LA-TOF-ICP-MS, 305-307

Downloaded by 80.82.77.83 on May 28, 2018 | https://pubs.acs.org Publication Date: August 16, 2007 | doi: 10.1021/bk-2007-0968.ix002

Subject Index Aconcahua source, Peruvian obsidian, 536 a D N A extraction and analysis from archaeological specimens, 78-98 ancient coastal migration detection from skeletal remains, 80 authentication and assessment, results, 92-93 burial context, biological relationships, 80-81 economic stratification, prehistoric populations, 81-82 molecular markers, 83 problems and properties, 82-85 sex determination techniques, 79-80 tuberculosis, mummy at Chiribaya Alta site, 82 Africa. See Botswana prehistoric mines; Curse tablets from Roman Carthage Alaska, ancient coastal migration detection by mtDNA from skeletal remains, 80 Alca source, Peruvian obsidian, 532, 534 A l i Kosh, Neolithic site in Iran, 138, 139/ Alkaline-based glazes, firing properties, 423^124 American trade monopoly in 16 century, Castilian Kingdom, 397398 Ancient D N A . See aDNA Andes, geographic origins, trophy heads, 99-113 Apatite values, skeletal remains, five Sardinian sites, 124, 126/ th

Archaeological obsidian sources, Peru, 522-552 Archaeological textiles from eastern North America colorant classification, 15-43 colorant testing protocol, 29-39 coloration, literature review, 1617 fiber and particulate residues, infrared examination, 44-77 Archaeological thin sections, microfocus X-ray analysis methods, 197-206 Artifact exportation limits, 506-507 Augustus. See Octavian Australia, Katipiri Formation, ESR dating of teeth, 3, 5, 6/ Ayacucho, strontium isotope ratios, modern guinea pigs, 104-106 Aztec human sacrifices, sex determination by aDNA techniques, 79-80

Β Baltimore Museum of Art, 343 Basra Petrofabric, 436 Bison, demographic modeling by aDNA data, Bayesian statistical techniques, 81 Bitumen traces in ceramic vessels from Neolithic Iran, 137-151 pottery sherds, sampling and characterization, 141-142 Black willow, charred, infrared spectra, 63, 64/ Blue-colored ceramic glazes from Mesopotamia, L A - I C P - M S analyses, 425-426

557

Glascock et al.; Archaeological Chemistry ACS Symposium Series; American Chemical Society: Washington, DC, 2007.


558 Bone and enamel, archaeological, strontium isotope analysis, 102-104 Bone chemistry, principles, 116-117 Bone materials in archaeological soils and sediments, 198,200-204 Botswana prehistoric mines, specular hermatite source fingerprinting, 460-479 Brick Chapel, St. Mary's City, building materials, 364-375 Brigham City Co-Operative Pottery, 448-449 British Columbia, Keatley Creek, prehistoric population economic stratification, aDNA determination, 81-82 Building materials, brick Chapel at St. Mary's City, 364-375 Bulk isotopic analysis (5 C and 5D), asphaltene in bitumen samples, 141-149 Burial context, biological relationships determination by aDNA variations, 80-81 13

C California glass beads, lead isotope analysis by LA-TOF-ICP-MS, 305-307/ marine shell beads, Olivella source zones, 169-170 population movement studies, Fish Slough Cave, Owen's Valley, 80 Canary Islands, majolica pottery characterization, 376-398 Canonical discriminant analysis, ochre artifacts from Jiskairumoko, I N A A data, 493, 500 Carbon stable isotope ratios in Olivella biplicata shell beads sourcing, 180-185/ Carthage. See Punic Carthage; Roman Carthage

Carylloma and Uyo Uyo obsidian sources, Peru, 538 Casa de Contratacion, 377-378, 397398 Castilian Kingdom American trade monopoly in 16 century, 397-398 Canary Islands, history, 377378 Central Petén, field-portable X R F identification of obsidian sources, 506-521 Ceramic glaze components, 423 Ceramic glazes from Mesopotamia L A - I C P - M S compositional analysis, 424-427 lead isotope analysis, 427-429 technology, 422-446 Ceramic pastes, bulk analysis, 282, 284,285/ Ceramic vessels from Neolithic Iran, bitumen traces, 137-151 Cerro Ticilago, Lisahuacho, and Potreropampa obsidian sources, Peru, 537-538 Chagha Sefid, Neolithic site in Iran, 138, 139/ Chapel bricks and clays, pétrographie analyses, 369-370/ Charred fibers, 61-67 Charring fibers, 49-50 Che Tsung, coins, elemental compositions, 233, 240/-241/ Chen Tsung coins, elemental compositions, 233-236/ Chicamuxen Church Formation clays, possible Chapel brick source, 371— 372/ China copper-based coins from Song dynasty, chemical composition by E D X R F , 231-245 Dragon Jar glazes, characterization by L A - I C P - M S and I N A A , 284287, 288/


th


559 Chinese copper-based coins from Song dynasty, chemical composition by E D X R F , 231-245 Chinese emperors' coins, elemental compositions, 233-243* Chiribaya Alta site, tuberculosis determination from aDNA studies, 82 Chivay source, obsidian, Peru, 534 Church of Jesus Christ of Latter-day Saints. See Latter-day Saint Clay deposits, St. Mary's County, 365/, 368 Clay sampling for brick and tile studies from St. Mary's County, 368-369 Climatic trends δ Ν and 5 C variations correlation with δ 0 variations, 126-131 δ 0 in paleoclimatic reconstruction, 127-131 Cluster analysis ochre artifacts from Jiskairumoko, I N A A data, 4 9 3 , 4 9 8 / 4 9 9 / 500 Philistia pottery grouping by chemical analyses, 407-411 Coins, copper Herodian prutah, physical measurement and elemental composition, 247-249 Song dynasty, chemical composition by E D X R F , 231-245 Coins, silver, Isfiya and Qumran coin hoards, chemical composition, 258274 Collagen values for skeletal remains from Sardinian sites, 123-125/ Colorado, Mesa Verde pottery sherds, Β lack-on-white paints, characterization, 287-292 Colorant testing protocol for archaeological textiles, 29-39 Colorants in eastern North American archaeological textiles, 15-43 1 5

13

1 8

1 8

Comparative Plant Fiber Collection (CPFC), 45, 47 distinctions in archaeological materials, 55, 59/-60 Conchopata ceramics, 350-351 Conchopata trophy heads, geographic origins, 100-109 strontium isotope results, 106-108 Cone collection. See Baltimore Museum of Art Contamination control, aDNA studies, 84-85 Cooking and eating in ancient Mesoamerican plazas, 210-230 Copper alloy artifacts, applications of laser ablation ICP-MS, 336-348 Copper-based coins from Song dynasty, E D X R F chemical composition determination, 2 3 1 245 Copper coins, Herodian prutah, E D X R F elemental compositions, 246-257 Copper in ceramic glazes, pottery from Latter-day Saint Utah, 456 Copper salts in fiber mineralization, 51 Coprolite human mtDNA extraction, Hinds Cave, Texas, dietary reconstruction, 81 Coprolites and population movement, discovery using human mtDNA techniques, 80 Cotallalli source, obsidian. See Chivay source, obsidian CPFC. See Comparative Plant Fiber Collection Cremation ceremonies in fiber charring, 49-50 Crocodylian teeth, ESR dating techniques, 5. 10, 11/ C u , internal standard for L A - I C P M S analysis, copper alloy artifacts, 339

65


560


Curse tablets from Roman Carthage, lead isotope analysis, 311-335

Data preparation, specular hematite source fingerprinting by I N A A , 467-468 Data quantification in L A - I C P - M S , 277-278 Data treatment, tin and lead concentrations in majolica pottery production, 383-384 Defixiones. See Curse tablets Deh Luran Plain, ceramic glaze samples for compositional analysis, 424-427,434, 436-437,440 Depth profiling, coating samples from Little Lost River Cave, 162-163 Detection limits in L A - I C P - M S protocol testing copper alloy analysis, 341 Wari ceramics elemental analysis, 353-354/ Devni-Khadri, India, ESR crocodilian teeth and elephantid tooth dating, 5, 7-10,11/ Diagenesis in strontium isotope analysis, 101-102 Didrachms. See Tyrian shekels and half-shekels Diet and stable isotopes, western Mediterranean prehistory, 118-120 Dietary reconstruction from coprolites, human mtDNA extraction, Hinds Cave, Texas, 81 Dietary research through stable isotopes, principles and interpretation, 115-117 Dikgatlampi workings, Botswana, spéculante sourcing, 465 Discriminant function analysis, I N A A geochemical data, 466, 469-477/

Disease, aDNA studies, tuberculosis in mummy from Chiribaya Alta site, 82 D N A , ancient. See aDNA Dragon Jar glaze characterization by L A - I C P - M S and I N A A , 284-287, 288/ Dyeing fiber technology, 51 Dyes and pigments, general characteristics, 18-19 Dyes, infrared identification, 71, 7 3 / 74 Dyestuffs with plant sources, 22/-24

Eastern North American archaeological textiles colorant classification, 15-43 colorant testing protocol, 29-39 coloration, literature review, 16-17 fiber and particulate residues, infrared examination, 44-77 Eating and cooking in ancient Mesoamerican plazas, 210-230 Economic stratification, prehistoric populations aDNA determinations, Keatley Creek, British Columbia, 81-82 EDS. See Energy dispersive spectrometry E D X R F . See Energy dispersive X-ray fluorescence Ekron, Iron IA Philistine Monochrome pottery, 418 El Chayal, Guatemala, obsidian source, 511 Electron microprobe analysis ( E M P A ) Roman Carthage curse tablet analysis, 315, 317-325/ theory and application, 261, 263 Electron spin resonance (ESR) dating, teeth, 1-14



561 Elemental analysis by X R F , silver Tyrian coins, 263-272/ Elemental composition, E D X R F copper-based coins from Song dynasty, 231-245 copper coins, Herodian prutah, 246257 Elemental concentrations and standard deviations, obsidian sources, Peru, 539, 540/-542/ Elemental contour maps, sherd surfaces, by L A - I C P - M S , 289292 ElvaX Regression program, 513 E M P A . See Electron microprobe analysis Enamel and bone, strontium isotope analysis, 102-104 Energy dispersive spectrometry (EDS), scanning electron microscopy, Seip textiles, 35 Energy dispersive X-ray fluorescence (EDXRF), elemental analyses copper-based coins, 231-245 copper coins, Herodian prutah, 246257 obsidian samples, 513-514, 516/ "English brick," 366 ESR. See Electron spin resonance dating Ethnoarchaeological studies, cooking and eating in Mesoamerica, 212215 Etowah Mound, Ohio, colorants in archaeological textiles, 44-77 Euclidean distance for chemical grouping by cluster analysis, 407 Eygin Gol Necropolis, Northern Mongolia, biological relations from burial context, determination, 8081

F Fiber and particulate residues, archaeological textiles by infrared techniques, 44-77 Fiber charring, 49-50 Fiber dyeing, 51 Fiber mineralization, 51 Field analysis by X R F , obsidian sources in Central Petén, Guatemala, 506-521 Fish Slough Cave, Owen's Valley, California, population movement studies, 80 Food and soil, chemical links, 2 1 1 212 Forensic photography, prehistoric textiles, 27, 29

G Glass beads from central California, lead isotope analysis by L A - T O F ICP-MS, 305-307/ Glaze and paint characterization by L A - I C P - M S , 284, 286-288/ Utah, historic, pottery glazes, chemical analysis, 452-457 See also Pottery Guatemala Central Petén, field-portable X R F identification of obsidian sources, 506-521 Las Pozas, Petén, ethnoarchaeological studies, cooking and eating, 215218/ Guinea pigs from Ayacucho, strontium isotope ratios, 104— 106


562


H Hafnium and neodymium concentrations in Wari ceramics, 361-362 Heavy metal sand metals, traceelement data, St. Mary's County, 371-372/ Heavy mineral separation, specular hematite source fingerprinting, 465-466 Herod Agrippa I, copper coins, elemental composition by E D X R F , 246-257 Herod's relationship with Octavian, 269, 271,273 Herodian prutah, elemental compositions, 246-257 Historical Ecology Project, Central Petén, Guatemala, 517 Honduras, Palmarejo, ethnological studies, cooking and eating, 217228 Honduras, Petoa, Santa Barbara, ethnological studies, cooking and eating, 215 Hopewell Mound Group, Ohio, archeological textile source. See Seip Mound Huamanga Basin, Ayacucho Valley, food supply for Wari heartland, 104 Human activities, determination by elemental soil data, 221— 228 Human bone and teeth, characterization by L A - I C P - M S , 292-294/ Human burials at Conchopata, strontium isotope ratios, 105/, 106 Human dental enamel, strontium isotope analysis by LA-TOF-ICPM S , 306-308

Iberian Peninsula, production centers, majolica pottery found on Canary Islands, 384, 385-398 Icelandic Norse-trading site, sulfur materials, simultaneous co-incident x-ray micro-fluorescence and microdiffraction analyses, 204-205 ICP-MS. See Inductively coupled plasma-mass spectrometry ICP-OES. See Inductively coupled plasma-optical emission spectroscopy. Idaho, Little Lost River Cave, black coating on pictographs, surface analysis, 152-166 I N A A . See Instrumental neutron activation analysis India, ESR crocodilian teeth and elephantid tooth dating from DevniKhadri, 5, 7-10, 11/ Indian hemp [N.A. plant] fibers, charred and uncharred, 61-64/ Inductively coupled plasma-mass spectrometry (ICP-MS) and ICP-OES chemical analyses, Philistine pottery, 402-411 correlation to L A - I C P - M S elemental analysis, Matisse bronze sculptures, 343-346 Olivella biplicata shell compositional chemistry, geographic patterning, 170-180 prehistoric textiles, 29, 35 Roman Carthage curse tablets, 319, 332, 333/ with laser-ablation sample, archaeological research introduction, 275-296 Inductively coupled plasma-optical emission spectroscopy (ICP-OES), soil chemicals, cooking and eating in Mesoamerican plazas, 210-230



563 Infrared distinctions between fibers in Comparative Plant Fiber Collection, 52, 55-59/ Infrared photography, 25 Infrared spectra examination comparative modern plant and animal fibers, 52-54/ fiber and particulate residues from archaeological textiles, 44-77 Inorganic mineral pigments, textile fibers, 19-21/ Instrumental neutron activation analysis (INAA) building materials from St. Mary's City Chapel, 364-375 majolican pottery sherds. Gran Canaria Island, chemical analyses, 381,383 majolican pottery sherds, origin, 392-397 Mesopotamian glazed ceramics, 430-433,435/, 437-440 obsidian sourcing, 278, 279-281 See also Neutron activation analysis Intermountain Region, North America, historic pottery, 447-459 Iran, Neolithic, bitumen traces in ceramic vessels, 137-151 Iran, Neolithic sites A l i Kosh, 138, 139/ Chagha Sefid, 138, 139/ Iraq, Mesopotamian ceramic glaze technology, 422-446 Iron Age Philistine pottery from Israel, intra-regional sourcing, 399421 Iron log ratio transformation, X R F results, majolica pottery origin, 384-385 Iron oxide. See Ochre Isfiya and Qumran coin hoards, chemical composition, 258-274 Isotope ratios for archaeology, 298309

13

Isotopic characterization 6 C and 5D values, asphaltene in bitumen samples, 146, 148/ 149/ Israel. See Coins, silver; Philistine Iron Age pottery Italy. See Roman Carthage; Sardinian prehistory Ixtepeque, Guatemala, obsidian source, 511-512

Jampatilla, Peru, obsidian source, 536 Jen Tsung, coins, elemental composition, 233,237/-239/ Jiskairumoko, Peru, ochre artifacts instrumental neutron activation analysis, 480-505 mathematical and statistical data treatment, 492-501

Κ Katipiri Formation, Australia, ESR dating of teeth, 3, 5, 6t Keatley Creek, British Columbia, prehistoric population economic stratification, aDNA determination, 81-82 King James Bible, M k 12:41-44, 247 Kriging modeling, ethnological studies, Palmarejo, 221-228

L La Cueva Pintada, Gran Canaria Island, majolica pottery archaeological site, 378, 379/ L A - I C P - M S (Laser ablationinductively coupled plasma-mass spectrometry)



564 archaeological research, 275-296 ceramic glazes, 424-427 copper alloy artifacts, 336-348 correlation to ICP-MS results, elemental analysis, Matisse bronze sculptures, 343-346 glaze recipe analysis, techniques, 449-452 historic Latter-day Saint pottery glazes, 447-459 Peruvian Wari ceramics, characterization, 349-363 LA-TOF-ICP-MS (Laser ablationtime of flight-inductively coupled plasma-mass spectrometry) laser-induced fractionation, 300301/ real world precision, analytical parameters, 299-302 Lake Eyre Basin, Australia, marsupial teeth dating, 3, 5, 6/ Lake Titicaca basin, ochre artifacts, open air residential site, 481-483, 484/ Lanthanum, log ratio transformation, I N A A results, majolica pottery origin, 392 Las Pozas, Peten, Guatemala, ethnoarchaeological studies, 215 Laser ablation-inductively coupled plasma-mass spectrometry. See L A ICP-MS Laser ablation-time of flightinductively coupled plasma-mass spectrometry. See LA-TOF-ICP-MS Latter-day Saint pottery glazes, analysis by L A - I C P - M S , 447-459 Lawrence Berkeley National Laboratory ( L B N L ) , obsidian sourcing research, 529, 532, 534, 539, 544/ Lead-based glazes, firing properties, 423-424

Lead-based glazes from historic Utah, chemical analysis by L A - I C P - M S , 452-457 Lead-based glazes from Mesopotamia, 422-446 Lead concentrations by X R F , majolican pottery sherds, 383, 384/ Lead for glazes, scarcity, 448-449 Lead isotope analysis archaeological method, 313 ceramic glazes from Mesopotamia, 427-429 LA-TOF-ICP-MS for archaeology, 298, 302-303/ 305-306/ 307/ ore origination studies, Roman Carthage curse tablets, 311-335 Lead isotope ratios, Roman Carthage curse tablets, 326, 328/^332/ Lighting and sample selection, archaeological textiles colorant testing, 37 Lignins in plant fibers, 49-50/ Ligurian origin for majolica pottery from Canary Islands by I N A A determination, 392 Limitations colorant testing protocol, archaeological textiles, 38-39 L A - I C P - M S analyses, 337 Linearity in protocol testing, L A - I C P M S copper alloy analysis, 340 Literature review, textile colorants, 17-27 Little Lost River Cave, Idaho, black coating on pictographs, surface analysis, 152-166

Majolica pottery from Canary Islands, 376-398 origin by X R F , 385-391/



565 Majolica pottery sites, Gran Canaria Island La Cueva Pintada, 379-381/ San Francisco convent, Las Palmas de Gran Canaria, 379-380, 382/ Mancos Black-on-white paints from Mesa Verde pottery characterization by L A - I C P - M S , 287-288/ elemental surface maps of pottery sherds, 289-290/ Manganese in ceramic glazes, pottery from Latter-day Saint Utah, 456 Manganese variations in transect samples, St. Mary's Hill, 370-371/ Manises, production center, majolica pottery, I N A A determinations, 392-397 Marine shell beads, sourcing, 167— 193 Marsupial teeth, dating by ESR techniques, 3, 5, 6/ Maryland, St. Mary's City, Brick Chapel, building materials, determination, 364-375 Maryland's history, 365-366 Maryland's geology, St. Mary's County, 365/ 368 Mass bias correction with L A - T O F ICP-MS, 300/ 301-302 Mass spectrometry for stable isotopic analyses, principle, 116 Matisse bronze sculptures, applications of laser ablation ICPM S (LA-ICP-MS), 343-347 Mesa Verde Black-on-white paints characterization by L A - I C P - M S , 287-288/ elemental surface maps of pottery sherds, 289, 290/-292 Mesa Verde painted pottery, black paints, characterization, 287-288/ Mesoamerican plazas, cooking and eating evidence from soil chemical data, 210-230

Mesopotamian ceramic glaze technology, 422-446 Mesopotamian glazed ceramics, compositional analysis variations, 430-440 Mesopotamian historical periods, ceramic technology, 443/ Metallic inclusions in Roman Carthage curse tablets, electron microprobe analysis, 315-317, 319325/ Method sequencing in colorant testing protocol, archaeological textiles, 38 Mexico ethnological studies, cooking and eating, 212-214, 215-218/ Pachuca, obsidian source, 512 Microfocus x-ray analysis methods, archaeological thin sections, 197206 Microscalé features, archaeological soils and sediments, analysis goals, 195 Middle Woodland period site. See Seip Mound Milkweed, common, charred, infrared spectrum, 63, 6 5 / Mineralized fibers, 51 spectra compared to archaeological textiles, 63, 67-69/ Minimal composition variation, discriminating obsidian sources, 281-282, 283/ Mississippian period site. See Etowah Mound Molecular sex and human behavior determinations, aDNA applications. See aDNA Mongolia, Northern, Eygin G o l Necropolis, biological relations from burial context, 80-81 Monti Arci, Sardinia, obsidian artifacts, sourcing, 279-281, 283/ Muxuccuxcab, Yucatan, Mexico, ethnoarchaeological studies, 214


566 Mycenaean pottery production by Aegean or Cyprus immigrants, 418


Ν N A A . See Neutron activation analysis National Museum of Carthage, 314 Native Americans, coastal migrations, 80 Neodymium and hafnium concentrations in Wari ceramics, 361-362 Neolithic domesticated animals and crops, western Mediterranean, 118120 Neolithic Iran, bitumen use, 137-151 Neutron activation analysis ( N A A ) obsidian analysis procedure, overview, 531 obsidian chemical characterization, 528-529,543-547 See also Instrumental neutron activation analysis New Wave UP213 laser, 338, 351 North America, eastern, archaeological textiles colorants, 15-43 fiber and particulate residues, 44-77 North America, intermountain region, historic pottery, 447-459 Norway, bone materials from archaeological sites, 198,200-204

Obsidian chemical characterization, experimental procedures, 527529, 530-532 geochemistry, 525-527 procurement at Trinidad de Nosotros, 515-518

research history in Peru, 529530 Obsidian provenance determinations, general, 278 systematic approach, 523-525 Obsidian sources Central Petén, Guatemala, determination by field-portable X R F , 506-521 Oregon, Sycan Marsh and Silver Lake source domes, 281-283/ Pachuca, Mexico, 512 Peru, 522-552 western Mediterranean artifacts, 279-281 Ochre artifacts at Jiskairumoko, Peru, I N A A , 480-505 archaeological contexts, 483,485486 characteristics, 487-491/ variability, 501-502 Ochre pigments, 19, 67,12f-11f Octavian, relationship with Herod, 269, 271,273 Ohio, archaeological textile colorants, 15-43,44-77 Ohio Historical Society, 32 Olivella biplicata shell beads, geographic sourcing methods, 167— 193 On Your Knees Cave, Alaska, ancient coastal migration, mtDNA from skeletal remains, 80 Optical microscopy, 25, 29, 34 Ore origination studies, Roman Carthage curse tablets, 311-335 Oregon, Sycan Marsh and Silver Lake, discriminating obsidian sources, 281-282,283/ Organic constituents, detection, 2 6 27 Osumacinta Viejo, Chiapas, Mexico, ethnoarchaeological studies, 214 Oxalate inclusions accompanying plant fibers, 48


567


Oxygen stable isotope ratios, sourcing Olivella biplicata shell beads, 180— 188

Pachuca, Mexico, obsidian source, 512 Painted fabric preparation for comparison to prehistoric textiles, 27-28/ Paints and glazes, characterization by L A - I C P - M S , 284, 286-288/ Palmarejo site, Honduras, ethnoarchaeological studies, 217228 Paloma, Peru site, human bone and teeth, characterization by L A - I C P M S , 292-294/ P C A . See Principal component analysis PCO. See Plasma-chemical oxidation P C R a D N A amplification for screening single nucleotide polymorphisms and length polymorphisms, 87-88, 90/-91/ P C R amplification inhibitors and repeat silica extraction, 88, 92 PCR amplification inhibitors in aDNA extractions, 85 Peru archeological obsidian sources, 522-552 Chiribaya Alta site, tuberculosis determination by D N A studies, 82 Conchopata, Wari site, trophy heads, geographic origins, 99-113 discriminating elements in obsidian sources, 543-549 ochre artifacts, instrumental neutron activation analysis, 480-505 Paloma site, human bone and teeth characterization by L A - I C P - M S , 292-294/

Wari ceramics, L A - I C P - M S analysis for characterization, 349363 Petoa, Santa Barbara, Honduras, ethnoarchaeological studies, 215 Pétrographie analysis Mesopotamian glazed ceramics, 434,436-437 sourcing Iron Age Philistine pottery, 412-417 Philistia and southern Israel, geography, 399-400/ 412 Philistia pottery, grouping by principal component analysis, 404-411 Philistine Bichrome pottery production, 419 Philistine Iron Age pottery from Israel, 399-421 Philistine Monochrome pottery production, 418 Phosphorus in soils, food preparation and consumption evidence, 215217,218/ Photography using non-visible regions of the electromagnetic spectrum, 24-25 Pictographs in Little Lost River Cave, black coating, surface analysis, 152-166 Pigments and dyes, general characteristics, 18—19 Pigments and infrared spectra, iron oxide, 67, 72/-73/ Plant and animal fibers, comparisons, 52-54/ Plant sources for dyestuff, 24 Plasma-chemical oxidation (PCO), radiocarbon dating, black coating, 153,164 Plaza spaces, prehistoric cooking and eating practices, 217, 218-228 Polymerase chain reaction. See PCR Portuguese origin, majolica pottery from Canary Islands by I N A A determination, 392



568 Pottery majolica, from Canary Islands, characterization, 376-399 Philistine, from Israel, sourcing, 399^21 See also Glaze and paint characterization Prehistoric populations, economic stratification, aDNA techniques, 8 1 82 Principal component analysis (PCA), 369 ochre artifacts from Jiskairumoko, I N A A data, 493,498/ Protein fibers, infrared spectra, 60, 63, 65/ Protocol testing accuracy L A - I C P - M S compared to I N A A , elemental analyses, Wari ceramics, 355-356/ L A - I C P - M S copper alloy analysis, 341,342/^343 Provenance research. See Source characterization; Sourcing Punic Carthage, history, 312 Puzolana source, obsidian, Peru, 535— 536 Q Quadratic regression model for elemental concentrations in obsidian artifacts, 513-514 Quispisisa source, obsidian in Peru, 535 Qumran and Isfiya coin hoards, chemical composition, 258-274 R

Repeat silica extraction and PCR amplification inhibitors, 88, 92 Repeatability, protocol testing, L A ICP-MS elemental analyses, Wari ceramics, 353, 354-355/

Reproducibility, protocol testing L A - I C P - M S compared to I N A A , elemental analyses, Wari ceramics, 354, 355 L A - I C P - M S copper alloy analysis, 341-342/ Roman Carthage curse tablets, lead isotope analysis, 311-335 Rubidium and zirconium concentrations in obsidian from Trinidad de Nosotros, 516/ Ruby Valley Pony Express Station, source of salt-glazed ceramic sherds, 455^156

Salt-glazed pottery from historic Latter-day Saint potteries, 455-456 Sample preparation obsidian samples, 530-531 skeletal remains for Sardin Sample selection, aDNA studies, 8 2 83 Sample selection and acquisition, Seip textiles, 32-34 Sampling criteria, sample preparation, skeletal remains for Sardinian prehistory diet studies, 120-123 Sampling strategy, strontium isotope analysis, 102 San Francisco convent at Las Palmas de Gran Canaria, majolica pottery site, 378-379 San Martin Jilotepeque, Guatemala, obsidian source, 510-511 San Vicente Xiloxochitla, Tiaxcala, Mexico, ethnoarchaeological studies, 213 Sand fraction, trace metal association in St Mary's County Chapel bricks, 369-370/ Sardinian prehistory, interpreting stable isotopic analyses, 120132



569 S A X S . See Small-angle x-ray scattering Scanning electron microscopy (SEM), 25 prehistoric textiles, 29 with energy dispersive spectrometry, Seip textiles, 35 Sebilong mine, Botswana, specularite sourcing, 464 Sediments, archaeological, microfocus small-angle x-ray scattering, 197— 200 Seip Mound, Ohio, archaeological textile colorants, 15-43,44-77 Seip textiles, 32-35 S E M . See Scanning electron microscopy Seville, production center, majolica pottery found on Canary Islands, 385-397 Shark teeth dating by ESR techniques, 10-13/ Shell bead sourcing, 167-193 Sherd surfaces, elemental contour maps by L A - I C P - M S , 289292 Sik'u '. See Trinidad de Nosotros Silver coins, Isfiya and Qumran coin hoards, chemical composition, 258274 Silver content in Tyrian shekels and half-shekels, political condition effects, 269, 271,273 Silver Lake and Sycan Marsh, Oregon, discriminating obsidian sources, 281-282, 283/ Siwalik Group, India, ESR crocodilian teeth and elephantid tooth dating, 5, 7-10,11/ Small-angle x-ray scattering (SAXS), microfocus, archaeological sediments, 197-200 See also X R D Social relations from soil chemistry, 215-217,218/

Soil chemistry, cooking and eating in Mesoamerican plazas, 210-230 Soil memory, 211-212 Soils and sediments, thin-section microfocus synchrotron x-ray scattering, diffraction and fluorescence analyses, 194-209 Song dynasty copper-based coins, chemical composition, E D X R F determination, 231-245 Source characterization, obsidian, systematic approach, overview, 523-525 Sourcing obsidian artifacts in western Mediterranean, 279-281, 283/ Sourcing specular hematite, discriminant function analysis, I N A A data, 466, 469-477/ Southern Africa mines. See Botswana prehistoric mines Spain. See Canary Islands; Castilian Kingdom; Iberian Peninsula Specular hematite from mines in Botswana, 460-479 Specularite. See Specular hematite Splash glazes in Mesopotamian pottery, 432,440-441/ St. Barbara's field clays as source for Chapel bricks, 372-373 St. Mary's City, brick Chapel building materials, characterization, 364-375 Stable isotopes, principles and interpretation, 115-117 Standardization in protocol testing, L A - I C P - M S elemental analyses, Wari ceramics, 352-353 Statistical grouping, chemical analyses, Philistia pottery, 404-411 Strontium isotope analysis archaeological enamel and bone, 102-104 by LA-TOF-ICP-MS, 298, 302, 304, 306-308 investigation, geographic origins of trophy heads, 99-113



570 overview for archaeology, 100-102 Strontium isotope ratios in the Andes, 104-108 Sulfur materials from Icelandic Norsetrading site, simultaneous coincident x-ray micro-fluorescence and micro-diffraction analyses, 204-205 Surfer, version 8.01, software, 225 Sycan Marsh and Silver Lake, Oregon, discriminating obsidian sources, 281-282,283/ Synchronous data acquisition, TOFICP-MS, 299

Tepe Tula, Neolithic site in Iran, 138, 139/ Ternary alloy, copper, tin, and lead, coins, 250-255 Terpane distribution patterns, chromatograms from modern bitumen seep, archaeological bitumen and pottery samples, 142— 146, 147/, 147/ Tetradrachms. See Tyrian shekels and half-shekels Texas, Hinds Cave, coprolites, human mtDNA extraction in dietary reconstruction, 81 Textiles, prehistoric, from eastern North America, colorant classification, 15-43 Thermal ionization mass spectrometry (TIMS), Roman Carthage curse table analysis, 315, 318 , 326-332/ Thin-section micromorphology for archaeological soil and sediment analysis, overview, 195-197 Tigris-Euphrates drainage network, 436 Time and flexibility, archaeological textile colorant testing protocol, 38

Time-of-flight inductively coupled plasma-mass spectrometry. See TOF-ICP-MS TIMS. See Thermal ionization mass spectrometry Tin-lead glaze coating, opaque-white, on Majolica pottery, 377 Tipuj, Guatemala, obsidian frequencies, 518 Titicaca Basin Type obsidian, 534 TOF-ICP-MS, lead isotope analysis, ceramic glazes, 427-429 Tools from obsidian, properties, 522523 Trace element abundances in curse tables, 332, 333/ Trace metal association with sand fraction in St Mary's County Chapel bricks, 369-370/ Trans coniferyl alcohol, 49-50/ Trans sinapyl alcohol, 49-50/ Transition metal model, discriminant fonction analysis, I N A A data, specular hematite sourcing, 468478 Trapped charge dating methods, 2-3 Trinidad de Nosotros in Central Petén lakes region, obsidian artifact location, 507-510 Trophy heads in central Andes, geographic origin, archaeological chemistry, 99-113 Tsodilo Hills mines, Botswana, specularite sourcing, 461, 462-464 Tuberculosis in Peruvian mummy, Chiribaya Alta site, by D N A studies, 82 Tunis, Tunisia. See Roman Carthage Tunisian lead ore isotope database, 326-327/ Tyre, Roman period history, 269, 271, 273 Tyrian shekels and half-shekels, chemical compositions, 258-274


571 U Utah, historic, pottery glazes, chemical analysis by LA-ICP-MS, 452-457 U V fluorescence photography, 24 U V reflected photography, 24 Uyo Uyo and Carylloma obsidian sources, Peru, 538


V Variability, ochre artifacts from Jiskairumoko, 501—502 Varian ICP-MS, quadrupole mass spectrometer, 337-338,351 Visual examination in colorant testing protocol, archaeological textiles, 36

W Wari ceramics, analytical chemical groupings by LA-ICP-MS and I N A A , 356-362 Wari heartland sites, food supply, 104 Wari realm, history, 350-351 Wari site, Conchopata, 99-113,350-351 Western Mediterranean prehistory, stable isotopes and diet, 118-120 Western Mediterranean sourcing obsidian artifacts, 279-281,283/ "Widow's mites" series, copper coins, elemental compositions, 246-257

X-ray diffraction (XRD) majolican pottery sherds from Gran Canaria Island, 383 microfocus synchrotron x-ray analysis method, 198-199/ Roman Carthage curse table analysis, 319, 332

See also Small-angle x-ray scattering X-ray fluorescence (XRF) field-portable equipment for obsidian sourcing, 506-521 majolican pottery sherds, 380-391/ microfocus synchrotron x-ray analysis method, 198-199/ obsidian analysis from Peru, discriminating elements, 547, 548/-549/ obsidian analysis procedure, 531532 obsidian chemical characterization, overview, 527-528 obsidian sourcing, Silver Lake and Sycan Marsh, 281-282,283/ theory and application, 260-262/ X-ray photoelectron spectroscopy (XPS), surface characterization, black deposit from Little Lost River Cave, 153-164 Xaaga, Oaxaca, Mexico, ethnoarchaeological studies, 214 XPS. See X-ray photoelectron spectroscopy X R D . See X-ray diffraction X R F . See X-ray fluorescence

Yanarangra obsidian source, Peru, 538

Zaragoza, Mexico, obsidian source, 512 Zinc-tin binary diagram, metal concentrations, Matisse bronze sculptures, 346 Zirconium and rubidium concentrations, Trinidad de Nosotros obsidian, 516/


LA-TOF-ICP-MS, 305-307

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