Forensic science in criminal prosecution - ACS Publications

Georgetown University, Washington, D.C. 20007. T n recent years, the courts have subjected some of the classic methods of law enforcement to closer sc...
3 downloads 0 Views 4MB Size
Forensic Science in JOSEPH M. ENGLISH Georgetown Universit y, Wash ingto n , D.C. 20007

N RECENT YEARS, the courts have Isubjected some of the classic methods of law enforcement to closer scrutiny than ever before. For centuries those methods used by enforcement agencies and the prosecution t o solve crimes and to bring the perpetrators t o justice, respectively, have depended upon: (1) confessions of guilt, (2) statements of witnesses to the crime, and ( 3 ) information derived from physical evidence, sometimes called “circumstantial” evidence.

Direct Evidence

The first two-ie., confessions and witnesses-historically have been characterized as “direct evidence.” The last, t h a t is, physical or circumstantial evidence, has been called “indirect evidence,” and, because it is “indirect,” there may have been a tendency t o give it less weight than the “direct” evidence of the coqfession or the witness’s statement. After all, who should know better the details of what happened and the identity of the person who did the deed than the guilty party himself or those who saxv the act committ ed ? Standing alone, free of the encumbrances of the real world, there would seem t o be no more reliable premise upon which t o base the quest for the truth of the matter and on which t o base wise adjudication than the premise t h a t the testimony of those who were present a t the occurrence may be taken as dependable. 40A

However, criminal justice is not administered in the rarefied air of pure thought and pure motives, but in a milieu of complex and sometimes conflicting information and, a t times, considerably less than pure motives-a milieu in which those who administer justice must somehow sort out facts from fictions and, constantly testing the “facts,” fit those which stand the test into place with such patience and skill t h a t the true picture comes clear. The world of the investigator and the jurist is one in which thought systems, therefore, loom importantly. True facts in inept though well-meaning hands can serve justice and injustice with an impartiality reminiscent of the roulette wheel. Cases come to mind in which, for sundry reasons, persons have seriously confused investigations by falsely confessing or by falsifying more or less essential details of the occurrence under investigation. An extortionist, for fairly obvious purpose, in one case confessed t o writing the threatening note which he had prevailed upon his young daughter t o write for him. An airman falsely confessed, after several days of questioning, to murdering a young woman whom he probably had never even met. Two others had confessed to the same crime. However, a mistaken crime laboratory blood grouping mislead the investigators, causing them t o intensify their interrogation of the airman and t o free the other sus-

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

pects. one of whom it now appears committed the crime. After conviction and six years in prison, the airman was cleared by belatedly developed information brought t o light by an energetic newspaper reporter, a dedicated priyate attorney, more careful crime laboratory n-ork, and more accurate testimony than appears to have been used in the original investigation and trial. The attorney spent his own funds contacting widely dispersed witnesses and for other expenses. Over $3000 of these expenditures have not been reimbursed. If some confessions are false, it hardly can be reasoned that all confessions are, therefore, unreliable and should be ignored as without evidential value. The problem may xell lie elsewhere-ie., with the conditions under which the confession was obtained, emotional instability of the person under questioning. excess of zeal on the part of the interrogator, or other factors. TT’hen all necessary conditions are as they should be, a confession is as valid, trustworthy, and reliable a source of accurate information as probably any other. There appears to be a widespread belief among the judiciary t h a t fault too frequently may lie with the investigator through naioet6, zeal, or bias. This overworked public servant, the investigator, almost inherently is under pressure from the community and the news media, through his chief, to “solve” or to “close” cases. Usually he works within a system which provides less

REPORT FOR ANALYTICAL CHEMISTS

Criminal Prosecution If you ever become a victim of crime or if you are mistakenly accused of committing a crime, the scientific disciplines known collectively as the forensic sciences may seem as important, suddenly, as the advances in medical science since Paracelsus.

motivation to look behind a confession than to accept it a t face value and thus t o facilitate an increase in his department’s statistical “accomplishments.” T h a t such a circumstance is a serious threat to objectivity cannot be gainsaid. Errors in Eyewitness Testimony

Let us look a t the evidential value of the testimony of eyewitnesses. For what might be considered very good reasons, this category of “direct” evidence is far less persuasive today than formerly. The fall from grace of eyewitness testimony has followed disquieting experience in cases in which sworn eyewitness testimony, like some confessions, has proved to be in error. Cases can be cited in which convi n c i n g 11 umber s of eyewitnesses have sworn t h a t they observed persons, later proved to be innocent, in the act of committing a felony. Kine such eyewitnesses once swore in a court of law that two defendants on trial were seen by each of the witnesses in the act of committing a robbery and murder. Eight of the nine had picked the two defendants out of what appeared to have been a well-conducted lineup. During the course of the trial, in which the two defendants had all but abandoned hope of acquittal, an astute newsman, once again, led the police to the actual robbers. T h e culprits had disposed of the victimized concern’s moneybags in the basement of the building in which the robbers lived. Each of the nine

witnesses who previously had identified the two earlier defendants later identified the true robbers. For some years, Xew York City banks were victimized by a check forger who regularly passed checks in very large amounts. One day a number of Wall Street banks were defrauded by this man of very large sums. Police were lead to suspect a certain hlr. “A,” an unexceptional suburbanite husband and father of two children. l l r , “,4”happened to be present on the “Street” that day. Six persons who had had direct contact with the forger identified l l r . “A” as the person who had appeared a t their banks and had negotiated the fraudulent instruments in their presence. It was only after seven years in prison that Mr. “A” was exonerated and released as a result of the identification of the real forger through an FBI laboratory analysis of the handwriting on the checks. 11r. “A” died within a year of his release from prison. Tl7hy was eyewitness testimony in error in these instances? The following may help to explain it. When human society was younger, individuals in their daily lives numbered among their acquaintances much larger percentages of the populations of their communities than is possible today. As a consequence, when an event was witnessed in former times, it was a case of the witness’s observing a friend or relative or someone whom the witness recognized. With increases in the numbers of people

populating our cities and towns, a witness who sees a total stranger in the act of passing a fraudulent check, killing a merchant, or committing some other reprehensible act, too often cannot be relied upon to retain an accurate mental image of the criminal. There is an old adage t o the effect that “Murder will out!” It is a homely way of saying that the truth of the matter, regardless of how obscure it may be, will in time be clearly exposed for all to see. The real weaknesses of the classical methods, as was said earlier, would appear to lie largely in the imperfections in the circumstances of their use and from faulty understanding of the inherent weaknesses and strengths of the methods. Now, admittedly, if it is a factand it seems to be a demonstrated one-that confessions and eyewitnesses are especially susceptible to abuse, then certainly the widespread negative judicial reaction is justified. What is offered in their stead? Physical Evidence

-4s the courts rely more and more on scientific evaluation of physical evidence, what assurance is there that this kind of evidence will not also be misused? T o avoid such misuse, there are several necessary conditions: There must, first and foremost, be an uncompromising dedication to finding the truth on the part of the examining scientist and everyone else involved in t h e

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

41A

Report for Analytical Chemists

From Heath UV-Vis to full AA-AE-AF capability in two low cost, modular steps: HI.

step one: add the new Heath EU-702-70 module and get complete flame emission capabi Iity for only . . . . . . .$835.00*

step two: add the EU-703-62 power supply . .$140.00* EU-703-61 chopper assembly . . . . . $ 70.00* EU-703-60 turret assembly . . . . . . . $130.00* and get complete AA-AE-AF capability for only . . . . . . . . . . . . . . .$340.00*

Misuse of Scientific Evidence

another example of how to save money while increasing capability. . . from the Modular Versatility People - Heath Company

FREE HEATH SCIENTIFIC INSTRUMENTATION CATALOG Investigate these and other new ideas in Spectroscopy Digital Instrumentation Lab Equipment and Test Ebuipment. Send for your FREE catalog now.

r-----------I

HEATH COMPANY, Dept. 560-01 Benton Harbor, Michigan 49022

II

Name Address-

I

City

I

~

~ = - a Schlumberger company

State Zpi ‘Mail order prices; FOB factory. Prices & specifications subject t o change without notice. EK-294

Circle No. 62 on Readers‘ Service Card

42A

1

I 0 Please send free Heath Scientific Instrumentation Catalog

I I

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

investigation, prosecution, and adjudication processes. There must be a high level of sophistication on the part of the scientist, the laboratory administration, the prosecutor, and the presiding judge, not to mention the defense attorney. This would include a keen awareness of the state of the art and possible pitfalls of each of the many categories of physical evidence encountered. But all of the sophistication and expertise which can be mustered can be brought to naught or worse in a climate in which those who play the crucial roles are wedded to one side or the other in the criminal justice process more firmly, perhaps, than to the cause of justice itself. The adversary system in which any method for obtaining the facts of a case must be used with the resultant excesses of zeal sometimes observed indeed may well be the one single cause of the problems experienced with direct evidence. Who is to say that the courts will not have equally misleading results from biased “analyses” of physical evidence, results which will be the more heinous for their aura of “science?” A broader and firmer link with the Nation’s universities may help this aspect of the situation. One shudders to contemplate what would be the likely quality of medicine if there were no medical schools, or if there were only as few universities providing the necessary support for education and research in medicine as now provide programs in the forensic sciences, as such.

II I I I I I I

I

T h a t a misuse of the scientific analysis of physical evidence comparable to the misuse of confessions and witnesses is possible on a serious scale may be observed in a number of cases which have come to light in which misinterpretation of data obtained in the examination and evaluation of physical evidence ~ occurred. ~ has These cases reveal serious defects in the professional preparation of investigators and of laboratory experts. Too often the cloak of expertise is gratuitously conferred on a poorly trained or untrained (in a scientific sense) police officer by a

These are a few of the troops. Optical “Building Blocks’’ for the generation and control of radiant energy from the far ultraviolet to the near infrared “Pre-integrated” components for your present requirements, optimized. and just as effective in your future arrangements And, you can add whatever you might need at any time confident of continued superlative performance

You can choose virtually any lamp commercially available, spectral types to multi-kilowatt high pressure arcs; from Schoeffel’s pre-selected lamp list Select any of eleven lamp housings -and power supplies, starters, almost any accessory (coolers, recirculators, ozone removal systems, etc 1 you might need, now or then. Quartz, low f-number single o r double condensing lens systems, focusing sleeves, filters, adapters, irises, light tubes, reflectors, pre-disperser systems

detection? Side-on and end-on photomultiplier , and the patented Thermo-Cooled% PMT Spectral scanners, spectral sensing sysT control-power supplies, photometers, re-

A comprehensivecatalogof more than routine interest is available for the asking Please ask.

Report for Analytical Chemists

Of all the TLC scanners available today, only the Nester/Faust 900 Scanner offers you this unique combination of features. . . source, detector and dual beam optical system with automatic base line compensation . , . in a single, easyto-use unit. In fact, the 900 is so simple to operate, you can get usable data in ten minutes, the first time you use it. All you do is place the plate on the easel and manually park the head over the plate surface, to the left of the first spot. The photometer output (single channel or differential) is then balanced, with the aid of the front panel meter, by a single control. The plate is scanned (8” plate takes 3 minutes) and the head, which stops at the end of the plate, is repositioned for the next row of spots. It’s that easy, and it gives you maximum base line

stability, automatically! There are no mechanical fasteners or linearity adjustments involved. And, any plate, slide or gel up to 10” x 20” and up to YZ’’thick can be scanned, without the need for accessories. The 900 is one of the most reliable electronic instruments you can buy and, because it’s modular in construction, can be geared to your particular needs and budget. For example, when used in conjunction with the 1504 Surnmatic Integrator, it provides automatic detection and immediate digital printout of the area under the analog curve. For information about other optional systems and accessories, plus a lot more data about the unique features of the Nester/Faust 900 TLC Scanner, write today. Nester / Faust Mfg. Corp., 2401 Ogletown road, Newark, Del. 1971 1

The N/F 900 makes TLC scanning easy... gives maximum base line stability

hard-pressed police administrator. The expert thus created by executive fiat has little time and few opportunities to upgrade his training. The work loads of the Nation’s crime laboratories are extremely heavy and are growing a t a fast pace apparently due to the court decisions in Miranda and other cases. Present work loads predictably would be even larger if currently requested examinations could be conducted. Investigators soon learn that certain examinations cannot be handled. There is no point in repeating these requests. Crime laboratory personnel can ill afford to take time from their case loads to acquaint themselves with the developments in the seiences or to obtain needed training even if enough adequate education and training programs were offered by the colleges and universities of the Nation. These institutions of learning, with a few notable exceptions, have too long ignored society’s needs in law enforcement education and training. High-quality educational programs in the disciplines of the crime laboratory, as such, are offered by even fewer institutions in the Nation’s academic community. Little wonder that there is what appears to be a monumental failure of communication between the academic and law enforcement communities. A contributing factor may be the innocence of much of the funding community. Foundations seem to be unaware that the forensic sciences constitute a valid academic area and that, in these sciences, there is enormous potential for addressing some of the more serious deficiencies of the criminal justice process and that this area is suffering, in its turn, from staggering problems due largely to chronic academic, governmental, and foundation community neglect. Standards Are Needed

If we prescind from the foregoing and turn to an examination of the heart of the workings of physical evidence evaluation, we find t h a t standards-setting is a major problem. There is little evidence of wide-spread agreement, for ex(continued on p a g e 47A) Circle No. 108 on Readers’ Service Card

44A

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

What? Never used REP1PETS"andDilutors? Did you know more than 70,000 L / I instruments are now used in research and clinical labs? Here's why: L/I Automatic Dilutor for aspirating and diluting 1. Simple operation. J u s t set' volume with knife-edge pointer, lift plunger to aspirate, and depress plunger t o deliver. (No mouth pipeting!) 2. LAMBDA-DIAL" increases accuracy. R e p l a c i n g any 1 m l REPIPET or Dilutor plunger, the LAMBDA-DIAL boosts accuracy to a phenomenal 1% at 10 lambdas! Reset to 0.1 lambda at 100 lambdas. 1 division=O.l lambda.

3. All PYREX Construction. Handle any reagent, including conc e n t r a t e d acids, c o n c e n t r a t e d alkalies, c h l o r i n a t e d h y d r o c a r bons, etc. Closed system eliminates odors and all contact with dangerous reagents.

. Reagents

I

stay pure. Integral

filters keep out the atmosphere and protect valuable reagents.

5. High accuracy (lYo) and reproducibility (0.1Y0). E a c h i n strument is adjustable and accurate over its entire range.

6. Fit any reagent container. All REPIPETS and Dilutors can be with caps and washers your reagent containers. O r ill furnish containers tosuit,

7. GRUNBAUM@Pipet extends versatility. Supplements REPIPETS and Dilutors by allowing you to transfer and store reagents. Self-cleaning, nond r i p p i n g , self-adjusting GRUNBAUM Pipets are available from 1 to 1,000 PI in 18 sizes.

8. Wide Selection. L / I stocks REPIPETS and Dilutors in 1/2, 1, 5, 10,20 and 5o ml sizes, Micro and Teflon tips included. Amber round

-

L/I Automatic REPIPET for dispensing tor.

extra charge. Prices: REPIPETS $52.50; Dilutors

$99*50;

Cie, 209 Rout;! De Colmar, 67 S t r a s b o u G - M e i n u e , France; B i o - R a d Laboratories G m b H , 8 M u n c h e n 66-Limesstra, 71, Postfach 2260, West G e r m a n y : B i o t r o n i k Wissenschaftllche G e r a t e G m b H , D a c h a u e r Str. 511, 8 M u n c h e n 50, West Germ a n y : Van O o r t m e r s s e n , N.V., P.O. B o x 501 T h e H a g u e , Netherlands.

$49-50;

GRUNBAUM Pipets: $6 to $10.

% LABINDUSTRIES The Error €/iminators 1802A Second Street, Berkeley, California 94710 Phone (415) 843-0220. Cable LABIND, Berkeley, CA (USA) Circle No. 92 on Readers' Service Card

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

45A

Read h o w Thermal Methods, the newest techniques of material characterization, offer you both quantitative and qualitative data

Thermal Methods are unique techniques for identifying material characteristics. What you do is subject a milligram-size sample of material to precisely controlled temperature changes. Property changes measu red by a specific transducer are recorded and can give you a world of information about the material. More specifically, it can identify the material for you, show differences between chemically similar materials, and show thermal or mechanical history of the sample. The thermogram, the record of this response, is like a fingerprint: positive identification.

Thermal Methods can also give you information o n the chemical behavior of m a t e r i a l s . You c a n d e t e c t a n d measure polymerizationof monomers and prepolymers. You can measure partial curing (B stage) of thermosetting resins. And that’s only the beginning. You can study chemical reaction kinetics in detail, such as rates of crystallization or polymerization. You can study physical changes in detail such as sublimation, vaporization, fusion, crystal-crystal transitions, and first-order and secondorder transitions (glass transitions). Also, changes in weight, volume, elastic and compressive moduli and

creep phenomena. And the best part of all this is that all these measurements are easy to make, analyses are fast (many taking less than ten minutes) and data are reproducible. Du Pont offers the only complete Thermal Methods Laboratory including capabilities for Differential Thermal Analysis, Differential Scanning C a l o r i met ry, T h e r m o m e c h a n i c a l Analysis a n d T h e r m o g r a v i m e t r i c Analysis. We have a new bulletin describing the many applications of the D u Pont Thermal Methods Laboratory. For your free copy, write Du Pont, Room 8728, Wilrnington, Delaware 19898.

@JmmInstruments

D u Pont Thermal Analysis Seminars presented daily at the Pittsburgh Conference.

REG u

sP

A ~ O F ~

Circle NO. 65 on Readers’ Service Card

,

Report for Analytical Chemists

ample, as to the extent of the qualitative and quantitative data extractable from soil evidence by the more advanced techniques which might safely be relied upon to provide the bases for source or origin determinations at useful levels of specificity. Identifying those acceptable and alternate laboratory procedures for obtaining data from each kind of evidence amenable to measurable data extraction may aid the courts in their efforts t o exclude incompetent testimony. Standard reference materials to serve widely separated laboratories may speed the handling of cases and raise the quality of their examinations. Other needs are for: 1. A multidiscipline approach to a better understanding of the scholarly legitimacy of the Ydentification” process as a scientific procedure for determining with as high a level of specificity a s possible the source of an item of questioned evidence in terms of comparable items of known source. 2. Programs of background sampling and data collection essential to the evaluation process in the de-

termination of just how unique a questioned piece of evidence actually is. 3. Broad check sample programs which would serve to keep individual experts informed as t o their true levels of expertise as compared with their fellows in a given area or with a given analytical method. 4. Programs to attract the better college graduates into the crime laboratory disciplines. 5 . Professional education and training programs such as those which have brought medicine to the professional level it has achieved and would promote the continuing close rapport between the academic community and the professional practitioners in the crime laboratories. 6. Programs of public education t o recognize the importance of competent examination and evaluation of physical evidence t o the proper administration of justice. 7. Programs to alert the general public and the foundation community to the need to be informed in the Forensic Sciences. 8. Curricula improvement in our

Joseph M. English is Director of the Forensic Sciences Center in the Institute of Criminal Law and Procedure, Georgetown University L a w Center. H e is also: assistant professor, forensic pathology, in the department of pathology, Georgetown University School of Medicine; adjunct professor in the Georgetown University Law School; and adjunct professor in the American University Center for the Administration of Criminal Justice. Mr. English received his B.S. degree at St. Joseph’s College, Philadelphia, Pa., in 1939 and his M.A. degree a t George Washington University, Washington, D . C., in 196Y. He served on the staff of the F B I Laboratory, Document Section, from 1942 to 1966 when he joined the Institute of Criminal Law, Georgetown University Law Center, to establish the Forensic Sciences Center. He is active in the American Academy of Forensic Sciences, the A A A S , the International Association of Chiefs of Police, Phi Delta Kappa, Society of Former

Special Agents of the F B I , and the Chesapeake B a y Chapter of the International Association for Identification. H e is chairman of the steering committee of the American Society for Testing Materials which is in the process of organizing a new permanent committee of A S T M in the forensic sciences. This month he is chairing the forensic sciences session at the Eastern Analytical Symposium, November 19, N e w York, N . Y . Circle NO. 15 on Readers’ Service Card

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970

47A

Report for Analytical Chemists

law schools to furnish those students who, in their professional lives, will be required to act on information furnished by scientific experts. 9. Curricula improvement in our medical and nursing schools for those who will be in positions t o preserve or to destroy utterly, evidence which could lead to the identification of an assailant. (See also Rose, John C., M.D. “Medical Centers and Crime Laboratories,” Proceedings of T h e First Georgetown

Conference o n Surface Analysis, October, 1969.) Many rapists have gone free to strike repeatedly because emergency room hospital per-

sonnel had no professional preparation to alert them to the importance of avoiding commingling of articles of the victim’s clothing, and obtaining adequate and proper swab specimens while ensuring against evidential contamination and disturbance of chain of custody. These are but a few of the problems the Nation faces in law enforcement and the preservation of a just order. They represent some of the more important problems which grow directly out of those of the Nation’s crime laboratories. Other problems exist in the state of research and the consequent state

of the a r t in a number of the crime laboratory disciplines, in the state of expert qualification and certification standards, in legal education, and the continuing professional preparation of law students, lawyers, and judges in the sophisticated utilization of expert testimony. What is most important is t h a t informed Americans, especially scientists as well as all others who share a dedication to the improvement of the administration of justice and of the human condition, be informed in this area, as in all others which are crucial to the wellbeing of society and its members.

JANUARY SESSIONS The following ACS Short Courses are newly scheduled for January 1971. The premier session of “Fluorescence and Phosphorescence Spectrometry” is being offered in Philadelphia. To register or obtain complete information on the courses, convenient lodging, and student discounts, please write to Education Office, American Chemical Society, 1155-16th St., N.W., Washington, D.C. 20036. During the two-week period prior to a course, registration should be made by telephone: area code 202, 737-3337 ext. 258.

forecasting, marketing, new ventures, finance, cost accounting, project and product development, and evaluation of operations. Because business and economic aspects are becoming more critical relative to technological factors, the course will emphasize competitive aspects of the chemical business. No previous training in business or economics is required.

FLUORESCENCE AND PHOSPHORESCENCE SPECTROMETRY

GC/MS/COMPUTER TECHNIQUES Jan. 8-9-New York City. Dr. Francis W. Karasek, Dr. William H. McFadden, and Walter E. Reynolds; fee $85; required text, L. S. Ettre and W. H. McFadden, eds., “Ancillary Techniques of Gas Chromatography,” John Wiley & Sons, Inc., $17.50. This course first reviews the fundamentals of gas chroma. tography and mass spectrometry, and then presents in more depth the principles important to the GC/MS combination instrumentation. Subject matter includes the characteristics of the different types of mass spectrometers, the GC/MS interfaces, discussion of instrumentation, the GC/MS combination, and computerization of the output. Although a B.S. in chemistry or related science is a desirable background, anyone with sufficient experience-or the assigned responsibility-to work with the instrumentation will benefit from the course.

BUSINESS ASPECTS OF CHEMISTRY Jan. 15-16-Chicago, Ill. sponsor, Chicago Section.

Dr. Aimison Jonnard; fee $80;

This course is designed to give chemists and chemical engineers a pragmatic introduction to the business and economic practices which govern the management of chemical corporations. Topics include economics of pricing and price 48A

Jan. 21-23-Philadelphia, Pa. Dr. George G. Guilbault; fee $115; required text, G. G. Guilbault, ed., “Fluorescence: Theory, Instrumentation, and Practice,” Marcel Dekker, New York, 1967, $17.75; sponsor, Philadelphia Section. This new course introduces the basic principles and practical applications of all types of luminescence. Emphasis is on fluorescence and phosphorescence, but chemiluminescence, bioluminescence, electrogenerated luminescence, and others are also covered. Topics include effects of structure and environment on luminescence; assay of inorganic and organic substances using luminescence; instrumentation; monitoring of a solid surface. There will be hands-on laboratory sessions with a variety of instruments. The course will be of value to chemists, biochemists, clinical and medicinal chemists, spectroscopists, and technicians. Two years of college chemistry and math is sufficient background.

MODERN ORGANIC SYNTHESIS Jan. 27-28-New York City. Edwin Vedejs; fee $75.

Dr. Barry M. Trost and Dr.

This course is intended for individuals who are concerned with putting organic molecules together. It covers both the methods and tools of organic synthesis, with heavy emphasis on modern aspects of synthesis. Individual syntheses are selected which afford maximum exposure to a variety of concepts and tools. Research supervisors, bench chemists, and teachers will all benefit from the course.

ANALYTICAL CHEMISTRY, VOL. 42, NO. 13, NOVEMBER 1970