boron. H . K . L . Gupta, D. F. Boltz, Wayne State U
Coblentz Society Symposium: Computer-Assisted Vibrational Spectroscopy Chairman:
P. R. Griffiths, Ohio U
2:00 Design and Applications of Computerized I n f r a r e d G r a t i n g Spectrophotometer. J. Mattson, U of Miami 2:25 Automated Raman Spectros copy. J. Scherer, U S D A 2:50 High-Speed Multicomponent Analysis by Fourier Transform Spectroscopy. K . Kizer, A. Mantz, Digilab Inc. 3:30 Identifying I n f r a r e d Spectra by P a t t e r n Recognition Tech niques. T . L . Isenhour, U of N o r t h Carolina 4:00 Interferometers vs. Monochromators: Separating Analog and Digital Advantages. P. R. Griffiths, Ohio U ; H . Sloane, Beckman Instru ments Inc.; R. W . Hannah, PerkinElmer Corp., R. O. Kagel, Dow Chemi cal Corp.
Ligand Assays and Other Radiometric Techniques Chairwoman: D. S. McCann, Wayne County General Hospital
2:00 Computer Analysis, Storage, and Retrieval of Clinical Radioim munoassay Data. B . G. England, U of Michigan Medical Center 3:00 Analytical Approaches for Measuring and Characterizing Hormone Receptors. J. A. Richards, U of Michigan Medical Center 3:40 Sensitive Radiometric Assay for Plasma Catecholamines. G. A. Johnson, J. D. Peuler, Upjohn Co. 4:20 Plasma Androgen Profiles. W. Szpunar, A. J. Blair, Jr., D . S. McCann, Wayne County General Hos pital 916 A · ANALYTICAL
CHEMISTRY,
4:40 Immunoassay of C E A Using Affinity Chromatography. R. E. Curry, D. Shaw, U of Delaware 5:00 Radioimmunoassay for V i n blastine and Vincristine. M . A. Root, K . Gerzon, R. W. Dyke, L i l l y Research Labs
Applications of SEM and Electron Probe Chairman:
P. Lublin, GTE Labs
2:00 Introductory Remarks. P. L u blin 2:10 Energy-Dispersive X - r a y Analysis in Scanning Electron M i croscope. E. Lifshin, General Electric Corp. 3:20 S E M Applications to Botani cal Research. B. Panessa, St. Vincent Hospital 4:00 Role of S E M and Electron Probe i n Dental Research. J. Lenke, American Dental Assoc. 4:40 Applications of S E M to Wound Repair Materials. F. Schil ler, Ethicon, Inc.
Computerized Data Analysis Chairman: J. Zynger, Eli Lilly & Co.
2:00 Evolution of Automatic D a t a Reduction Systems for Chromatog raphy. A. T . Leung, R. A. Henry, Spectra Physics, Inc. 2:20 N e w Expandable Family of Operator-Oriented Computing I n tegrators. J. Eckelkamp, T . Ste phens, Columbia Scientific I n d . 2:40 Innovative Pattern Recogni tion Technique for Chromato graphic Signal Analysis. H . V. Jones, Jr., R. K . Wackerbarth, C. W. Horton, Sr., Columbia Scientific I n d . 3:20 Automatic D a t a Reduction Using H i e r a r c h i a l System. A. T. Leung, E. Montoya, Spectra-Physics, Inc. 3:40 Computing Integrators Offer Flexible Calculation Methods to Streamline Laboratory Proce dures. E. Montoya, G. Smith, Spec tra-Physics, Inc. 4:00 Application of P a t t e r n Rec ognition to the Interpretation of Particulate Composition D a t a from Southwestern Desert Atmosphere. P. Gaarenstroom, M . Pichler, S. P. Perone, Purdue U ; J. Moyers, U of Ar izona 4:20 Application of Computerized Pattern Recognition to Mass Spec t r a l Sequence Analysis of Oligodeoxribonucleotides. D . R. Burgard, S. P. Perone, J. L . Wiebers, Purdue U 4:40 Development of Instrument Specific Microcomputer. M . Over ton, L . L . Adler, Jr., D . E. Smith, F D A
VOL. 47, NO. 1 1 , SEPTEMBER
1975
5:00 Computer Networks Employ ing Microcomputers. L . Alber, M . Overton, D. E. Smith, F D A
Atomic Absorption Spectroscopy II: Instrumentation Chairman: J. J. Hazdra, Illinois Benedictine Coll
2:00 Application of Atomic Ab sorption Instrument Containing a Microprocessor. W. B. Barnett, Perkin-Elmer Corp. 2:20 Temporal Behavior of Line Profiles of Pulsed Sources and Cells for Atomic Spectroscopy. E. H . Piepmeier, Oregon State U ; L . de Galan, Technische Hogeschool Delft, The Netherlands 2:40 Investigation of Contained D C Arced Column for Spectrochemical Analysis. C. Evoniuk, R. Woodriff, Montana State U 3:20 Application of Image Dissec tor Multichannel Spectrometer to Multielement Atomic Absorption Spectrometry. K . M . Aldous, J. Gar den, D . G. Mitchell, New York State Department of Health 3:40 Sequential Hollow Cathodes for Multielement Analysis and Background Correction in Atomic Absorption Spectroscopy. D . A. Bath, R. Woodriff, Montana State U 4:00 Effect of Nonanalyte Light Attenuation on Accuracy i n Trace Element Analysis in Complex A l loys. J. Y. Marks, R. J. Spellman, B . Wysocki, M.E.R.L. 4:20 In-depth Study of Ionization Interferences in Flameless Atomization. M . F. Bancroft, R. G. Schleicher, S. B. Smith, Jr., J. Y. Hwang, Instrumentation Lab 4:40 Use of Covalent Hydrides in Product of Electrodeless Discharge Lamps. G. E. Bentley, M . L . Parsons, Arizona State U
Thursday Morning, October 9
Benedetti-Pichler Award Symposium Chairman:
P. N. Keliher, Villanova U
9:00 Presentation of Benedetti-Pi chler Award to Petr Zuman, Clarkson College of Technology 9:05 Benedetti-Pichler Award A d dress. Polarography and M i c r o chemistry. P. Zuman 10:20 Applications of Immobilized Enzymes on Microchemical and Clinical Analysis. P. W. Carr, L . D. Bowers, U of Georgia; L . M . Canning, Jr., Phillips Roxane Co. 11:00 U l t r a t r a c e M e t a l Analysis in Environmental and Biological Systems. T . H . Risby, Pennsylvania State U
Polymer Characterization Techniques I Chairwoman: J. Q. Grasselli, Standard Oil Co. (Ohio)
10:20 Characterization of Poly mer Crazing Processes by Laser Diffraction. C. C. Hsiao, U of Minne sota 10:50 Relaxation Spectroscopy of Glassy Polymers. T . F. Schatzki, Western Regional Research Lab 11:20 Structure Analysis of Crys talline Polymers by Electron Dif fraction. W. J. Claffey, P. H . Geil, CWRU
Air-Water Pollution Analysis Chairman:
J. J. Gilfrich, Naval Research Lab
10:20 Optical Emission Analyses of Water and Wastes w i t h Demoun table Hollow Cathode Source. J. D. Johnson, Spectrogram Corp. 10:40 1000 O i l Spills, A Bench Chemist's Experience i n EPA's O i l and Hazardous Materials Program. J. W. Barron, EPA, Annapolis 11:00 High-Pressure Liquid Chro matographic Separation and Spec t r a l Identification of Aromatic Components of Fuel Oils and E n v i ronmental Samples. J. V. Hunter, J. Sabatino, Rutgers—The State U 11:20 Determination of T o t a l O r ganic Carbon in N a t u r a l Waters by Plasma Emission Spectrometry. E. Canelli, K . M . Aldous, D . G. Mitchell, New York State Department of Health 11:40 Determination of N i t r a t e at Parts Per Billion Level via Enzyme Catalyzed Reaction. L . N . K l a t t , O R N L ; D . R. Senn, P. W. Carr, U of Georgia 12:00 Determination of Trace M e t a l Concentrations in Environ mental Samples Using D C Argon Plasma. M . D . Sands, Raytheon Co.; W. G. Cox, Naval Underwater Sys tems Center
Atomic Absorption Spectroscopy III: Applications Chairman: Co.
P. Wolcott, C. C. Pfeiffer, B r a i n Bio Center 11:20 Determination of Refracto r y Elements Ba, M o , N i , Si, Sn, T i , and V i n Real World Samples by N e w High-Temperature Flameless Atomizer. J. J. Sotera, M . F. Ban croft, J. Y. Hwang, Instrumentation Laboratory Inc. 11:40 Determination of Silicon in Glasses and Minerals by Atomic Absorption Spectroscopy. R. A. Burdo, W. M . Wise, Corning Glass Works
Liquid Chromatography: General Chairman: Inc.
M. T. Jackson,
Spectra-Physics,
10:20 Quantitative Liquid Chro matographic Analysis at Nanogram Levels Using U V and Fluorescence Detection. M . T. Jackson, V. M . Smith, R. A. Henry, Spectra-Physics, Inc. 10:40 Trace Analysis of N a t u r a l Products by Liquid Chromatogra phy w i t h Electrochemical Detec tion. L . J. Felice, R. M . Riggin, P. Zoutendam, P. T . Kissinger, Purdue U 11:00 Positive Identification of Liquid Chromatographic Peaks Utilizing M u l t i p l e Wavelength De tection Techniques. R. W. Yost, W. M . MacLean, J. J. Stoveken, PerkinElmer 11:20 I o n Chromatography— Principles. H . Small, Dow Chemical Co. 11:40 Ion Chromatography Appli cations. T . S. Stevens, Dow Chemical Co. 12:00 Separation and Identifica tion of F a t t y Acid Esters of Su crose. S. E. Swanson, R. F. Broman, M . L . Gross, U of Nebraska 12:20 High-Speed Liquid Exclu sion Chromatography. Κ . Ε. Alden, Jr., R. L . Limpert, W. A. Dark, Waters Assoc. 12:40 Evaluation of Sampling Valves for High-Speed Liquid Chromatography. C. E. Stevenson, L . J. Lorenz, E l i L i l l y & Co.
Thursday Afternoon
Polymer Characterization Techniques II Chairwoman: J. G. Grasselli, Standard Oil Co. (Ohio)
2:00 Electron Microscopy and Rheology of N a t u r a l Rubber: A Combined Study. R. W. Smith, V. F. Folt, B. F. Goodrich Co. 2:30 Mass Spectrometry Analysis of Epoxy Resins. C. J. Wolf, M . A. Grayson, D. L . Fantor, R. L . Levy, McDonnel Douglas 3:20 Spectroscopic Characteriza tion of Nylon 6 and Poly(ethylene terephthalate) Fibers. J. P. Sibilia, Allied Chemical Corp. 3:40 Use of Nuclear Magnetic Resonance to Characterize N i t r i l e Containing Polymers. J. R. Mooney, Standard O i l Co. (Ohio) 4:20 Applications of Gel Perme ation Chromatography to Polymer Analysis: High-Speed G P C . D . Har mon, B . F. Goodrich Co.
Electroanalytical Symposium I Chairman:
Gas Chromatography
J. C. Guillaumln, Detroit Edison
10:20 Effects of Blood Collection Devices on Trace M e t a l Analysis. M . L . Franklin, Hoffman-LaRoche; E. E. Pickett, U of Missouri 10:40 Determination of T r a c e Metals in Foods by Graphite F u r nace Atomic Absorption Spectros copy. D . C. Manning, Perkin-Elmer Corp. 11:00 Determination of Zinc i n Fingernails by Nonflame Atomic Absorption Spectroscopy. A. Sohler,
Solid Chromatography. R. L . Grob, M . A. Kaiser, Villanova U ; M . J. O'Brien, Merck Sharpe & Dohme 11:20 Use of High-Temperature Nematic Liquid Crystal for GasLiquid Chromatography Separa tions of Steroid Geometric Isomers. K . Johnston, G. Muschik, W. L . Zielinski, Jr., N C I Frederick Cancer Re search Center 11:40 Anomalous Beilstein Test and Some Possible Problems w i t h Spectrophotometric G C Detectors Which Use Green Copper Band Spectra. C. E. Moore, D . Fogarty, G. Marks, Loyola U 12:00 Determination of N a t u r a l and Synthetic Capsaicinoids i n Capsicum Fruits and Extracts Using Gas Chromatography. M . Bensinger, Alcolac, Inc.; A. Allen, Ka lamazoo Spice Extraction Co.; T . Biftu, Ethiopian Spice Extraction Co., Ethiopia
Chairman:
R. L. Grob, Villanova U
10:20 Determination of Polyun saturated Fatty Acids by Gas-Liq uid Chromatographic Method. G. Durany, Central Soya; B . Jaselskis, Loyola U 10:40 On-Line I R Spectroscopy of G L C Effluents—Some Analytical Applications. V. Viswanathan, G. Manius, G. Capitano, HoffmannLaRoche, Inc. 11:00 Studies of Interactions at Chemical Solid Surface Using Gas-
918 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 1 1 , SEPTEMBER 1975
D. A. Hall, Eli Lilly & Co.
2:00 Spectroelectrochemical Studies of V i t a m i n B ] 2 and Related Cobalamins in Aqueous Media. H . B. Mark, Jr., T . M . Kenyhercz, U of Cincinnati 2:30 SCN-Catalyzed A C Polarography of G a ( I I I ) at Elevated T e m peratures. E. D . Moorhead, G. A. Forsberg, U of Kentucky 2:50 Determination of U r a n i u m Following Reduction w i t h Ferrous Ion in Phosphoric Acid Utilizing Amperometric End-Point Detec tion. K . Lewis, U.S. Energy Research and Development Administration 3:30 Computer-Controlled Elec-
troanalytical Coulostatic Generator. M . Wang, Michigan State U ; B . K . Hahn, D u Pont; C. G. Enke, M i c h i gan State U 3:50 Some T e t r a a r y l b o r a t e - P V C Membrane Electrodes. C. E. Moore, B. Jaselskis, B. H i r u n m i t k n a k o n , Loyola U 4:10 Voltametry at Styrene I m pregnated Graphite Electrode. W. G. Cox, Naval Underwater Systems Center 4:30 Computer-Controlled I n s t r u ment for Stationary Electrode Pulse Voltametry. S. C. Rifkin, D. H . Evans, U of Wisconsin
AMERICAN CHEMICAL SOCIETY PUBLICATIONS IN MICROFORM
Liquid Chromatography: Biological Applications Chairman:
W. E. Shumaker, Waters Assoc.
2:00 Analysis of Ionic Substances by Reversed Phase Liquid Chromatography—Ion Pairing Approach. D. P. Wittmer, J. A. Korpi, Waters Assoc; W. G. Haney, U of Missouri 2:30 Use of High-Speed Liquid Chromatography for Plant G r o w t h Substance Research. M . L . Brenner, A. Ciha, C. R. Andersen, U of Minnesota 3:20 Use of Liquid Chromatography in Determining Metabolic Profiles of 4-Ethylsulfonyl-l-naphthalene sulfonamide ( E N S ) in Various Animal Species. J. W. Stanley, F. R. Fullerton, National Center for Toxicological Research 3:50 I n - V i t r o Synthesis and Secretion of Alphaecdysone by R i n g Glands of Fly Sarcophaga Bullata. W. Bollenbacher, L . I . Gilbert, N o r t h western U 4:20 Applications of High-Performance Liquid Chromatography to Medicine and Clinical Pharmacology. R. L . Wolen, B . D. Obermeyer, L . D. Bechtol, W. Nance, Indiana U 4:50 Role of High-Pressure Liquid Chromatography in Carcinogenesis Research. W. Hagerty, M . D . Corbett, E. A M u r r i l l , Midwest Research Inst.
• Over a million pages of chemistry's premier publications • Back volumes and current subscriptions available • Copying privileges built in to microfilm subscriptions • Current availability of nonprint materials in microfiche • For full details, write or call: Mr. Kenneth Phillips Special Issues Sales American Chemical Society 1155 16th St. N . W . Washington DC 20036 Tel.: (202) 872-4364 and ask for a free copy of the booklet on the "Information Implosion !"
Atomic Absorption Spectroscopy IV: Applications Chairman: Co.
J. C. Guillaumin, Detroit Edison
2:00 Some Considerations for P r e cision and Accuracy in Analysis of M e r c u r y i n Standard Reference Materials by Cold-Vapor Atomic Absorption. M . S. Epstein, T . C. Rains, I . L . Barnes, N B S 2:20 Innovation in Determination of V , N i , Fe, and Cu in Crude Oils by Flameless Atomizer. T . L . Corum, R. G. Schleicher, R. H . Emmel, J. Y. Hwang, Instrumentation Laboratory Inc. 920 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 11, SEPTEMBER
1975
Introducing the Rheodyne
Syringe loading sample Injector uuith single knob control.
Here's the liquid chromatography valve to totally eliminate sample waste 7000 psi operating pressure Low pressure loading of large or small samples by syringe Zero sample loss Uninterrupted solvent flow Rheodyne's new Model 7105 Syringe Loading Sample Injector eliminates the disadvantages of both fixed loop and earlier syringe injection methods used in high pressure liquid chromatography. Yet, the new injector retains the advantages of high pressure capability, convenient use of conventional syringes, variability of sample size, zero sample wastage, solvent compatibility and uninterrupted solvent flow. Select sample volumes ranging in size from less than 1 microliter to 100 microliters (or up to 1 ml. with larger sample loop) with your syringe. There is no waste of sample or interruption of flow. Low price. Fast delivery. More information. Price of the Rheodyne Model 7105 Syringe Loading Sample Injector is S680. Delivery is stock to 30 days AR0. To place an order or get more information, please address Rheodyne, 2809- 10th Street, Berkeley, Calif. 94710. Phone 415-548-5374. .•"
2:40 Determination of Cobalt in Highly Complexée! Radioactive Samples by Flameless Atomic A b sorption Spectroscopy. C. M . Young, J. M . Baldwin, Allied Chemical Corp. 3:20 Some Analytical Possibilities of Cathodic Sputtering in AAS. M . D . Amos, P. A . Bennett, Varian Techt r o n Pty. L t d . 3:40 Application of Microsampling C u p / N i t r o u s Oxide Acetylene Flame Atomic Absorption Spectrometer. D . G. Mitchell, K . W. Jackson, M . K a h l , Κ . Μ . Aldous, New York State Department of Health 4:00 Nutrients in Soil Solution Analysis Using Constant Tempera ture Furnace Atomic Absorption. R. A. Olsen, A. Mubarak, R. Woodriff, Montana State U 4:20 Determination, by Hydride Generation and Atomic Absorption Spectrometry, of Microgram Amounts of Arsenic and Selenium in Metallurgical Products. R.V.D. Robert, National Inst, for Metallurgy, South Africa
Friday Morning, October 10
Electroanalytical Symposium II Chairman: D. A. Hall, Eli Lilly & Co.
9:00 Detection of Anions and Carbonium Ions Based on Polarography of Chloral. W. Szafranski, P. Zuman, Clarkson Coll of Technology 9:30 Computer-Assisted Controlled-Potential Coulometry in Determination of U r a n i u m . S. T. Crosmun, U of Tennessee; T . R. Muel ler, O R N L 9:50 Determination of Trace I m purities in Fused Silica by Differ ential Pulse Anodic Stripping V o l tametry. Y. Su, W . R. Strzegowski, J. P. Williams, D . E. Campbell, Corning Glass Works 10:30 Electrochemical Reduction and Intramolecular Cyclization of 6-Bromo-l-phenyl-l-hexyne, 6Iodo-1 -phenyl- 1-hexyne, and 1Bromo-5-decyne D . M . La Perrière, Β. Willett, W. Michael Moore, D . G. Peters, Indiana U 10:50 Electrochemistry of Cephalothin. D . A. Hall, C. J. Schneider, D . M . Berry, E l i L i l l y & Co. 11:10 Electrochemistry of Cinoxacin. E. C. Rickard, Eli L i l l y & Co.
Process Emission Monitoring Chairman: W. F. Fuller, Du Pont
9:00 Fourier Multiplex Spectros copy Applied to Trace Gas M o n i toring and Analysis. R. E. Gillespie, D. Mattson, K . R. Lindelin, Eocom Corp. 9:20 Photometric Analyzer Sys tem for Total Reduced Sulfur
ftHCODUNC CIRCLE 192 ON READER SERVICE CARD
922 A · ANALYTICAL CHEMISTRY, VOL. 47, NO. 11, SEPTEMBER 1975
(TRS) and S 0 2 Measurements. R. E. Bûcher, R. S. Saltzman, D u Pont 9:40 Permeation Sampling M e t h ods for Petrochemical Applications. J. McKinley, Kintek Labs 10:20 M u l t i p o r t Introduction System for Gas Chromatography and Its Application to A i r Pollution. C. R. Hastings Vogt, D . R. Younker, U of Missouri; W. A. Aue, Dalhousie U 10:40 Toxic Gas Monitor w i t h P a r t per Billion Sensitivity. A. W. Mantz, K . L . Kizer, Digilab, Inc.
Spectroscopy and the Automobile Chairman: A. Bober, U.S. Customs Lab
9:00 Introduction. A. Bober 9:10 Spectroscopy and the Automobile—Glass and Ceramics. H . L . Hoover, Corning Glass Works 9:40 O i l Analysis . . . A Proven Method to Reduce Operating Costs. J. A. Lundquist, Quaker State Oil Refining Corp. 10:30 Trace M e t a l Determination in Petroleum and Petroleum Products by Atomic Absorption and I n duced Coupled Plasma Emission Spectroscopies. A. W. Varnes, M . S. Vigler, A. Eskamani, Standard Oil Co.
of Ohio
11:00 Use of I n f r a r e d Spectroscopy in Rubber Products Related to the Automobile. J. Koenig, Case Western Reserve 11:30 Atomic Absorption Spectroscopy in Automobile Industry. L . C. Westwood, Ford Motor Co.
Liquid Chromatography: Trace Analysis Chairman: P. Talarico, Waters Assoc.
9:00 Use of High-Pressure Liquid Chromatography in Study of Stability of Thiamine Hydrochloride. J. A. Feldman, H . Vora, Duquesne U 9:25 Determination of Chlorinated Dibenzo-p-dioxins in Pentachlorophenol by Liquid Chromatography. C. D . Pfeiffer, Dow Chemical, USA 10:20 Liquid Chromatographic Determination of Low Levels of 25-Hydroxycholecalciferol and 1Alphahydroxycholecalciferol. P. A. Hartman, P. B . Bowman, Upjohn Co. 10:50 Trace Enrichment: N e w Method for Analysis of Organic Pollutants. J. M . Attebery, Waters Assoc. 11:15 Determination of Trace Contaminants by H P L C . S. A. A l i , E. N . Gerhardt, Emory Industries 11:40 Liquid Chromatography: Application of Trace Analysis to Electronic Manufacturing. F. N . Larsen, C. L . Long, Bendix Corp.
