Pittcon Technical Program - ACS Publications - American Chemical

PITTCON T P

PITTCON T P ec h n ic a l

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Sunday, March 2, 2008, to Thursday, March 6, 2008 New Orleans

Sunday

afternoon

Development of a Field-Portable Nucleic-Acid-Based Sensor

Plenary/Award

HIV/AIDS-Related Diagnostics for Resource-Limited Countries, Room 272

Pittcon Heritage Award, La Nouvelle Orleans Ballroom C

Multi-partner Collaborative Approach to Diagnostic Assay Development CD4 Testing in Limited-Resource Settings: Where Are We Now? Liposome-Based CD4 Lateral-Flow Assay for HIV-Related Diagnostics Low-Cost HIV Viral Load Test (Cavidi ExaVir Version 3) Is Useful for Monitoring HIV Infection in Adults and Children Living in Remote Settings with Minimal Laboratory Facilities

Systems Biology and Systems Medicine

Symposia ACS Division of Analytical Chemistry: Environmental Impact of Hurricane Katrina on New Orleans and the Surrounding Area, Room 276

Characterizing the Dissolved Organic Matter within Katrina Floodwaters Chemical, Toxicological, and Benthic Community Analysis of Wetlands in the Greater New Orleans Area Sediment and Air Contamination inside Flooded Homes Advanced Bioanalytical and Chemical Techniques for Public Health Assessments Mold and Endotoxin Exposures Post-Katrina Astrochemistry: It’s Out of This World, Room 244

Chemistry in the Far Reaches of the Solar System: Expected and Unexpected In Situ Analysis of Rocks and Soils on Mars: α-Particle X-ray Spectrometer on the Mars Exploration Rover Mission Chemistry of Star Formation Identifying Molecules in Space: Combining the Analytical Power of Spectroscopy and Radio Astronomy Vibrational Astrospectroscopy Detection of Chemical and Biological Hazards in Food, Room 265

Rapid Nondestructive Spectral Imaging Technologies for On-line Food Safety Inspection Bioconjugated Nanoparticles for Bioanalysis and Bioseparation Nanobiosensors for Food Defense Bacteriophage, Bioreporters, and Bioluminescent Monitoring for Food Safety Assurance © 2008 American Chemical Societ y

HPLC on the Edge, Room 252

UHPLC in Capillary Columns Temperature: A Useful Parameter in HPLC Optimization and Method Development Comparison of the Performance of Some Modern HPLC Columns in the Separation of Complex Mixtures Extreme Separations Using Monolithic Columns Optimization of Peak Capacity Productivity in LC/LC through Design of High-Speed Gradient-Elution Chromatography New Strategies in Designing Fuel Cell Catalysts, Room 267

Application of SECM to the Rapid Synthesis and Screening of Electrocatalysts for Fuel Cells Metal–Metal Oxide Synergetic Effects in Oxygen Reduction Electrocatalysts: Investigations by SECM and RotatingDisk Voltammetry Effect of Pt Particle Size on the Kinetics of the Oxygen-Reduction Reaction From Mechanism to Design of New Catalysts for Oxygen Reduction Enzymes as Fuel-Cell Catalysts: Concepts and Principles

F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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Archaeology of the French Explorer La Salle’s 1684 Wrecked Ship La Belle: Artifact Preservation Using Polymers, Room 255

Pharmaceutical Outsourcing/Insourcing: Managing the Technical Process at a Third-Party Organization, Room 260

Artifacts and Science: Developing Polymers for Artifact Conservation Overview of the La Belle Assemblage: Conservation Challenges of Water-Logged Artifacts Conservation of Armaments: Strategies for Working on Composite Artifacts Conservation of Rigging and Cordage Conservation of a Miscellaneous Assemblage of Tools Conservation of Hair Conservation of Paper

Outsourcing Manufacture and Qualification of Pharmaceutical Reference Standards Successful Transfer of an HPLC Method-Development Procedure from a Pharmaceutical Laboratory into a ThirdParty Contract Analytical Laboratory Developing Successful Partnerships with Contract Pharmaceutical Organizations Accelerating Early-Phase Clinical Candidates in Big Pharma Making Data Available to Clients Real Time Pharmaceutical Outsourcing: A View from Both Sides Challenges for Development, Validation, and Transfer of Solid-State Analytical Methods: Using Laboratory-Workflow Analysis To Determine Critical LIMS Requirements

Organized contributed sessions ACS Division of Analytical Chemistry: New Directions in Analytical Instrumentation and Techniques, Room 243

Organic/Inorganic Hybrid Semiconductor Photocatalysts That Demonstrate Target Selectivity New Approach Using NMR To Directly Measure the Surface Area of Particulate Suspensions Determination of Enantiomeric Compositions of Analytes Using Novel Fluorescent Chiral Molecular Micelles and Steady-State Fluorescence Measurements Novel Tool for Sorting Spectral Files into Calibration, Tolerance Interval, and Validation Sample Sets for Use in Development and Validation of Individual Discriminate Partial Least Squares Material Discriminators Direct Deposition LC/FTIR: New Instrument for Structural Information about Minor Components and Polymers Fluid Steering in Microfluidic Devices with Chemical Valves and Inexpensive Magnets Simple Fabrication of Fritless Chromatographic Microchips Packed with Conventional Reversed-Phase Silica Particles and Small-Molecule Separations Internal Energy Deposited on Thermometer Molecules by Venturi-Assisted ESI and an Array of Micromachined Ultrasonic Electrosprays

Oral sessions Bioanalytical Applications of Fluorescence and Luminescence, Room 262

Fluorescent Hyperspectral Imaging of Biological Samples: Evaluating the Sensitivity of Our Quantitative Measurement Phthalocyanine-Based NIR Fluorescence Systems for SNP Detection Quantifying Affinities of Membrane-Associated Protein–Protein Interactions Using Ratiometric and FRET Imaging Liposomes Outperform Colloidal Gold, Enzymes, and Fluorophores as Analytical Reagents Fluorimetric Determinations of Nucleic Acids, Anions, and Oxygen Using Osmium Complexes Handheld Device for Fine-Needle-Aspiration Biopsy in Cancer Screening Recombinant Forms of Anionic Tobacco Peroxidase as Prospective Chemiluminescent Reagents Bioluminescent Dye-Doped Silica Nanoparticles for Targeting and Imaging Bioanalytical Electrochemistry I, Room 263

Nanotechnology Applications to Chemical and Biological Defense, Room 241

Emerging and New Nanotechnology for Chemical and Biological Defense Spectral Reproducibility in Surface-Enhanced Spectroscopies Multilayered SERS Substrate Geometries and Their Application to Chemical Nanoimaging Probes for Biological Agent Detection Studies of Electron-Beam Lithographically Prepared PillarSilver Nanodiscs as SERS Substrates SERS for Rapid and Sensitive Virus Detection U.K. Chemical and Biological Defense Applications of Nanotechnology SERS Technology Solutions for Rapid Trace-Level Detection of Chemical and Biological Agents Surface-Enhanced Raman Chemical Imaging of Bacteria 530

A n a ly t i c a l C h e m i s t r y / F e b r u a r y 1 , 2 0 0 8

Enhancing the Performance of Amperometric Assays Using a Novel Signal Processing Algorithm: Application to RapidSampling Microdialysis On-Chip LC Using In-Channel Electrochemical Detection Towards Multiplexed Electrogenerated Chemiluminescent Detection Simultaneous Determination of Ascorbic Acid and Hydrogen Peroxide Using Layered Metallo-polymer and Protein Films Effect of Dissolved Chlorine on an MS2 Bacteriophage Immunoassay as Studied by Electrochemical and Fluorescence Detection Cylindrical Pore Nanoelectrodes by FIB Milling of an Insulating Polymer: Toward Biological/Electrochemical Interfacing Development of a Novel Electrochemical Immunosensor for


West Nile Virus Rapid Measurements of Uric Acid at Pulmonary Artery Endothelial Cells Exposed to Oxygen Stress with a Nanostructured Carbon-Fiber Sensor Biofuels and Petrochemicals (half session), Room 269

Alternative Method for Analysis of Methanol in Biodiesel Optimization of a Biodiesel GC Separation Using Automated Method-Development Software Increasing the Performance and Robustness of High-Resolution Capillary Columns for the Analysis of Glycerides in Biodiesel Fatty-Acid Methyl Esters Derived from Palm Kernel and Palm Oil Feedstocks Use of ASE in Understanding Biomass Conversion Processes Cells on Microchips, Room 261

Tracking Bacterial Response to Chemical Gradients in Microfluidic Devices Monitoring Cellular Oxygen Consumption in Microfluidic Devices On-Device CO2 Control To Facilitate Microfluidic Cell Culture Cell-Culture Chip Using Low-Shear Mass Transport Addressing a Vascular-Endothelium Array with Blood Components Using Underlying Microfluidic Channels Continuous Low-Voltage DC Electroporation on a Microfluidic Chip with Polyelectrolytic Salt Bridges Lab-on-a-Chip: A Novel Approach To Estimate Toxicity of Nanoparticles Chemical Solution to Alternative Fuel Research, Room 270

DNA-Based Nanostructures as Nanomotor CO and Methanol Electrooxidation on Uniform AuNanoparticle Arrays in Alkaline Media: Role of Particle Size and Interparticle Distance Characterization and Quantification of Biofuels Using GC-FID/MS Analysis of Biomass Hydrolysates: Comparison of an HPLC/ ELSD Method with a Trisilylation/GC Method Impact of Sample Pathway and Storage-Vessel Composition on Mercury Recovery in Stack Gas and Natural Gas Streams GC × GC Analysis of High-Ethanol-Containing Motor Fuels Analysis of Residual Ethanol in Combustion-Engine Exhaust Gases Using Bioethanol Fuels by Thermal Desorption MicroGC Determination of Sulfate and Chloride in Denatured Ethyl Alcohol According to ASTM D 7319 Developments in GC, Room 264

Analysis of Bleed in GC Inlet Port Septum Unsymmetrical Dicationic Ionic Liquids: Manipulation of Physicochemical Properties Using Specific Structural Architectures Integration and Optimization of Hardware and Software for

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a Differential Flow Modulated GC × GC System Pulsed-Discharge Detector with Multiple Collecting Electrodes Planar Micro-Flame Ionization Detector with Integrated Guard Reversed-Phase Gas–Liquid Chromatography: New Frontier Axial Temperature Gradients in GC Miniaturized Atomic-Emission Detector Using RF Helium Plasma Equipped with Coaxial Micro-Plasma Torch for Portable GC Environmental Analysis of Metals (half session), Room 269

Application of Polyamic Acid for the Detection and Reduction of Toxic Cr(VI) Generating Selectivity in Ligand-Functionalized Microcantilever Arrays for Metal Ion Sensing and Identification Liquid–Liquid Extraction, Speciation, Preconcentration, Determination of Vanadium(v) with P-nitro Calix(6)arene Hydoxamic Acid SPE of Metals onto Capillary-Channeled Polymer Fibers Modified with Polyacrylic Acid with ICP-AES Detection LC at the Extreme: Ultrahigh Pressure and High Temperature, Room 245

High Efficiency Semi-Preparative LC at Elevated Temperatures Effect of Temperature on Solvent-Strength Linearity in RPLC Explore the Various Approaches To Evaluate the Stability and Lifetime of RP-HPLC Columns in High pH Conditions Theoretical Considerations When Carrying Out LC at Ultrahigh Pressure Achieving Optimum UHPLC Column Performance by Measuring and Reducing Overall System Dispersion Novel Ultrahigh Pressure LC Method for the Analysis of Vitamins in Cell-Culture Medium Evaluation of Diamond Particles as Stationary Phases for LC Nanoparticles in Biospectroscopy, Room 271

Gold Nanocluster: Enhanced Luminol Chemiluminescence in Neutral Solution and Its Analytical Application Design and Synthesis of Gadolinium Phosphate Particles as Novel MRI Contrast Agent and Application for Tumor Imaging Lanthanide-Based Nanocrystals as Fluorescent Markers for Bioassays Ratiometric Polyacrylamide Nanoparticle NO Sensors for Intracellular NO Imaging Carbon Nanotube Modification Making Molecular Beacons Biostable NIR and Related Techniques in Process Analysis, Room 274

Rapid, Calibrated, High-Resolution, Spectral Imaging Using Tunable Laser Source F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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Automated Grain-Analysis System New NIR Solutions To Satisfy Diverse Quantitative and Qualitative Analytical Needs Spectral Pretreatment for Brand NIR Instrument Standardization Part-Per-Million Sensitivity in NIR Spectroscopy: Methods for the Field Analysis of Low-Concentration Analytes Hyperspectral Identification of Fast-Moving Materials with a New High-Speed Chemometric Method Interferometric Noise Reduction in TDLAS by the Use of Diffuse Reflections Isotopic Ratio Analysis of Water by Cavity Ring-Down Spectroscopy for Application to Human Metabolic Studies

Symposium

Sample Preparation: General, Room 242

Single-Cell Enzyme Assays Subcellular Analysis of Single Cells Metabolic Cytometry: Sphingolipids in Single Cells Analyzing Cells Inside and Out Using Microfluidics and Capillary LC/MS Aptamers as Affinity Probes in Chemical Cytometry

Advances in Automated Sample Preparation Measuring Physicochemical Constants Using Headspace GC Active Single-Drop Microextraction for Simultaneous Extraction and Derivatization of Gaseous Diisocyanates Solid-Phase Extraction: Nanoparticles vs. Micrometer-Sized Particles New Applications of Accelerated Solvent Extraction From Alfalfa through Popcorn to Sweet: Analytical Chemistry of Rice Flavors Cryogenic Modulation for Near-Real-Time Vapor Analysis Integration of Analytical Chemistry into the Polymer Platform and Product Planning

Monday

morning

Awards Chromatography Forum of Delaware Valley Dal Nogare Award, Room 252

Random Walk through LC High-Speed HPLC: Increasing Speed in HPLC Analytical Separations as Molecular Interaction Amplifiers Chiral Recognition Mechanisms: Case of the Macrocyclic Glycopeptides Selectors Understanding Chromatographic Surfaces: An Interdisciplinary Approach Pittsburgh Conference Achievement Award, Room 255

High-Resolution Tandem MS of Intact Protein Ions Gaseous Protein Confirmations versus Native Solution Structures Reaching New Heights in Top-Down Proteomics Pushing the Biological MS Envelope: Benefits of Accurate Mass Measurement for MS and MS/MS of Proteins and Lipids Probing the Catalysts of Polyketide Synthases by FTICR MS Cracking the Histone Code Using MS-Based Proteomics

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ACS Division of Analytical Chemistry: Interdisciplinary Analytical Chemistry, Room 276

Systems Biology, Analytical Chemistry, and the New Medicine Achieving Scientific Goals through Integration: Genetic Engineering in Biosensing and Micro/Nanoanalysis Polymer Electronics for Chemical Sensors From Nuclear to Analytical Chemistry to Clinical Studies on Cardiovascular Disease Chemical Cytometry: Chemical Analysis of Single Cells, Room 272

From Bench to the Bedside: Novel Analytical Techniques That Will Impact Healthcare, Room 267

Spectroscopy in Medicine: Path to Clinical Relevance Engineering Practical Protocols and Models for Histopathology of Human Tissues Using IR Spectroscopic Imaging Vibrational Microscopy and Imaging: Applications to Skin Pharmacology, Biochemistry, and Biophysics Planar Array IR Spectroscopy: Prospects for the Detection of Proteins at Physiologically Relevant Concentrations Coherent Anti-Stokes Raman Scattering Microscopy: Chemically Selective Imaging for Biology and Medicine High-Throughput Analysis in the Pharmaceutical Industry, Room 265

Strategies for Increasing Bioanalytical Throughput for Drug Discovery and Development Support High-Throughput Bioanalysis by LC/MS/MS in Pharmaceutical Industry Low-Volume, Parallel LC: Novel Approach to Overcoming Analysis-Time Constraints for Analytical Applications in the Pharmaceutical Industry Increasing Throughput in the Discovery ADME/PK Screening Arena: MS Strategies and New Technology Advances in Capillary and Nano HPLC Technology for High-Throughput Drug and Biological Sample Analysis Recent Developments in the Separation of Spent Nuclear Fuel, Room 244

Interaction of the Light Actinides with Peroxide: Ternary Actinide Peroxide–Carbonate Complexes in Solution and Solid State for Advanced Separation Chromatographic Materials for the Separation of Trivalent Lanthanides from the Minor Actinides Separations, Coordination, and Solvation of F-Elements in Ionic Liquids


Actinide–Lanthanide Separations in Advanced Nuclear Fuel Cycles: TALSPEAK in Context Historical Perspectives on the Separation of Spent Nuclear Fuel

Organized contributed sessions Analytical Methodologies Applied as Environmental Remediation Strategies, Room 262

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Dual-Electrode Biuret-Based Peptide Detection following Capillary HPLC Application of FSCV to in Vivo 5-Hydroxytryptamine Monitoring Voltammetric and Behavioral Analyses of Novel Transgenic Huntington’s Disease Model Rats Measurements Using Electrodes with Nanometer-Scale Separations in Ionic Solutions

Microbial Metabolite Production for Enhanced Subsurface Redox Activity and Contaminant Immobilization Overview of Environmental Remediation Technologies Developed by the DOE Permanganate Natural Oxidant Demand: A New ASTM Protocol In Situ Metal Sequestration by Ureolytic Microbial Calcium Carbonate Precipitation Use of Apatite for Chemical Stabilization of Contaminants in Soils and Sediments Non-hazardous Automated Colorimetric Method for Nitrate Analysis Oxidation–Reduction Reactions Influencing the Transformation of Mixed Contaminants in the Presence of Zero Valent Iron and Biofilms Evaluation of the Applicability and Effectiveness of Organoclays as Active Capping Materials

Oral sessions

Ionophore-Based Chemical Sensors I, Room 271

Applications of Fluorescence and Luminescence, Room 264

Mathematical Model of Current Polarized IonophoreBased Ion-Selective Membranes: Large-Current Chronopotentiometry Beyond Sensing under Equilibrium: Photoresponsive Nanoprobes for Rapid, Localized Acid-Based Titration Toward Robust All-Solid-State Polymeric Ion Sensors Electrochemical Sample Matrix Elimination for Trace-Level Potentiometric Detection Bioassays with Potentiometric Detection All-Solid-State Sodium, Potassium, and Chloride Ion-Selective Electrodes in Blood Serum Analysis under FlowThrough Conditions New Solid-State Ag/AgCl Reference Electrodes Based on Gelled Hydrophobic Ionic Liquids Toward a Design for Particles To Resolve Intracellular Ion Concentrations

Affinity Probes: Bioseparations, Room 270

Novel CE with Laser-Induced Fluorescence Detection Assay for Measuring Protein Palmitoylation Selective Analysis of VEGF and VEGF Peptide Variants by Aptamer-Based Affinity-Probe CE Generation of an Aptamer Antidote for an Anticoagulant Competitive Immunoassay Methods for Detection of Metabolites and Proteins Using Micromosaic Patterning Capillary-Driven Flow Chip for Simple and Quick SPR Measurement Preparation of Highly Integrated Molecular Structure for the Open-Channel Micro-Total Analysis System with Ink-JetDispensed Nanodroplet Rapid Identification of Pathogens in Food Samples Using Simplified Immunoassay System

Extending the Spectral Range of Fluorescence Instrument Qualification into the UV and NIR Development of Size-Controllable Luminescent Silica Nanoparticles Using Reverse Microemulsion Fluorescence Imaging Analysis and Systems Applied to Water Chemistry Carbonic Anhydrase Encapsulated Nanoparticles as Zinc Biosensor Gold Nanoparticle-Based FRET for Bioassay Development Trace Analysis Using Laser-Induced Fluorescence with Tunable Laser Facile Procedure for Preparing High-Quality CdTe Quantum Dots in Aqueous Solution and Application of As-Prepared Quantum Dots for Determination of Copper(II) Ions Rapid Fuel Test

SEAC Organized Session on Electrochemistry, Room 245

Bioanalytical Applications of MS, Room 263

Characterization of Catecholamine Secretion in Murine Adrenal Slices Using Fast-Scan Cyclic Voltammetry and Constant-Potential Amperometry Electroanalytical Methods in Understanding Developmental Disorders Spatial and Temporal Analysis of Naturally Occurring Dopamine Release in Freely Moving Rats Anodic Voltammetry and Spectroelectrochemistry of dsDNA as a Way To Examine DNA Interactions with Drugs and Conformation Change

Gas-Phase Ion–Electron Reactions for the Structural Characterization of Oligosaccharides Discovery of DNA Affinity Binding Ligands Inspired by G-Rich Oncogene Promoter Regions Analysis of Toxic Species Including Mercury Species and Mercury Glutathione Complexes Using SIDMS with Nanospray TOFMS Detection MS Imaging of Small Molecules Using Laser Desorption/ Ionization MS Characterization of Macromolecular Protein Assemblies by F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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Surface-Induced Dissociation: Expanding the Role of MS in Structural Biology Electrophoretic Separation with High-Throughput MALDI MS Detection and Quantification for Polypeptide Profiling in Biological Tissues Demonstration of a Novel Methodology for Sub-Microsecond Hydroxyl Radical Protein Footprinting by Electron Beam Pulse Water Radiolysis Ionic Liquids for Use as Matrices in MALDI MS Bioanalytical Electrochemistry II, Room 260

Improvement of Electrochemical Determination of Some Drugs at Surface-Modified Electrodes Sensitivity Enhancement and Ion Distribution from Electrochemical Processes in ESI MS of Biological Metabolites Investigating Inhibition of Cytochrome P450cam Genotoxic Metabolites with an Electrochemical Layer-by-Layer DNA Sensor Simultaneous Real-Time Detection of pH and Histamine Release from Gastric Glands in the Stomach Electrochemical Detection of Dopamine at PC12 Cells Demonstrates That Estradiol Inhibits Depolarization-Induced Exocytosis via Phospholipase A2 Temperature-Dependent Changes in Sympathetic Neuroeffector Transmission in Mesenteric Arteries in Hypertension Environmental Samples and Preparation I, Room 236

Multiple Path Sampling via Rapid Sample Stream Switching for Air Monitoring Applications Method Development for Extraction, Cleanup, and Separation of Organic Pollutant in Extract of Contaminated Environmental Sample New Sample Transfer Technique by Internally Expanded Desorptive Flow for Needle-Trap Devices Advanced Automation of SPE Methods Development of the Needle-Trap Device as Time-Weighted Average Diffusive Sampler Development and Evaluation of Needle-Trap Devices Certified for Automation, a Replacement for EPA 1664A Development of a Syringe-Pump-Assisted Purge and Trap Technique for Needle-Trap Device Food Science: UV–Vis, NIR, AA, LC, GC, and Electronic Nose, Room 242

Quantitative Analysis of Phenolic Content and Antioxidant Capacity of Soy Hull Extract Rapid Classification and Quantification of Raw Materials and Adulterants in Pet Food Manufacturing Supplies Determination of Toxic Metal Ion Concentrations in FlameTreated Meat Products Direct Determination of Metal Ions in Wine and Fruit Juice Samples Using Internal Standardization and Fast Sequential Multi-element Flame AA Spectrometry Analysis of Bound and Free Amino Acids in Foods and Feeds Dynamic Headspace To Detect Aromas in Juices and Juice Drink 534


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Development of a Rapid Headspace Solid-Phase Microextraction GC/TOFMS Method for Aroma Profiles Part I: Method Development and Compound Identification Predictive Fermentation Monitoring in Industrial Food Production with an Electronic Nose Microsystem FTIR: Reflectance/Imaging/Chemometrics Applications, Room 261

UV Radiation Effects on Reflectance FTIR Microscopy of Clean B. subtilis Spores ATR-FTIR Spectroscopic Imaging for the Study of Fingerprints Spatial Resolution in IR Reflectance Imaging: NIR, Mid-IR, and ATR Thermal Processing of Protein on Optical Substrate Reveals Structural Changes via FTIR Microspectroscopy Field-Based Determination of Water for Condition Monitoring of In-Service Fluids by FTIR ATR-FTIR Coupled with Multivariate Least Squares Modeling To Understand the Fundamental Adsorption Properties of Polyelectrolyte/Surfactant Mixtures at the TiO2/ Water Interface Novel Techniques for Identification of Mixtures Using FTIR and Raman Spectroscopy Advanced Multiple-Angle Incidence Resolution Spectrometry for Thin-Layer Analysis on a Low-Refractive-Index Substrate Fuel Characterization and Analysis: Present and Future, Room 241

FTICR MS Coupled Off-line with LC for Structural Studies of Heavy Sulfur Aromatic Compounds in Petroleum Quantitative Determination of Corrosive Sulfur in Mineral Insulating Oils with IC, HPLC, and CZE Chemical Transformation for Structural Elucidation of Large Organic Compounds Advances in Characterizing Asphaltenes Combining Macroand Micro-ATR-FTIR Imaging Classification and Prediction of Jet Fuel Properties by NIR Spectroscopy Simultaneous Determination of Hundreds of Petroleum Components through the Use of Spectral Accuracy with FI-TOF MS Characterization of Hydrocarbon Fractions in Petrochemical Samples by Automated On-line HPLC+HRGC/MS Multidimensional System Predicted Fuel Properties from Raman Spectra Using Chemometrics General Interest: LC/GC, Room 269

Development of a New Series of Low-Bleed, High-Inertness Capillary GC Columns through Improved Deactivation Chemistry and Stationary Phase Synthesis Improving Durability and Selectivity of Silica-Based Stationary Phases for Use in High-pH Applications Selectivity Comparison of Cyclodextrin-Based Capillary GC


Stationary Phases Characterization of Phosphonium Ionic Liquids through a Linear Solvation Energy Relationship and Their Use as GLC Stationary Phases Reliable Determination of Trace Compounds with a Newly Developed UV–Vis Detector Using Stationary Phase Selectivity To Optimize UHPLC Analyses Novel Advances in Traditional GC Stationary Phases Influence of Eluent Quality on Gradient HPLC Separations HPLC: Pharmaceutical Applications, Room 349

New Weak-Anion-Exchange/Reversed-Phase, Mixed-Mode Column and Its Use in Pharmaceutical HPLC Analysis High-Throughput Method in Support of Cleaning Validation Studies Using Ultra Performance LC with UV and MS Detection Analysis of Cationic Liposomes by HPLC with Evaporative Light-Scattering Detection Analytical Tools for Early Phase Drug Product Development Determination of the Chiral Conversion of Drugs in Biologic Fluids on New Ram-Chiral Columns by HPLC Evaluation of Performance of a New Generation of Polysaccharide-Based Chiral Stationary Phases for HPLC and SFC Effect of Trace Amount of Water in the Mobile Phase of Normal-Phase Chiral HPLC on Selectivity and Resolution of Optical Isomers Efficient Development of Chiral Chromatographic Methods Sensors I, Room 350

On-site Vapor Detection of Chemical Warfare Agents by Monitoring Tape Method Miniature, Handheld, Close-Range, Solar-Blind, Standoff Explosives and Biological Materials Sensor Determination of H 2S and Organosulfur Compounds in Hydrocarbons by Differential Ion Mobility Spectrometry On-line Detection of Contaminations in Drinking Water by a Combined Electronic Micronose and Optospectrometric System Aptamer–Metal Surface Binding Interactions Stochastic Detection of Monovalent Cations in Ionic Liquids Microfluidic/Nanofluidic Sensors Using Catalytic DNA for Heavy Metal Detection Development and Optimization of Molecular Beacons as Biosensors for Surface Hybridization Using Lock Nucleic Acid

Monday

afternoon

Award Ralph N. Adams Award in Bioanalytical Chemistry, Room 272

Biochemical Individuality, Health, and Disease: New Opportunities for Bioanalytical Chemistry

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Improvements in Methods for in Vivo Detection of Neurotransmitters Bioanalysis of Hoosiers and Tar Heels Analytical Methods for the Investigation of Peptide Transport and Metabolism at the Blood–Brain Barrier Multidimensional LC/MS for the Analysis of Complex Mixtures of Proteins

Symposia ACS Division of Analytical Chemistry: New Perspectives in Optical Sensing—From Ions to Molecules and Beyond, Room 252

Development of Fluorescence Sensors for Real-Time Monitoring of Zinc Release Events in Pancreatic Cells Optoelectronic Sensing of VICs with Organic Nanobelts and Nanowires Computationally Driven Design of Photoinduced ElectronTransfer-Based Sensors Integrated Nanosensors Using Porous Photonic Crystals Fluorescence Imaging of Biological NO and Mobile Zinc Best Practices for HPLC Method Development in Pharmaceutical Analysis, Room 265

Modern HPLC Method Development: Overview of Fundamentals, Advances, and Column Selection Development and Use of Orthogonal Methods for Impurity Profiling of Pharmaceuticals by HPLC Selecting an “Orthogonal” Column during HPLC Method Development Challenges for Method Development at the Discovery/Development Interface: Balancing Speed with Practical Application Strategies for Utilizing Fast LC in Method Development Mobile Micro- and Nanoinstruments, Room 267

Mobile Instruments: Fast, Cheap, and under Wireless Control Totally Self-Contained GC/Toroidal MS for Field Application Life on a Chip: Integrating the Animate and Inanimate Worlds Miniaturized MS Microfabricated Bioanalysis Systems for in Situ Detection of Organic Biomarkers on Mars Novel Biospectroscopy for Amyloid Diseases, Room 244

Polymorphism in Amyloid Fibrils and Their Assembly Intermediates: Moving Target for Structural Analysis Flow-Induced Alignment of Amyloid Fibrils Revealed by Linear Dichroism Structure Determination of Amyloid Peptides and Proteins Solution-State Protein Fibril Development Monitored by Large VCD Intensities H/D Exchange Deep UV Resonance Raman Spectroscopy for Characterizing the Cross-Core Structure of Amyloid Fibrils F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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Science for Art, Room 255

Disaster Response and Recovery: Role of the Chemist Technical Analysis of Three Paintings Attributed to Jackson Pollock Characterization of Environmental Impacts on Cultural Property Surface and Beyond: New Insights in Old Glass Bugging Bugs: Tracking Insect Infestations in Cultural Artifacts 19th James L. Waters Annual Symposium, Room 276

DNA Sequencing

Organized contributed sessions Environmental Characterization and Management of High-Level Radioactive Waste, Room 245

Immobilization of High-Level Defense Waste at the Savannah River Site Corrosion Control Strategies for High-Level Nuclear Waste Tanks Separation and Purification and β-Liquid Scintillation Analysis of Sm-151 on Savannah River Site and Hanford Site DOE High-Level Waste Rapid Methods for Environmental Radiochemistry In Situ pH Adjustment To Minimize Migration of Metals and Radionuclides in Groundwater Hanford Tank Waste Sludge Characterization: Navigating the Analytical Maelstrom Hanford Tank Waste Sludge Characterization: Bridging the Gap between Analytical Results and Composition Rapid Radionuclide Remediation Ionophore-Based Chemical Sensors II, Room 271

New Picture of Ionic Secretion from Epithelial Cells Obtained in Vitro Using Ion-Selective Electrodes and Quantitative Mass Transport Reconstruction Photocontrolled Binding and Release of Guest Species at Spiropyran-Modified Surfaces Receptor-Based, Solvent-Free Extractions for the Development of Fluorous Solid-Phase Microextraction Ionophore-Doped Ion-Selective Electrodes (ISEs) with Perfluorinated Polymeric Matrixes All-Solid-State Reference Electrodes: Choosing the Right Membrane Matrix Direct Measurement of Total Calcium in Physiological Fluids with Pulsed Chronopotentiometry at Polymeric Ion-Selective Membranes Chemical Sensors Based on Chemical Sensing Probes and Devices Fine-Tuning the Behavior of Ion-Selective Electrodes

Oral sessions

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’Omics: Proteomics, Lipidomics, Metabolomics, Room 263

Phospholipid Profiling of Yeast Comprehensive and Comparative Analysis of Phospholipid Profile of Mammalian Tissues from Mice Fed Different Diets by MALDI-FTMS Multianalyte Analysis Using Electrode Array Detection and Microchip CE Extracting Biological Significance from NMR-Based Metabolomics Data Novel Electrochemical Array Detector with Enhanced Selectivity for Microchip CE Achieve Class Separation, NMR-Based Metabolomics pHResponsive Protein Microcompartmentation in Synthetic Cytoplasm Application of High-Resolution Multireflecting TOFMS with ESI for Metabolite Profiling Advances in Separation Science I, Room 270

On-line SPE/LC/MS for Ultratrace Analysis of Antibiotics in River- and Groundwater SPE under Hydrophilic Interaction Conditions: Novel Approach for Sample Preparation Preconcentration and Separation of Cr(III) and Cr(VI) Using Sawdust as a Sorbent Nucleotide Ion Exchange with Surface-Confined Ionic Liquid Stationary Phases Quantification of Neomycin B, Neomycin C, and Apramycin in Animal Feeds by LC Fluorescence Detection with Post-Column Derivatization Formation of Ion Exchangers on Graphitic Carbon Phases through in Situ Generation of Diazonium Precursors LSER Characterization of a Novel Zwitterionic Stationary Phase for HPLC Electrochemical Degradation of Quercetin: Isolation and Structural Elucidation of the Degradation Products Affinity Probes: Sensing, Room 243

Aptamer-Based Assay on Lateral Flow Strip Evaluation of Pyrroloquinoline Quinone Doped Polymeric Micro/Nanospheres as Sensitive Labels for Binding Assays Optimization of Antibody-Conjugated Magnetic Nanoparticles for Immunoassays Genome-Inspired DNA Binding Ligands for Insulin and IGF Proteins Aptamer-Conjugated Nanoparticles for Cancer Biomarker Studies Single-Molecule Detection: Observing Intracellular and Extracellular Molecular Interactions Fluorescence Correlation Spectroscopy for the Investigation of Aptamer/Receptor Interactions on Cell Membranes Lab-on-a-Chip Biosensor for Glucose Based on a Packed Immobilized Enzyme Reactor


Analyzing Cellular Components with Microfluidics, Room 264

Amperometric and Fluorescent Monitoring of Release from Cells in a Network Patterned with Sucrose Lift-Off Lithography Fully Integrated Microfluidic Device for Performing Cell Lysis with Real-Time CE/Electrospray MS Detection of Proteins from Single Cells Optimization of Laser-Based Sampling and Immunolabeling for Single-Cell Analysis by CE Parallel Monitoring of Cellular Secretions on a Microfluidic Chip Microfluidic Devices To Characterize the Cell–Cell Signaling Molecules Released from Neurons with Off-Line MS Exploitation of Laminar Flow for Cell Assays on a Chip Development of an Automated High-Throughput Microfluidic Device for the Study of Single-Cell Kinase Activity Developments in Data Analysis and Methodology (half session), Room 241

Software Tools for Formulation Development: Beyond the Spreadsheet Automation of Spectrophotometric Titrations Differentiation of Emerald Origins Using X-ray Spectroscopy and Chemometrics Laboratory Startup and Renovation: Tips for Success Developments in Sensors and Imaging (half session), Room 241

Widely Tunable DFB Lasers for Sensing Applications Spectroelectrochemical Detection of [Re(dmpe)3+] IR Imaging: Responding to Challenges in Sample Analyses Thermography: Moving beyond Predictive Maintenance to Product Development, Industrial Imaging, and Marketing Innovation in Sequencing and Genetic Analysis, Room 242

RCA-CE Assay for Sensitive DNA Detection High-Throughput, Continuous-Flow, Real-Time, Quantitative PCR Device Low-Voltage Microfluidic Electrochemical Reactor for Alkaline DNA Dehybridization and SNP Detection Continuous-Flow, Microfluidic Reactor for Gene Expression Analysis and Quantification at the Single-Molecule Level Electrochemical Genosensor System with the Disposable Electrochemical Printed Chips for Disease Diagnosis and Food Verification from Unpurified Amplicons Modular Microfluidic System for Alu Element Sequencing LC/MS: Software and General Applications, Room 269

Chromatographic Method Development: Approach Incorporating UPLC, MS, and Modeling Software To Streamline the Process of Creating Robust Methods Identification and Examination of Thermal Degradation Products of Pharmaceuticals by HPLC/TOF/MS Understanding the Cytotoxic Effects of Quercetin on Can-

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cerous Cells Characterization of Organic Matter in a Waste Landfill Leachate: SEC/LC/MS and Liquid/Liquid Extraction Comprehensive Selenium Speciation Analysis of Selenium-Enriched Samples through LC/Particle-Beam MS Robust Microwave Extraction Protocol for the Determination of Mercury Species in Fish and Tissue Samples Automation of Thin Film SPME for High-Throughput Drug Analysis Using Robotic Autosampler Determination of Heavy Metals and Their Species in Inorganic and Organic Fertilizers Using Microwave-Assisted Extraction and IC/LC/ICPMS Detection LC: Specialized Applications I, Room 349

Achieving High-Speed HPLC Performance at Moderate Pressures New Cation-Exchange/Reversed-Phase, Mixed-Mode Stationary Phase and Its Application for Separating Pharmaceuticals High-Resolution HPLC Performance under Both Isocratic and Gradient Conditions Monolithic Diamond Materials for LC Application of Unusual Solvents in 2D LC Reversed-Phase LC Stationary Phase Designed for Separating Basic Substances under Acidic Conditions Reversed-Phase Column Selectivity Triangle Based on the Snyder Hydrophobic Subtraction Model New HILIC/Reversed-Phase Mixed-Mode Column and Its Applications MS: Sample Preparation/Method Development, Room 262

Quantitative Isobaric Labeling for Isomeric Glycans Analysis ESI MS for the Investigation of Modified Gold Monolayer Protected Clusters MS Using Single-Photon Ionization Coupled with Thermal Analysis Binding Constant Determination by ESI MS Titrations To Screen Enantioselective Interactions between Macrocyclic Antibiotics and Amino Acid Derivatives Characterization of Oak Flavor Compounds Using Ion Trap GC/MS/MS Dynamic Method for MS Determination of In-Cylinder Oil Evaporation Neurochemistry, Room 260

Using High-Speed Chronoamperometry To Determine Native Serotonin Transporter Function in Human Lymphoblasts Amperometric Measurements of Transmitters Released from Single Vesicles in MN9D Dopaminergic Cells Evaluation of Calcium-Dependent Dopamine Release in Synapsin Triple-Knockout Mice Investigating Nonvesicular Dopamine Release in the Mouse Striatum with Fast-Scan Cyclic Voltammetry Electrochemical Comparison of Dopamine Release and F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

537


Uptake in eGFP Transgenic Mice and Wild-Type Mice Probing the Effect of Elevated Extracellular Dopamine Concentration on D2 Receptors’ Functionality In Vivo Electrochemical Monitoring of Norepinephrine Release in the Rat Anteroventral Thalamic Nucleus Examining Vesicular Release from Midbrain Dopamine Neurons with Amperometry and Fluorescent Calcium Imaging Raman, FTIR, and Related Techniques, Room 261

Sum-Frequency Generation Nonlinear Optical Ellipsometry Mechanistic and Kinetic Studies of Crystallization and Polymorphic Phase Transition in Small Organic Molecular Crystals by Terahertz Spectroscopy Evaluation of the Effects of the Use of Different ATR Accessories on Spectral Comparison Evaluation of Methods for Collecting Representative Raman Spectra from Heterogeneous Samples Principal Components Analysis Applied to Photobleaching in Raman Spectroscopy Raman Database and Spectral Classification of Minerals Assessment of Effective Fluoridation of Dental Enamel by Means of Raman Scattering Overview of Quantitative Analysis Using Raman Spectroscopy Sample Preparation: Bioanalytical, Room 350

Minimizing Tissue Damage in Electroosmotic Sampling Capillary-Based Porous Polymer Monoliths for Collecting Neuropeptide Releasate Further Advancement on Development of Immunoaffinity SPME Probes: Comparison of Different Types of Antibodies Electroosmotic Sampling from Hippocampal Cultures Advances and Challenges in Automation of Speciation for Biological Applications Development of High-Spatial-Resolution Solid-Phase Microextraction Preparation and Its Analytical Application of Molecularly Imprinted Nanoparticles and Nanofibers Development and Optimization of C18-Based Coatings for Solid-Phase Microextraction

Tuesday

morning

Award Pittsburgh Analytical Chemistry Award, Room 272

Nontraditional Separation Techniques Features of a Micro-GC Based on Sorptive Extraction and Plasma-Emission Detection Recent Advances in Analytical Glycobiology Microfluidic Technologies with MS Detection: Attractive Approach for Biomarker Discovery Applications New Types of Ion Traps Using Planar Non-Equipotential Electrodes 538


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Symposia ACS Division of Analytical Chemistry: Analytical Chemistry for Crime Scene Investigation I, Room 276

Analytical Chemistry and Forensic Science: Requirements for Credibility and Reliability Exist at the Crime Scene, in the Laboratory, and in the Courtroom Application of a Portable Raman Spectrometer for the Confirmation of Chemical Identification in the Field Trace Evidence Challenges for Forensic Analytical Methods New Forensic Analytical Methods for Latent Blood, Fingerprint Detection, and Trace Residues Advances in Analytical Methods for Characterization of Complex Petroleum and Biofuel Molecules, Room 252

Petroleomics: Chemistry of the Underworld Molecular Characterization of Heavy Petroleums Applications of 1H-NMR to Biodiesel Research Hydrocarbon Analysis with the Supersonic GC/MS: Novel Concept of Isomer Abundance Analysis HPLC with Diode Array UV–Vis Adsorption Detection for the Analysis of Polycyclic Aromatic Hydrocarbons in Complex Fuel-Product Mixtures Art, Cosmetics, and Medicine in Ancient Eras: The Analytical Chemist’s View, Room 255

GC/MS Studies of Modern Oil-Based Artists’ Paint Media Nanotechnology for the Conservation of Cultural Heritage Leonardo da Vinci’s Mona Lisa Uncovered Beyond the Decoding of the Hair Color of Pharaoh Ramses II Medicinal Properties of Egyptian Makeup Revealed by Microelectrochemistry Cellular Assays in Microfluidic Systems, Room 244

Microfluidic Devices for Studying Bacterial Function and Response Tracking Signaling in Single Cells Subcellular Analysis Using Microfluidic Systems Luminescent Quantum-Dot FRET-Based Protease Probes in Microfluidic Channels Current Status and Trends of LC/MS n Application in Trace-Level-Impurity Identification in Pharmaceuticals, Room 265

Impurity Identification: More Information and Fast Decision-Making with Increased Sampling and Control LC/MSn Analysis of Impurities in Drug Products and Drug Substances: Current Status, Strategies, and Case Studies Using Unit Resolution and High-Resolution MS Evaluation of the Importance of Accurate Mass, Mass Resolution, and Dynamic Range for Impurity-Profiling Applications Using Multistage MS Reaction Monitoring and Impurity Analysis for Drug-Substance Synthesis LC/MS, LC/MS/MS, and H/D Exchange Methodologies


for Structural Characterization of Impurities and Contaminants in Pharmaceuticals Miniature/Micro Gas Sensors for Biological and Biomedical Applications, Room 267

Planar Microchip-Based Multiarray Sensor for Simultaneous Measurement of Oxygen, NO, Lactate, and Glucose Colorimetric Sensor Arrays Electrochemical Detection of Molecules Regulating Cerebral Blood Flow Cross-Reactive Sensor Arrays for Forensic Applications S-Nitrosothiol Sensors Based on Miniaturized Amperometric Nitric Oxide Probes: Design and Biomedical Applications

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Hydrophilic Interaction Chromatography in Pyrimidine Anticancer Drug Development Ultrasensitive Anion Analysis Using ESI-MS and LC/ESIMS in the Positive-Ion Mode Evaluation of Pathways Associated with Benzo[a]pyrene Carcinogenesis via Quantification of Multiple DNA Adducts Using LC/MS/MS Detection of Nitro Compounds in Tobacco Smoke and Diesel Exhaust Using GC/Electron Monochromator MS Application of a Novel Fused-Core Silica Particle for LC/MS Analysis

Oral sessions

Organized contributed sessions

Advances in Atomic Spectroscopy Capabilities, Room 260

ACS Division of Analytical Chemistry: Aptamers in Separation Science, Room 243

In-Torch Vaporization ICP-AES with a Charge Injection Device Area Sensor Detector and Its Application to Rapid Determination of Stoichiometry of Quantum Dots Development of an ICP/ESI Dual-Source TOFMS for Rapid Speciation and Metallomic Analysis Temperature-Related Stability in Plasma Spectrometry Characterization of a Sr-90 Source Expanding the Limits of Closed-Vessel Microwave Sample Preparation Simultaneous Multiple Element Detection by LCPB/HC-OES AAS: Answer to Food Regulatory Compliance Using New Technology Carbon-Related Matrix Effects in ICP-AES

Nucleic Acid Aptamers as Target-Specific Chiral Selectors: LC and CE Applications Proteomic Pathway to Discovery of DNA Binding Ligands Aptamers Selected from Live Cancer Cells Selection Methods for Nucleic Acid Affinity Reagents Separation of Proteins Using Affinity Aptamers Using CE-SELEX for the Selection of Cell- or OrganelleBinding Aptamers Detection of Ricin Using Aptamers and Affinity-Probe CE Isolating Aptamers Using Micro-Free-Flow Electrophoresis Analytical Challenges in the Food Industry, Room 261

Implications of Analytical Advances for Product Safety Decision Making Analytical Challenges in the Contract Laboratory in Support of the Food Industry Confirming Safety, Quality, and Authenticity of Ingredients on Time and on Budget Identification, Confirmation, and Quantification of Allergens in Foods Recent Advances in Extraction of Hydrolyzed Food Samples Using Accelerated Solvent Extraction Dietary Fiber: The Challenge of Quantitating a Diverse Mixture Development of a Low-Bleed Stabilized Polyethylene Glycol Capillary Column Determination of Multiclass, Multiresidue, Sulfur-Containing Antibiotics in Animal Tissues Using Integrated Pulsed Amperometric Technique following HPLC

Advances in Separation Science II, Room 270

Chiral Separation Mode Screening in Pharmaceutical Method Development Using Multiparallel Microflow LC Development of New HPLC Chiral Stationary Phases Based on Ruthenium(II) Polypyridyl Complexes Performance Optimization in Electric Field Gradient Focusing Strategies for Assessing Mass Balance in Partially Degraded Samples Development of Analytical Methods To Facilitate the Identification and Structure Elucidation of Heparin-Derived Oligosaccharide Substructures High-Performance 1D and 2D Microfluidic Separations Programmed Elution and Peak Profiles in Electric Field Gradient Focusing Optimization of Steady-State Recycle SSR Parameters Utilizing Polarimetry in Chiral Separations

Applications of Novel Chromatography Coupled to MS Methods, Room 245

Bioanalytical Separations I, Room 263

Analysis of Endometrioid Ovarian Adenocarcinoma Using Microseparation Coupled with MS Effects of Gas Contaminants on Column Life and Consistency of Results Monolithic Material as On-line Extraction Support for HighThroughput LC/MS/MS Analysis of Biological Samples

Increasing the Throughput of Intact Antibody Characterization by Combining Rapid LC/MS Analysis with Novel Software for Automated Data Processing and Comparison In Vitro and in Vivo Detection of Matrix Metalloproteinase Activities with Microdialysis Sampling and MS Investigation of Insulin in the Nuclei of Human Fetal ThyF e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

539


mus Cells by Combining Cell Biology and Affinity MALDI MS Analysis of Subcellular Metabolic Profile of Doxorubicin Using HPLC/MS/MS Chromatographic and Electrophoretic Analysis of Phosphorothiolate Oligonucleotides Determination of Carbachol in Opthalmic Solutions Using Ion Chromatography Chloramphenicol Acetyltransferase Separations from E. coli Cell Lysates Using Capillary-Channeled Polymer Fibers as the Stationary Phase in HPLC Increasing the Sensitivity of Quantitative Bioanalysis Assays with Microbore and Capillary Scale UPLC/MS/MS Separations Bioelectrochemistry, Room 264

IR Transmission Spectroelectrochemistry Studies of Cytochrome c Using an Optically Transparent Diamond Electrode Equilibrium pH and Proton Exchange Kinetics within Dormant Bacterial Spores Continuous Amperometric Detection of Co-Released Serotonin and Melatonin from the Mucosa in the Ileum Latent Fingermarks Imaging by Scanning Electrochemical Microscopy Charge Transfer Study through Single- and Double-Stranded Peptide Nucleic Acid Films Electrochemical Biosensor for Single-Base Mismatch Detection Guanidinium Receptor for Selective Voltammetric Heparin Detection Mimicking the Citric Acid Cycle at a Carbon Electrode Development and Applications of Lab-on-a-Chip (half session), Room 349

Lab-on-a-Chip for Proteomics Developing Microfluidic Chips for Coupling CE with MALDI MS Selection and Sorting of Primary Cells Using Micropallet Arrays Electrochemical PMMA MicroTAS for the Detection of Cryptosporidium parvum Development and Novel Applications of Raman Spectroscopy, Room 262

Characterization of CMC-Wrapped Carbon Nanotubes in the Spin-Coated Thin Film by Resonance Raman Spectroscopy UV Resonance Raman Measurements of Poly-l-Lysine’s Conformational Energy Landscapes at Different Environments UV Resonance Raman Elucidation of Electronic Transitions in Alanine-Based Peptides Novel Screening Method for Enzyme Activity and Enantioselectivity Using SERRS Nanoscale Probes for Biomolecular Detection Using SurfaceEnhanced Vibrational Spectroscopy 540


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Sensitivity Study of Silver-Coated HEPA Filter Using Surface-Enhanced Raman Spectroscopy Eliminating Fluorescence: Expanding Dispersive Raman Technology into the 1-µm Regime Investigation into the Importance of Instrument Calibration for Accurate Sample Identification Using Raman Spectroscopy and Library Searching Environmental Samples and Preparation II, Room 236

Productivity Enhancements for Sample Preparation for Environmental Labs Using Accelerated Solvent Extraction Automated Solid-Phase Extractions of Organochlorine Pesticides from Water Enrichment and Separation of Bifenthrin Enantiomers via SPE and Chiral HPLC Comparison of Thin-Film SPME and Twister Extraction for Analysis of PAHs in Aqueous Samples with Controlled Agitation Conditions Development of Coated Needle for Improved Extracting Solvent Drop Retention for Use with Liquid Phase Microextraction In-Fiber Standardization Technique for Time-Weighted Average Water Sampling Improving Productivity for Organic Analysis Sample Preparation Determination of Veterinary Drug Residues in Fish by an Automated SPE-HPLC System Food Science: MS, LC/MS, GC/MS, TOF/MS, and ICPMS, Room 242

SIFT-MS: New Tool for Real-Time, High-Sensitivity, Quantitative Analysis of Flavor Compounds in Chocolate and Cheese Identification and Quantification of Ethoxyquin Degradation Product Rapid Method for Determination of α-Hydroxy Acids in Seawater and Biological Fluids Robust and Definitive GC/MS Method for the Analysis of Melamine in Dry Protein Materials Rapid Determination of Trans-Resveratrol in Red Wine by SPME with On-Fiber Derivatization and Multidimensional GC/MS Application of a Rapid Headspace SPME GC/TOFMS Method for the Characterization of Coffee and Icewine Aroma Profiles II: Utilization of Statistical Techniques for Classification of Icewine and Coffee Samples Synthesis, Characterization, and Quantification of 2-Hydroxy-4-Methylseleno-Butanoic Acid with HPLC/ESI MS and HPLC/ICPMS Unwanted Species Interconversions as a Challenge for Speciation Analysis of Mercury in Fish Tissue GC: Food and Environmental Analysis (half session), Room 269

GC Analysis of PCBs in Fish Oil by Direct Injection without Any Sample Cleanup


Thermal Desorption Is Not Just for Air Monitoring Anymore! Characterization of Organometallics and Humic Substances in Soils by Methylation Pyrolysis GC with MS and Pulsed Flame Photometric Detection Field Analysis of Total PCBs in Soils by Thermal Desorption/GC GC: High-Throughput Analysis (half session), Room 269

Simple, Integrated GC Heart-Cut Device for Automated Air Monitoring Applications Picoliter Sample Injection System Using Ink-Jet for Capillary GC Direct Resistively Heated Columns for Fast and Portable GC Practical Considerations and Approaches To Improve the Speed of GC Analysis of Complex Mixtures through the Use of High-Pressure and Ultrahigh-Resolution Capillary Columns Lab Informatics I, Room 274

Tools for Designing an FDA 21 CFR Part 11 Compliant Application Thin LIMS: An IT Infrastructure for 21st Century cGMP Quality Operations New Part 11 Guidance for Clinical Investigations Laboratory Informatics as a Tool for Tracking ISO 17025 Requirements Analytical Instrument Integration to LIMS Using an Electronic Laboratory Notebook System Interface Technology Focusing on the Analytes in Complicated Mixtures by Componentization and Filtering of LC/MS Data Analyzing Your Options for Analysis Integrating Informatics into Everyday Laboratory Procedures MS: Applications in Homeland Security and Advances in New Instrumentation, Room 271

Novel Integrated Swatch Test Fixture for Assessment of Toxic Industrial Chemical Resistance of Individual Protective Equipment Detection and Quantification of Sodium Azide and Potassium Cyanide in Drinking Water by ESI-TOFMS: Study for the U.S. Dept. of Homeland Security Mass Spectrograph with Faraday-Strip Array Detection for Ambient MS Shelter Testing Method Development with Ruggedized Preconcentrators on a Portable GC/MS Mini 11 Handheld MS and Its Applications in Biomedical Areas Cryogenic FTMS Characterizing the Heating of Ions in FAIMS Using the Protein Conformation Thermometry Applications of a Micro-MS in MEMS Technology Novel Processes of Quality Control (half session), Room 349

Process Monitoring of an Epitaxial Reactor by FTIR

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Applications of Cantilever-Enhanced Photoacoustic FTIR Gas Analysis New Approaches to Automated Voltammetry Importance and Method of Using Reference Materials in Measuring Reliability of Analytical Results and Why Customers Should Use Them Novel Tools for Biological and Chemical Agent Analysis, Room 350

Design and Performance of a Halo Ion Trap Mass Analyzer Applications of a Toroidal Ion Trap MS to Chemical Warfare Agents and Toxic Industrial Chemicals Detection of Liquid and Cocktail Explosives by Ion Mobility Spectrometry Arson Accelerant Analysis Using Liquid-Phase Microextraction/GC Raman Identification of Biothreats Two-Wavelength Excitation and Fluorescence Triggered Bioaerosol Sorting and Capture System Biomarker-Based Differentiation of Bacillus Endospores Using GC/MS Collective Protection Airflow Mapping

Tuesday

afternoon

Award Pittsburgh Spectroscopy Award, Room 272

UV Resonance Raman Discovery of Gibbs Free Energy Landscape for Protein α-Helix Folding Exposing Chirality in Molecular Vibrations with Help from Sandy 2D Correlation Deep UV Resonance Raman Spectroscopy Recent Studies of Raman Coherence and Ligand Binding Bar-coding Bacteria by Surface-Enhanced Raman Microscopy

Symposia 50 Years of SAS: Looking to the Future with Atomic Spectroscopy, Room 252

Sources, Spectrometers, and Systems: Timelines in Atomic Spectrometry ICPMS: Linking Atomic Spectroscopy’s Future to Its Past Array Detectors in Atomic Spectroscopy: Continuing Revolution—Past, Present, and Future Innovation in Analytical Plasma Spectrometry from the DC Arc to Plasmas on a Chip Developing the Tools versus Employing the Tools: New Emphasis in Atomic Spectroscopy? 50 Years of SAS: Looking to the Future with Vibrational Spectroscopy, Room 255

Future of Industrial Vibrational Spectroscopy: InnovationDriven Quest for a High-Sensitivity Interface between Chromatographs and Vibrational Spectrometers F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

5 41


Impact of Vibrational and Visible Reflectance Spectroscopies at the Extremes of Biological Structures: Studies Extending from Supramolecular Assemblies to Tissues and Organs Mining the Information Content Buried in IR and NIR Bandshapes by Temporal (Perturbation) and Spatial (Imaging) Methodologies IR and Raman Microscopy and Imaging: Are We Looking Where We Think We’re Looking? Achievements and Unusual Challenges in MS, Room 244 14C

Accelerator MS and Applications to the Analysis of Artworks and Artifacts of Particular Interest Precision Mass Measurement: Cyclotron Is Not qB/m—Does E = mc2? Novel Approaches to Global Metabolomics Combination of SPE and SELDI for Screening and Accurate Analysis by MS Isotope Ratio Determination on a Comet Nucleus by IonTrap MS ACS Division of Analytical Chemistry: Analytical Chemistry for Crime Scene Investigation II, Room 276

Validation and Standards for Forensic Analytical Chemistry at the Modern Crime Scene Forensic Elemental Analysis of Materials Using LIBS, µXRF, and LA-ICPMS Developments in Trace VOCs Analysis for Field Forensics Applications CE/MS and Microspectrophotometry for Trace Forensic Analysis of Fibers Electrochemical Detection: Small Is Beautiful, Room 267

Ultrasensitive Biosensing Enabled by Nanostructured Electrodes Electrodes and Electrochemistry in the 8 nL Fly Brain Carbon Nanotubes: Optimum Electrode Material? Redox Magnetohydrodynamic Fluidics in Microelectrochemical Systems Electrochemical Detection of Peptides Fluidics at the Nanoscale: Pores, Pipettes, and Channels, Room 265

Templating the Evaporation of Liquids for Nanolithography Counting Molecules with Nanotubes: New Paradigm in Biosensor Design Single Ion-Channel Recordings Using Glass Nanopore Membranes Nanofluidic Channels for Proteomic Sample Preparation Nanofluidic Devices for AC Electrokinetic Separations LAB 2015 (roundtable discussion), Room 342

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Organized contributed sessions ACS Division of Analytical Chemistry: Theory and Practice of Fast LC, Room 243

Leveraging New Chromatographic Technologies To Improve Efficiency in Analytical Development Revisiting the Trade-offs between Speed and Resolution in Modern HPLC: Particle Size and Column Length UHPLC for Pharmaceutical Analyses Fast LC Using Columns Packed with Small Particles Fast LC Method Development Using Sub-2-µm Particles: Practical Considerations for Pharmaceutical Analysis Role of Efficiency and Selectivity in Small-Particle-Based LC Separations Investigating Thermal and Instrumental Influences on Sub3-µm Columns Current Status and Trends in the Application of LC and UHPLC Hyphenated with Tandem MS for Pharmaceutical Analysis, Room 245

Tandem MS with Evaporative Light-Scattering Detection: Powerful Analytical Combination for the Analysis of Select Pharmaceuticals Application of LC/MS as an Everyday Tool in the Analytical Process Development of API LTQ Orbitrap: Defining Its Place in the Drug Development and Impurity Analysis Workflows Addressing the Need for Speed: High Throughput and High Confidence with Novel LC/MS/MS Solutions Nanospray for Drug Degradation and Impurity Profiling Automated Sample Enrichment and High-Sensitivity Analysis of DMPK Samples Using HPLC/Chip QQQ MS Realizing the Benefits of Sub-2-µm Particle LC Hyphenated with MS/MS for Pharmaceutical Analysis Effective Use of LC/MSn Molecular Fingerprinting for the Rapid Structural Identification of Pharmaceutical Impurities Pharmaceutical Analysis: Latest Trends in Taste and Flavor Assessment in Drug Product Formulations (half session), Room 261

Analytical Methods for the Analysis of Flavors in Pharmaceuticals Improving the Manufacturing Quality Consistency of Food and Soft-Drink Products Using the Electronic Nose and Tongue Drug Product Characterization by Macropixel Analysis of Chemical Images Overview of Electronic Tongue and Nose Applications for Improving the Taste and Flavor Acceptance of Pharmaceutical Products

Oral sessions Bioanalytical Separations II, Room 263

Superoxide Production in Mitochondria 542



Separation and Quantification of Modified Nucleosides in Urine Samples by CE with Laser-Induced Fluorescence Detection Cation Separations by CE Using Organic Salts and Modifiers in the Background Electrolyte Possibilities in the Identification and Quantification of Flavonoids Simultaneously with Acids, Sugars, and Sugar Alcohols in Natural Matrices by GC/MS/MS On-Line Method for Determining in Vitro Amino Acid Flux in Sub-Minute Timescales Using Fast Micellar Electrokinetic Chromatography Isolation and Detection of Calcium Phosphate Crystals from Synovial Fluid Using Bisphosphonate-Modified Magnetic Beads Water-Soluble Vitamin and Amino Acid Analysis in Cell-Culture Media Using Separation Technology High-Speed Amino Acid Analysis on 1.8 µm Reversed-Phase Columns Clinical/Toxicology, Room 264

New Method for the Analysis of Physiological Amino Acids Rapid and Facile Detection of Stimulants and Their Metabolites in Urine Using SPE/Thermal Desorption–Ion Mobility Spectrometry with Alternating Least Squares Rapid Measure of Drug–Drug Interaction Utilizing Generic Gradient Ultra-Performance LC and Tandem MS Determination of Ratio of Testosterone and Epi-Testosterone by SPME/LC/MS Method Assessment of Current Atomic Spectrometric Methods for the Determination of Lead in Blood via Performance in the New York State Proficiency Testing Program Gradation of Gliomas: 1H NMR Metabolic Study Monitoring of Propofo Concentrations in Breath and Blood by SPME/GC/MS and PTR-MS: Chance and Limitations of a New Clinical Tool Development and Applications of Nanotechnology and Microscopy, Room 271

Nanostructured Scaffolds as Synthetic Models of Enzyme Complexes Aptamer-Conjugated Gold-Nanoparticle-Based Colorimetric Assay for the Detection of Cancer Cells New Approach to the Measured Size of Nonspherical Samples Seeing and Sizing Nanoparticles in Liquids: Multiparticle Tracking of Brownian Motion Electrokinetic Transport in Single Nanocapillaries via Axially Opposed, Dual Confocal Microscopy Formation of Lipid Nanotubules from Surface-Attached Liposomes Using Electric Fields Detection and Control of Single DNA Molecule Stretching on Solid Surface Meeting Microanalysis Challenges Using a Flexible X-ray Fluorescence Microscope Developments in Physical Measurements (half session), Room 274

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Good Weighing Practice: Applied Risk Management and Product Life Cycle Management for Weighing Systems Establishing a Correlation between Agent Permeation and Simulant Permeation Thermophysical Properties Characterization of Materials Used in Electronics Applications New Technique for Quantitative Visualization of Membrane Transport FTIR: General Applications and Materials Analysis, Room 270

Comparing the Reactivity of the Alkane-Solvated Reaction Intermediates Co2(CO)7(heptane) and Mn 2(CO)9(heptane) by Time-Resolved IR Absorption Spectroscopy Step-Scan FTIR Spectroscopy with a New Research Vacuum Spectrometer Does Size Really Matter? Study of Interference Effects on Reflectance Microspectroscopy of Particles Smaller Than the Wavelength of Incident Radiation FTIR Imaging of Anisotropic Polymer Films with Polarized Radiation Advantages of Cantilever Enhanced Photoacoustic Detection in FTIR Gas Analysis Macro ATR Imaging: Another Imaging Solution Time-Resolved FTIR/Attenuated Total Reflection Spectroscopy for the Measurement of Molecular Diffusion in Polymer Membranes Thermal Decomposition Studies of Biodegradable Polymers by TGA/FTIR Spectroscopy Homeland Security and Forensic Analysis, Room 262

FTIR and Raman Spectroscopies and Scanning Electron Microscopy for the Analysis of Pharmaceutical Adhesive Labels Water Security: Detecting Chemical Agent Hydrolysis Products by SERS Validation of Diffuse Reflectance IR Spectroscopy as a Means To Discriminate Blood from Various Forensically Relevant Substrates Development and Optimization of Sorbent Polymer Coatings for Detection of Chemicals and Explosives Molecularly Imprinted Polymer-Coated SPME Fibers for Enhanced GC/MS Detection of Chemical Agents GC Analysis of Peroxide-Based, Nitroaromatic, Nitramine, and Nitrate Ester Explosives on a Revised Explosives-Specific Column Pair Towards the Development of a Self-Powered Explosive Sensor Classification of Accelerants by GC/Differential Mobility Spectrometry and Temperature Constraint Cascade Correlation Neural Networks LC/MS: Pharmaceutical Applications, Room 242

Development of Practical Rules for High-Throughput MSDirected Purification of a Medicinal Chemistry Library Based on UPLC/MS F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

543


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Tandem LC/MS Approaches for Extended Detection Times of Drug Administration in Vulnerable Groups Automated Method Scouting To Speed Up the Development of On-Line SPE/LC/MS Analysis of Antibiotics Automated LC/MS/MS Protocol To Enhance Throughput of Physicochemical Property Profiling in Drug Discovery Hydrophilic Interaction Chromatography with MS Detection for the Separation of Basic Pharmaceuticals and Peptides Monitoring the Interactions of Quercetin with Nucleic Acids Structural Elucidation of an Unknown Impurity Present in a Simvastatin Impurity Profile Utilizing Sub-2-µm Porous Particle LC Combined with oa-TOF and MSE

Separations of Protein Digests by Gradient Elution Microchip Electrochromatography on Monolithic Stationary Phases Stabilized, Functionalized Lipid Bilayer Capillary Coatings for Protein Separations Open-Tubular Capillary Electrochromatography Coupled to LIF for the Determination of Cardiac Markers Properties of Binary Guanosine Gels for Bionanotechnology and Separations Unique Media for CE and Capillary Electrokinetic Chromatography

Materials: Miscellaneous, Room 269

Quantitative Measurement of Simvastatin Using Fast LC/MS Rapid Screening and Identification of Ginseng Natural Products Using UPLC/oa-TOFMS and Statistical Analysis Novel RP Column Chemistry with Superior Performance in MS-Compatible Conditions and Exceptional Stability in Wide Range of pH Understanding the Revisions to USP Monograph : Residual Solvents

Selective Transport of Fluorous-Tagged Molecules through Supported Liquid Membranes High-Throughput Characterization of Contamination in Manufacturing Environments Using an Industrialized Electron Beam Analyzer Quality Assurance Strategies in Synchrotron XANES Measurements Measurement of Thickness and Detection of Degradation in Ceramic Thermal Barrier Coatings on Aircraft Turbine Blades Using Time-Domain Terahertz Consideration of Surface Processing Conditions on Metal Material for SEM and Optical Microscopy Using the Plasma-Sputtering Method Analysis of Extractables in Nylon Syringe Filters Calibration Protocols in Ultra-Pure Water Analysis Neurochemistry II, Room 260

In Vivo Pharmacological Manipulation of Nitric Oxide Synthases at the Rat Vitreoretinal Interface Direct Microanalysis of Nitric-Oxide-Related Metabolites in Sensory Neurons of Aplysia californica by CE Selective Detection of Nitric Oxide Using a Xerogel-Modified Amperometric Platinum Electrode Genome-Assisted Neuropeptide Discovery with Bioinformatics and MS Neuropeptidomics of a Song Bird Using MS Development of a Leu-Enkephalin Luminex Assay and Its Application for Quantitative Analysis of Enhanced Microdialysis Sampling Fluorescence Imaging of Exocytotic Release and Free-Radical Distribution in NGF-Treated PC12 Cells Practical Aspects of High-Sensitivity in Vivo Monitoring of Endogenous Neuropeptides by Microdialysis with Capillary LC Multistage MS Novel Phases and Separation Methodology for CE(C), Room 349

Guanosine Gels for Protein Separations in CE Thermally Triggered Miniaturized Separations with a Phospholipid Additive in the CE Separation Medium Sample Transport and Separations on 2D Planar Microfluidic Devices 544


Pharmaceutical Analysis Using Chromatographic Methods (half session), Room 261

Sample Preparation: Pharmaceutical (half session), Room 274

Automated Fractionation System That Increases Recovery and Optimizes Precision of Solid-Phase Extraction Evaluation of Microextraction by Packed Sorbent for Extraction of Drugs from Whole Blood Samples New Separation Materials Design Based on Electron Donor/Acceptor Comparison of SPE and Immobilized Liquid Extraction’s Capabilities To Efficiently Extract Organic Compounds via an Automated System Sensors II, Room 350

Small-Molecule-Responsive Conical Nanotube Embedded in Polymer Membrane Engineering Pore Density in Stabilized Porous Phospholipid Nanoshells for in Vivo and Intracellular Sensing RI Monitoring through Photonic Crystal Imagery Resistive Pulse Studies of Proteins Using an Artificial Conical Nanopore Sensor Sensitive Binding Assay for the Detection of Group Streptococcus DNA Utilizing Prosthetic Group Encapsulated DNA-Tagged Liposomes for Enzymatic Amplification SERS Immunomicrowell Arrays for Multiplexed Foodborne Pathogenic Bacteria Detection Label-Free Diffusion Measurement Using a Whispering Gallery Mode Biosensor

Wednesday

morning

Awards Analytical Chemistry Award for Young Investigators in Separation Science, Room 276


Bioanalytical Separations in Multilayer Microfluidic Devices Microfabricated PCR-Microemulsion Generator: New Tool for Single-Molecule and Single-Cell Genetic Analysis Biocompatible Polymeric Materials for Microseparations Mask-Directed Microreplication CE and Droplets Bomem-Michelson Award, Room 252

Going Nonlinear To Study the Structure and Dynamics of Molecular Assembly at Complex Interfaces Planar Array IR Spectroscopy: Academia + Industry = Product Multivariate Spectroscopy of Lipid-Based Soft Materials Lipid Microdomain Formation: Characterization by IR Spectroscopy and Ultrasonic Velocimetry Protein Microarrays with High Sensitivity

Symposia Applications of Vibrational Spectroscopy in Biomedical Research, Room 255

Quantitative Biological Raman Spectroscopy Raman Spectroscopy, Imaging, and Tomography of Bone Tissue Novel Nanoarray SERS Substrates for High-Sensitivity Biomedical Pathogen Sensing and Classification IR Spectroscopy in Clinical Chemistry: Advances in Instrumentation for Blood Monitoring Molecular Structures of Proteins, Peptides, and Lipids at Interfaces Studied by Linear and Nonlinear Vibrational Spectroscopy Biofuels, Room 244

BioEnergy Science Center: Can New Analytical Instrumentation Help To Overcome the Recalcitrance of Biomass? Joint BioEnergy Institute Great Lakes Bioenergy Research Center: High-Throughput Analysis of Plant Materials as a Resource for Biofuels 3D Spatial Profiling of Lignocellulosic Materials by Coupling Light Scattering and MS High-Resolution Solution-State NMR of Unfractionated Plant Cell Walls: Potential for Biomass Selection and Process Optimization Cancer Biomarkers: Proteomics, Glycoproteomics, Glycomics, and Metabolomics, Room 265

Proteomics Tools To Fast-Track Cancer Biomarker Development Markers of Cancer Using a Lectin Glycoarray Approach Glycans and Peptide for Detection of Hepatocellular Carcinoma Lipidomic Profiling as a Cancer Diagnostic and Prognostic Approach Metabolite Profiles of Sphingolipid and Phospholipid of Colon Cancer Tissues: Lipid Biomarker Study for Colon Cancers

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MS Approaches for Structural Analysis of Nucleic Acids and Their Complexes, Room 267

MS-Based Approaches to Examining the Redox Chemistry of Pyrimidine Cyclobutane Dimers Chemical Probes and Photodissociation for Characterization of DNA/Drug Complexes ESI-FTICR Analysis of Retroviral Protein–RNA Assemblies Quantitative Identification and Characterization of RNA Mixtures Gas-Phase Ion–Electron Reactions and Hydrogen Exchange for Nucleic Acid Structural Characterization Next-Generation Genome Sequencing Technologies, Room 272

Automated Microfluidic Sanger Sequencing Sample Prep Genome Analyzer System: Cost-Effective, High-Throughput Genomics Using Solexa DNA Sequencing Technology Single-Molecule DNA Sequencing by Synthesis Progress toward Ultrafast DNA Sequencing Using Nanopores Single-Molecule DNA Sequencing Using Nanofluidics and Nanoelectrodes

Organized contributed sessions ACS Division of Analytical Chemistry: MS Meets the World, Room 243

Multiple Discrete-Dynode-Multiplier Isotope Ratio MS Wide Mass Range Trapping of PEG Sample Mixture Using MALDI FTMS MALDI TOFMS Examination of Poly(3-hexylthiophene)s Formed at Low Temperatures Using Chemical Oxidative Coupling Methods Combating Counterfeit Drugs with MS in the Open Air Functionally Selective Ion-Mobility Shift Reagents for Structural MS LC/MS/MS Mapping of the Oxidation of apoB in LowDensity Lipoproteins Unambiguous Determination of Isobaric Modifications by LC Retention Time and MS Metaproteomics Approach for Taxonomic Classification of Bacteria Using MS-Based Sequencing of Peptide Ions Analytical Chemistry Applied to the Study and Preservation of Art and Cultural Works, Room 245

Analytical Chemistry in the Museum World: Short Overview and Recent Advances in the Metropolitan Museum of Art Peeling Back History with X-rays: How Confocal X-ray Fluorescence Microscopy Helped Reattribute a 17th Century Flemish Masterpiece Single-Sided NMR of Artists’ Materials UV–Vis Fluorescence Properties of Dyes and Lakes: Implications for the Noninvasive Characterization of Polychrome Surfaces Application of EGA, PyGC/MS, and TD-GC/MS for the Testing of Materials for Use in Storage and Display in Museums F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

545


Secondary Ion MS Studies on Paintings Using DART MS in Preservation Research at the Library of Congress Analysis of Art and Archaeological Materials Using Proteomics Techniques Fluidics at the Nanoscale: Pores, Pipettes, and Channels, Room 271

Ion Transport through Nanopores: From Living Cells to Diodes and Transistors Solvent Behavior in Hydrophobic Silica Nanotubes Nanoporous Colloidal Membranes with Controlled Molecular Transport Electrochemical Characterization of Nanoporous Films Fabricated from a Polystyrene–Poly(methylmethacrylate) Diblock Copolymer Immobilized on an Electrode Surface Biomolecular Recognition in Nanoscale Confined Spaces Detecting “Short” DNAs with Artificial Nanopore Membranes by Resistive-Pulse Sensing Lithography Using Nanotubes Scanning Ion Conductance Microscopy: Imaging Cells and Synthetic Membranes Spectroscopy in the Field: Miniature Spectrometers at Work, Room 261

Identification of Anthrax Spores and Hoax Materials in Mail and on Sorting Equipment On-Line Grading of Beef Carcass Tenderness Using Vis–NIR Spectroscopy Applications of Portable IR and Raman Spectrometers for Homeland Defense Handheld Spectral Analyzers for Field and Consumer-Based Applications Applications of Next-Generation Miniaturized NIR and MidIR TDLAS Gas Analyzers Handheld Raman as a Field Tool in the Fight against Illegitimately Possessed Controlled Substances NIR Spectrometers in the Field: Design Considerations for Practical Applications Incoming Raw Material Authentication with Handheld Raman: Expanded Selectivity Study

Oral sessions Advances in Analysis of Food and Agricultural Products, Room 242

Chiral Fingerprint of an Herbicidal Product Resolved by SFC Automated Powder Pipetting with Random-Access Sample Management and Weight Checking FTIR Microspectroscopic Imaging Provides Objective Chemically Defined Morphological Class Discrimination in Wheat InSb Imaging Provides Nondestructive Subsurface Polychromatic Chemical Discrimination of Germinated Seeds Dietary Supplement Laboratory Proficiency Testing: NIST Pilot Program 546


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Compartment-Resolved, Trace Mineral Element Detection in Fresh Vegetables Using UV Nanosecond Laser-Induced Breakdown Spectroscopy Detection of ppm Pesticides in Imported Fruit and Vegetables by SERS Reproducibility of Nitrogen/Protein Determination by Combustion Method on Nonhomogeneous Food Samples Advances in Bioanalytical Analysis (half session), Room 342

SPE of Proteins from Buffered Solutions Using CapillaryChanneled Polymer as a Stationary Phase for Recovery, MALDI and ESI MS Viral Titre Metabolomic Analysis Using Comprehensive 2D GC Determination of Sulfur-Containing Metabolites of Asparagus in Human Urine with SBSE-GC × GC/TOFMS Advances in Cellular/Tissue Imaging Techniques, Room 241

Mid-IR Transmission Characteristics of the Crotalus adamanteus IR Image Sensor Pit Organ Using IR Microscopy Effects of Radio Protectant Amifostine on Irradiated Rat Brain Tissues Studied by FTIR Microspectroscopy and Imaging Probing Ocular Tissue by Confocal Raman Microscopy: Investigation of Advanced Glycation End Product Adducts in Bruch’s Membrane Differentiation of Individual Stem Cells Characterized by FTIR and Raman Imaging Rapid Return on Investment of Raman Microscopy: Why Many of Your Colleagues Are Now Raman Users Large-Area FTIR Imaging at High Spatial Resolution with Biological Samples: How Differing Levels of Spatial Resolution Can Influence Interpretation Bioanalytical Separations III, Room 263

Thermodynamic Study of Solute Molecules in Confined Liquid–Solid Interfaces by Using Single-Molecule Imaging Influence of Temperature on the Diffusion Coefficient of Peptides Development and Application of Coupled HPLC–OPTLC Glycoprotein Design Strategies: Carbohydrate Remodeling Adsorption Isotherms of Proteins on Polyester CapillaryChanneled Polymer Fibers by Frontal Analysis High-Throughput Protein Separation Using Ion-Exchange HPLC Columns with Nonporous Resin Wire Filament Sample Introduction Device for GC Application of Contactless Conductivity Detection in the Analysis of Non-UV-Absorbing Water-Soluble Vitamins by Capillary LC Biosensors, Room 260

Fiber-Optic Probe for Brain Tumor Analysis Using Nonresonant Multiphoton Photoacoustic Spectroscopy


Micron-Scale Amperometric Sensors for Detecting Reactive Oxygen Species Related to Noise-Induced Hearing Loss in Situ and in Vivo Detection, Validation, and Identification of Lung-Cancer Cell-Surface Biomarkers with Aptamer Probes Development of On-Line Rapid Sampling Microdialysis Monitoring for the Study of Human Intestinal Ischemia Development of an Aptamer-Based Cell Capture Microfluidic Device for Cancer Detection Monitoring Astronaut Health: Detection of Preventive Drugs in Urine by a SERS Chip Monitoring Biofilm Dynamics Using a Disposable Cell Chip Optical Fibers with Silver Nanostructured Tips as SurfaceEnhanced Raman Scattering Probes Characterization of Polymers and Plastics I, Room 269

Multidetector Hydrodynamic Chromatography as a Tool for Characterizing Particle Size and Shape Polymer Distribution Profiling Using Direct Deposition GPC-IR High-Throughput and Robust SEC Measurement Using Newly Developed All-in-One SEC Instrument for Polymers Optimization of Capillary-Channeled Polymeric Fibers as Stationary Phases for the Separation of Water-Soluble Polymers by RP-HPLC Interpreted IR and Raman Databases Terahertz Pulsed Imaging Study of Water Diffusion in Different Viscosity-Grade HPMC Samples New Applications of Surface-Modified GPC Columns Chemical Heterogeneity and Dimensionless Size Ratios in Copolymers Electrochemistry: Environment and Materials, Room 264

Electroless Deposition of TiO2/Ti onto Metal Substrates Electrochemical QCM Studies of Cr(III)-DTPA and V(V)Gallic Acid Complexes at Bismuth Film Electrodes for Catalytic Adsorptive Stripping Voltammetry Separation and Detection of Multimetal Ions by Ion-Chromatography–Anodic Stripping Amperometry: Green, Simple, and Sensitive Method Examination of Electrochemical Activity at the Carboxyl Latex-Particles-Coated Electrodes by Redox of FcTMA+ and Fe(CN)6 4– Electrochemical Sensing at Conducting Polymer Films Modified with Platinum/Palladium Submicron Particles Analysis of Stainless Steels for Use as Bipolar Plates in PEM Fuel Cells Electrochemistry at Carbon Nanotube Network Electrodes Plasma-Deposited Fluorocarbon Films as Novel Insulation Material for Bifunctional AFM-Scanning Probes Environment: Analysis of Biological Materials (half session), Room 342

Rapid Nanoparticle Capture and Lateral Flow Detection of Viruses from Drinking Water Antidepressant Pharmaceuticals in Two U.S. Streams and in

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Fish Brain Tissue Exposed to Wastewater Effluent Meaningful Prefractionation of Humic Substances for the Purpose of Improved ESI MS Characterization Lab Informatics II, Room 274

Going Paperless: Converting from Paper Forms to an Electronic Laboratory Notebook Streamlined Sample Workflow and Information Management for the Routine Chromatography Laboratories Calculating the Benefits for the Introduction of Laboratory Informatics Solutions Lessons Learned from Global Laboratory Informatics Projects Justifying a LIMS Purchase Building an Electronic Laboratory Notebook for Routine Analyses Enterprise-Wide Data Management Connects People, Places, and Data Achieving Great Science: Bringing Together Physical Measurements and Chemical Analysis Material Sciences: Development and Novel Applications, Room 270

Noncontact Measurement of Specialty Coating Curing and Wet/Dry Film Thickness with Time-Domain Terahertz Molecularly Imprinted Xerogels for Glucose Detection Dedicated Accessories for UV–vis/NIR Measurements of Various Materials Carbon-Coated Silica as a Packing Material in LC Characterization of Carbon Nanotubes and Graphitized Carbons as Adsorbents for a Microfabricated Vapor Preconcentrator/Focuser Advantages of Clustering in the Phase Classification of Hyperspectral Materials Images Predicting and Testing Cyanide-Free, Electroless Deposition of Gold onto Metal Substrates Microreactions in Capillaries, Room 349

Electrophoretically Mediated Microanalysis for the Determination of Total Antioxidant Capacity Novel Microfluidics Device for Highly Sensitive and Rapid Immunoassay for des-γ-Carboxyprothrombin Parallel Fluorescent Enzyme Assays Using a Microfabricated Multichannel CE Chip In-Line CE Assay for Serum Creatinine: Fundamental Investigations toward Improving Sensitivity Crystals of Human Lactate Dehydrogenase Isozyme 1 Show Different Levels of Enzyme Activity Segmented Flow Analysis Using Microfluidic Devices and High-Efficiency CE Digital Microfluidic Approach to Homogeneous Enzyme Assays Improved Temporal Resolution with Segmented Flow Process Analytical Techniques, Room 262

Robust Noninvasive Determination of Powder Blend Homogeneity Using NIR Spectrometry and Chemometrics F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

547


Graphical System Design as a Framework for the Implementation of Process Analytical Technology Simultaneous Chemical and Morphological Analysis of Pharmaceutical Granules Reduced-Footprint, Rugged NIR Sensors Integrated in Microreactors for Real-Time Multicomponent Analysis Eliminating Steam from an Extinguished-Fire Gas Matrix for FTIR Analysis Pore-Size Characterization of Silica Monoliths Using Capillary Flow Porometry Real-Time Particle Classification Using Pattern Recognition

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Symposia ACS Division of Analytical Chemistry: Hydrophilic Interaction Chromatography (HILIC), Room 255

Electrostatic-Repulsion–Hydrophilic-Interaction Chromatography: Gradient Chromatography without the Gradient HILIC of Pharmaceuticals on Various Columns Separation of Histone Variants and Combinatorially Modified Forms by Ion-Exchange HILIC HILIC for Analyzing Glycoprotein- and Glycolipid-Derived Oligosaccharides Stationary Phases for HILIC

Special Interest with MS, Room 350

Spectral Accuracy for Formula Identification in MS Challenges of Accurately Deconvoluting Mass Spectrally Overlapped Ion Signals Classification of Jet Fuel Physical Properties by Fuzzy RuleBuilding Expert Systems Applied to Two-Way Fast GC/ Fast MS Data Objects High-Throughput Identification by Comparing Compounds in a Molecular Structure Database with Accurate Mass Fragmentation Data Coupling a Novel Atmospheric-Pressure Ionization Source with Laser Ablation To Perform Imaging MS Coaxial Ion Trap Using Concentric Planar Electrode Arrays Comparison of Ambient Ionization Sources for Use in MS High-Efficiency Ion Transport for Preparative MS

Wednesday

afternoon

Awards Charles N. Reilley and Young Investigator Awards, Room 276

Nanometric Building Blocks and Devices Electrostatic Gating at Glass Nanopore Electrodes Bioelectrocatalysis for Biofuel Cells and Biosensors Magnetic Fields at Electrodes Seeing Electrons Hopping through Molecules Williams-Wright Award, Room 252

Reflections on Vibrations of Blockbuster Pharmaceuticals Peptide Conformational Studies with Optical Spectroscopy, Global and Local, Using Isotopic Labeling Industrial Vibrational Spectroscopy: Fun or Functional? UV Raman Studies of the Electronic Structure Peptide and Proteins: Development of Quantitative Methods for MilliAngstrom Structure Determinations Greenhouse Gas Measurement in the Atmosphere Multistep and Parallel Reactions in Microdroplet Arrays Industrial Applications of Spectral Imaging at 400– 11,000 nm Rina’s Magic Recipe: Mix Chirality, Molecular Vibrations, Pharmaceuticals, and Lots of Proteins

548


Analytical Microinstrumentation for Sustainable Natural Resources, Room 244

Microfabricated Chemical Measurement Instrumentation Electroactive Microarrays for DNA Analysis, Immunochemical Detection, and Chemical Synthesis Biointerface Design for Chip-Based Assays Adaptive (Switchable) Materials: Key to Futuristic Low-Power Analysis Chemical and Biological Ubiquitous RFID Sensors: High Performance at Low Cost Chemical Sensors for Cellular Messengers Come of Age, Room 272

Tracking Neurotransmitter Fate from Storage to Release to Inactivation Probing Functional Differences in Sympathetic Neuroeffector Transmission to Rat Mesenteric Arteries and Veins Multielectrode Sensors To Monitor Transmitters Released from Single Cells Quantitative Aspects of Single-Cell Electroporation: Window on the Cell Single-Molecule Studies of Synaptic Vesicles MS of Synthetic Polymers: Use of MS/MS, Room 265

Applications of MS/MS in the Polymer Industry MALDI-TOF/TOF CID Studies of Styrenic Polymer Fragmentation Reactions Tandem MS of Alkali-Cationized Polyethers: Dissociation Mechanisms and Structural Information MALDI-TOF/TOF MS/MS of Poly(Ester Amides) Utilizing Ion Mobility and Tandem MS for the Characterization of Polyethers Progress in Molecular Targeting: From Bioanalytical to Biomedical, Room 267

Targeted Multifunctional Nanoparticle Probes: In Vivo Detection and Therapy of Brain Tumor Vascular Zip Codes and Synaptic Targeting of Drugs and Nanoparticles Several Novel Microarray Platforms for Post-Genomic Research and Clinical Applications Molecular-Level Targeting of Cancer Cells


Organized contributed sessions Achievements and Unusual Challenges in MS, Room 261

Merits of Nanoelectrospray for High-Quality Data from Complex Samples Characterization of Phenolic Compounds in Vegetable Oils Using CZE and HPLC/ESI-TOFMS Combination of Accurate Mass Measurement and H/D Exchange Using DART MS as a Means to the Identification of Food and Pharmaceutical Adulterants Multiresidue Method for the Analysis of 101 Pesticides and Their Degradates in Environmental Samples by LC/TOFMS UPLC-TOF: Tool for the Quantitative Analysis of Multiple Classes of Veterinary Drug Residues in Food Discovery of Contaminants in Complex Food Matrices Using Statistical Tools with LC/TOFMS and Identification with LC/Q-TOFMS New Territory in FAIMS: Enabling Higher Operational Field Strengths Using a MEMS-Fabricated FAIMS Device Automated Deconvolution of Composite Mass Spectra Obtained with an Open-Air Ionization Source Based on Exact Masses and Relative Isotopic Abundances

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Comparison of 1D and Comprehensive 2D Chromatographic Techniques Simplification of Multidimensional HPLC and Column Switching Green Analytical Chemistry, Room 271

Green Analytical Chemistry: Convergence of Thought Processes Selection of Green Analytical Methods Innovations, Applications, and Education in Green Analytical Chemistry Implementation of Green Analytical Chemistry in Quantitative Methods for Emerging Environmental Contaminants Greening Culture of the U.S. Geological Survey’s National Water Quality Laboratory Green Chromatography and Reaction Monitoring by Microscale HPLC Using Capillary-Based Microreactor Screening System in Green Analytical Chemistry PAT and Pharmaceutical Quality

Oral sessions Characterization of Polymers and Plastics II, Room 269

ACS Division of Analytical Chemistry: New Concept and Instruments for Biosensors, Room 243

Amplification by Polymerization in 96-Well Plate-Based High-Throughput DNA Biosensing Detection of Nucleic Acids Based on Bioluminescence Resonance Energy Transfer between Renilla Luciferase and Quantum Dots Patterned Nanoarray Substrates for Biosensing with Surface Enhanced Raman Scattering Signal Amplification Method Using Au Nanoparticle for Detection of Explosives by SPR Sensor Conformational-Change-Induced Surface Stress for Biosensors Development of Affinity Matrices on Microfluidic Surfaces to Capture Glycoproteins Electrochemical Needle-Type Sensors for Subcutaneous Detection of NO and S-Nitrosothiols Thyrocyte Sodium-Iodide Symporter as the Basis for a Highly Selective and Sensitive Perchlorate Biosensor Comprehensive Multidimensional Separations, Room 245

Discovery-Based Metabolomics Using GC×GC/TOFMS and Chemometric Data Analysis Arson Accelerant Identification by Chemometric Analysis of GC×GC/TOFMS Chromatograms Implications of the Modulation Ratio for Quantitation in Comprehensive Multidimensional Separations: Theoretical Approach Stop-Flow GC: GC with Pneumatic Switching Chronic Disease Biomonitoring through GC×GC: Recent Advances and Perspectives

Single-Molecule Tracking Studies of Free Volume Transitions in Nanoscale Hydrogel Films Separation of Water-Soluble Polymers Utilizing CapillaryChanneled Polymer Fibers as Stationary Phases for HPLC Fluorescence Imaging and Surface Analysis in the Solution of Bonding Problems from Invisible Residues of Mold Release Agents on Plastic Parts Local “pH” within Protein-Loaded Biodegradable Polymer Platforms Metallization of Polyimide Substrates Ultrasonic Degradation of Cellulose versus Amylose Studied by Multidetector SEC Determination of the Acid–Base Balance in Polyols by Titration Mechanoluminescence Produced during Impulsive Deformation of Polymers Chemical Application on Studies of Art and Archaeological Materials (half session), Room 264

Separation and Identification of Organic Compounds in Artwork Resins and Waxes with Comprehensive 2D GC with MS Detection Enhancing Polymerization in Oil Paint Films Using Spectroscopy and Chemometrics To Extract Chemical Information about Mixtures Life on Mars: SERS-Active Lab on a Chip for Amino Acid Detection Environmental: Analysis of Organic Compounds, Room 242

Automated Extraction Procedure for Improved Recovery of Phenols and Phenoxy Herbicides F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

549


Analysis of EPA Method 535 Acetamide Herbicide Degradates by LC/MS/MS Using a Unique Stationary Phase Column Comprehensive Investigation of Degradation Products of Molinate by Various Oxidation Systems Using HPLC/ Ion-Trap MS and GC/MS Improving the Sensitivity, Ruggedness, and Accuracy of Pesticide Analysis Use and Reproducibility of a New Column Series for the Analysis of Polynuclear Aromatic Hydrocarbons Polydimethylsiloxane-Based Device for the Sampling and Analysis of Volatile Organic Compounds Monitoring BTEX and Aldehydes in Car Exhaust from a Gasoline Engine by SPME/GC-FID during the Use of Different Chemical Cleaners Speciation of VOCs from an Animal Feeding Operation Environmental: Quality Assurance and Regulatory Issues (half session), Room 241

Automated SPE To Achieve EPA Compliance Reference Materials Related to Organic Speciation in Particulate Matter Rapid, Accurate, Analytical Technique for the Direct Analysis of Mercury in Sorbent Traps, Coal, and Coal-Related Samples SPE Protocols for Rapid UPLC/MS Determination of Sulfonamide and Tetracycline Antibacterials in Milk GC/MS Instrument and Method Developments, Room 270

Identification and Quantification of Hetero-Atom-Containing Organics in New and Used Insulating Mineral Oils with GC: AED/MS Evaluation of GC Column Stationary Phases Designed for the Analysis of Pesticide Residues Avoiding False Negative SVOC Results Caused by Hydrocarbon Interferences with Dilution and Deconvolution Comprehensive Analysis of Drugs of Abuse in Urine with Automated Disposable Pipette Extraction Soft Photoionization MS as Detection Method for GC: 2D and 3D Comprehensive Separation Performance Comparison of a Hand-Portable GC/TMS to Laboratory GC/MS Instruments for Field Measurements of Targeted Chemical Compounds Pulsed Flow Modulation: Novel Concept for Comprehensive 2D GC×GC/MS with Supersonic Molecular Beams Detection of Marijuana and Cocaine Metabolites in Adulterated Urine Using SPE/Ion Mobility Spectrometry and GC/MS

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LC/MS: Biological Applications I, Room 260

LC/MS/MS Analysis of Phosphorothioate Oligonucleotides Monitoring the Effect of Selenium and Cadmium on Phytochelatin Production in the Eichhornia crassipes via LC/ICPMS/ESI-MS Structural Characterization of Humic Acids Using LC at the Critical Condition Combined with High-Resolution MS and IR Spectrometry Synthesis and HPLC/MS Characterization of α-Hydroxy Acid Capped Lys-Met and Arg-Met Oligopeptides Investigation of Protein Interactions of γ-Glutamyl Carboxylase and Vitamin K-Dependent Substrates Using Capillary LC and MS Structural Characterization of Actin/Cofilin and Actin/Myosin Complexes by MS Multidimensional Separations of Proteins and Peptides for Relative Protein Quantification and Identification Increasing Sequence Coverage of Integral Membrane Proteins through Transmembrane Peptide Detection LC: High-Throughput Chemical Applications, Room 263

Chromatographic Performance of Two New Sub-3-μm Particles Integration of Automated Tablet Dissolution Instrumentation with Multiple Channel Parallel On-Line Microflow HPLC Ultrafast LC: Current Technology and Capabilities HPLC Mobile Phase Temperature Control Using PEEK Components New Approaches for Fast and Robust LC Separation Effect of a Capillary Taylor Reactor on the Performance of a Capillary Column in Fast HPLC LC: Specialized Applications II, Room 349

Oxidative Degradation Study of PEG Using Reversed-Phase Direct Deposition LC-IR Spiral Countercurrent Chromatography Preparation of Polymer Monoliths for Size-Exclusion Chromatography of Proteins Development of Stable and Highly Sensitive Thin-Film Carbon Electrodes Separation of Cu(II)-Azamacrocyclic Complexes Using Ion Exchange and Reversed-Phase Chromatography New HPLC Detector Using Condensation Nucleation LightScattering Detection Technique for High-Sensitivity Analysis Analysis of Dietary Supplements by HPLC-DAD Cyclic Voltammetry in a Chromatographic Detection Cell

Laboratory Management (half session), Room 241

Particle Separations from Organelles to Organisms, Room 274

What Is on and over the Horizon for Informatics? LIMS: Secret Weapon to Regulatory Compliance Enhancing Your LIMS with a Mobile Device Find Chromatography Applications Quickly with a WebBased Tool for Searching and Viewing AnIML Data

Continuous Separation and Fractionation of Mitochondria by Micro-Free-Flow Electrophoresis Microfluidic Cell Sorting Using Photonic Forces for Host– Pathogen Studies Hydrodynamic Study in Capillary-Channeled Polymer Films

550



Using Fluorescently Labeled THP-1 Cells Microfluidic Flow Cytometry for Point-of-Care Diagnostics Isolation and Analysis of Mitochondrial Subtypes from Aging Rat Myoblast Cells Separation of Proteins by Free-Flow Electrophoresis Isoelectric Focusing without Carrier Ampholyte Open-Tubular Capillary Cell Affinity Chromatography: Single and Tandem Blood Cell Separation Ionic Liquids in the Detection of Microbial Contamination by CE Process Analytical Chemistry, Room 262

Automated Analysis of Carbonyl for the Oleochemical Industry Applications of Laser-Induced Breakdown Spectroscopy in Materials Identification and Process Control Off- and On-Line Measurement of Material Density Variations with Time-Domain Terahertz Instrumentation Monitoring Organic Reactions in Real Time by HPLC Design of a Novel Supported Liquid Membrane for Selective Fluorous Separations Novel Chiral Selectors for CE Pros and Cons of Analyzing a Metal Ion by UV–vis versus HPLC Sampling and Sample Preparation in Bioanalysis, Room 350

Continuous Analysis of Aerosols Using a 3D Lab-on-a-Chip Device Determination of Benzodiazepines Concentrations in Human Plasma Using Immunoaffinity Solid-Phase Microextraction Probes Heparin-Immobilized Microspheres for Enhanced Relative Recovery of Cytokines during Microdialysis Sampling Automated Derivatization and Analysis of Malonyldialdehyde from Small-Volume Tissue Samples Using ColumnSwitching Technology and High-Performance LC Analysis of Protein Phosphorylation Using Solid-Phase Enrichment Integrated Affinity Monolith and Semipermeable Membrane Preconcentrators for Polymer Microchip CE Capture of Nucleic Acids Using Photoactivated Polycarbonate 96-Well Microfluidic Chip Large-Volume Stacking Using the Electroosmotic Flow Pump in CE/MS Spectroscopic Applications for Nuclear, Fuel Cells, and Metal Analyses (half session), Room 264

Differentiation of Uranyl Ion Cast Films Utilizing SurfaceEnhanced Vibrational Spectroscopy Automated Analytical Separations for the Nuclear Laboratory Multipurpose Fuel Cell for in Situ and in Operando IR and XAS Spectroscopy Maintaining High Precision with Rapid Analysis, HighThroughput Precious Metals Analysis on ICP

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Spectroscopic Tools for Pharmaceutical Applications, Room 342

Application of a Compact Raman Spectrometer for Pharmaceutical Post-Packaging Analysis Impurity Profiling: Identifying Side Products from Synthesis of a Drug Using Direct Deposition GC-IR New Imaging Techniques in Raman Spectroscopy: Defining New Standards for High-Speed Imaging Data Acquisition for Pharmaceutical Formulations Pushing NIR to the Limit: High-Absorbance Spectroscopy in the Pharmaceutical Industry pH-Dependent Spectroscopy of Tetracycline and Tetracycline Analogs 3D Terahertz Pulsed Imaging To Investigate Key Quality Attributes of Coated Theophylline Tablets Terahertz Pulsed Imaging as a Process Analytical Technique for Sustained Release Tablets Determination of Penicillamine in Pharmaceutical Preparation by UV–vis Spectrophotometry Using Ruthenium(III) Chloride and Its Characterization by Spectral Analysis

Thursday

morning

Symposia ACS Division of Analytical Chemistry: “Quant”—New Look at Introductory Quantitative Analysis, Room 252

The Many Ways of Teaching Introductory Quantitative Analysis in the Western USA What Is Needed for a Successful and Useful Textbook? Revising the Quantitative Analysis Course: What To Keep? What To Change? Rethinking Quant: Importance of Analytical Thinking Case Studies Supporting “Eurocurriculum II for Analytical Chemistry” Bioanalytical Applications and NIR Fluorescence, Room 265

NIR Fluorescence of Carbocyanines: Variety of Structures Affords Wide Selection of Wavelengths and Applications Systematic Evaluation and Use of Targeted, Labeled, Optical Contrast Agents Quantitative, Multicolor Molecular Imaging for Therapeutic Efficacy Monitoring and in Vivo Disease Profiling Metal Phthalocyanine NIR Dyes as Reporters for HighThroughput Screening Assays: Energy-Transfer Processes for Finding Inhibitors of L1 Endonuclease Fluorescent Biosensors for Cell Pathways Label-Free Bioanalytical Detection Using Plasmon Resonance Spectroscopy: New Capabilities Inspire New Applications, Room 267

SPR-Based Label-Free Analysis in Drug Discovery: Recent Developments Molecule–Surface Plasmon Interactions: Issues and Potential F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

551


for Spectroscopy and Sensing Plasmon-Controlled Fluorescence: A New Paradigm in Fluorescence Spectroscopy Label-Free Surface-Enhanced Spectroscopic Detection of Biomolecules and Biomolecular Interactions Combining Surface Plasmons, Diffraction Gratings, and Nanoparticles for Ultrasensitive Biosensing

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Miniature-Ion-Trap MS with Circular Trapping Geometry Sampling Solutions for Field-Portable GC/MS: Issues and Technology—Past, Present, and Future Breaking the Limit of Pumping Capacity: Portable MS with Atmospheric-Pressure Ionization Sources Miniature MS on Space and Planetary Missions


Nanoparticle Biosensors, Room 255

Surface-Enhanced Raman Nanoparticle Tags for in Vivo Cancer Detection Biofunctionalized Nanoparticles: From Forensic Science to Targeted Intracellular Sensing Plasmon Rulers for Measuring Dynamical Distance Changes in Biological Macromolecular Assemblies Nanoflares: Probes for Transfection, RNA Visualization, and Detection Biomolecular Analysis Using Functionalized Silver Nanoparticles Neurochemical Monitoring: New Electrode Materials and Measurement Methodologies, Room 244

Rapid Monitoring of Serotonin Regulation in the Rat Hippocampus Carbon-Nanotube-Modified Microelectrodes for Rapid Detection of Serotonin Nonlinear Time Series of Electrochemical Data for Neurochemical Analysis 5-Hydroxytryptamine and Nitric Oxide Signaling in the Gastrointestinal Tract In Vitro Electrochemical Studies of Serotonin Disposition in the Intestinal Mucosa of Neonatal and Adult Guinea Pigs

New Era of LC, Room 261

New Era of LC: Immediate Effects of High-Throughput Analysis on Drug Development and Therapeutic Drug Monitoring Critical Look at the Application of Ultra-High Pressure, Elevated Temperature, and Particle Size on Chromatographic Performance Novel Application of Advanced LC/Tandem MS to the Pharmacokinetic Study Expanding the Horizons of High-Speed Chromatographic Analysis Using Sub-2-µm HPLC Packings Detector Calibration for High-Temperature Nonlinear LC Development of New Automated Selectivity Testing Equipment for Monolithic Columns LC/MS Studies of Pralidoxime Chloride: Preparing for Chemical Terrorism Improve HPLC Throughput with Automation and Real-Time Diagnostics Atomic and Molecular Spectroscopy in Honor of James D. Winefordner, Room 245

The Arctic: Where Rapid Climate Change Is Reality Climate Change in the Northeast U.S.: Past, Present, and Future Recent Climate Change: Natural and Human-Induced Role of Modeling in Climate Change

Plasmonics and SERS: Applications and Potential in Biomedical Diagnostics Laser-Ablation ICPMS with Femtosecond Lasers ETV Can Add Another Dimension to Your ICPMS Fundamental Role of S/N Ratios in Analytical Chemistry Limit of Quantitation in Atomic Spectrometry: An Unambiguous Concept? Fundamental Advances in Atomic Spectrometry New Fundamental Studies in ICPMS

Mysterious Mechanisms of Abused Substances, Room 243

Young Scientist Session: Proteomics and Glycomics in Biomarker Discovery, Room 271

Subsecond Dopamine Release during Drug Taking Unfaithful Transporters: Unmasking Novel Sites of Action for Abused Drugs Neurochemical Comparison of Striatal Dopamine Function in Drinking Regulated Dopamine Transporter Function and Its Relationship to Cocaine Behavioral Activation and Addiction 70 New Agonies over Ecstasy: Serotonin and Psychostimulants

Development of a Quantitative, Label-Free Approach for Glycopeptide Analysis: First Step Towards GlycopeptideBased Biomarker Discovery Clinical Glycomics Approach for the Early Detection of Diseases Sequence Analysis of Urinary Peptides to Monitor in Vivo Disease-Dependent Protease Regulation Novel Glycoproteomics Approach for the Characterization of Glycopeptides from Complex Biological Mixtures Identification of β-Amyloid and Nitrated and Oxidized Ubiquitins by Ion-Trap MS Glycan Profiling in Plasma: Fundamentals and Applications to Ovarian Cancer MS Strategies for Glycomic and Glycoproteomic Biomarker

Panel Discussion on Global Warming, Room 276

Truly Portable MS, Room 272

Handheld Analytical Instrumentation with Mobility Spectrometry for On-Site Rapid Measurements of Chemical Vapors of Industrial and Medical Importance 552



Discovery Multimethodological Approach to Glycoproteomic and Glycomic Mapping of Healthy and Breast Cancer Blood Serum Samples

Oral sessions Biodiesel Analysis via Spectroscopic and Chromatographic Methods, Room 241

Elemental Analysis of Biodiesel, Biodiesel Blends, and Associated Raw Materials by ICP Analysis of Biodiesel Using Supercritical Fluid Chromatography Simultaneous and Real-Time Measurement of Mono-, Di-, and Triglycerides in a Continuous Flow Biodiesel Reactor Using an EP-NIR Spectrometer Simple and Innovative Methodology for Determination of Glycerol in Biodiesel and Biodiesel Blends by Ion Chromatography Recent Advance on Quantitative Characterization of Mineral Diesel and Biodiesel Blends by Comprehensive 2D GC Recent Developments To Enhance Productivity in the GC Characterization of Pure Biodiesel (B100) in Compliance with ASTM D6584, EN14103, EN14105, and EN14110 Integra-Gap Technology and MXT Metal Columns: Biodiesel Glycerides Analysis Made Easy and Reliable Development and Applications of a New Range of LowBleed, High-Temperature Capillary Columns Based on an Improved Liquid Phase Synthesis and Stainless Steel Surface Deactivation Technology

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Gas Sensors in Extreme Environments: Extending Temperature, Pressure, and Humidity Limits Detection of Organic Peroxide Explosives through the Fenton Reaction Electrochemical Synthesis of Metal and Semiconductor Nanowires for Sensing Applications Comparison of Different Carbon-Fiber Kinetics by Fast-Scan Cyclic Voltammetry Nanostructured Electrochemical Sensor for Rapid Analysis of 2000-Fold Diluted Urine Environmental: Air and Aerosols, Room 269

Definition Hydrocarbons in Exhaust Gas by Thermocathalytical Methods Analytical Characteristics of a Sensor To Control Oxide of Carbon from Structure of Transport Emission Analysis of Structure Exhaust and Smoke Gases by Thermocathalytical Methods Application of Needle-Trip Device for Time-Weighted Average Diffusive Sampling Novel Concept for in Situ Capture of Taste and Odor in Drinking Water Development of a Versatile Man-Portable Obscurant Aerosol Generator: Characterization of Aerosols in Laboratory and Field Environments Telescope System: Fresh Approach to Open-Path FTIR Widely Tunable Quantum-Cascade Laser-Based Hollow Waveguide Gas Sensors for Multianalyte Detection Environmental: Analysis of Drinking Water and Waste water, Room 264

Multivariate Chemometrics Protocol for Analysis of Oral Mucosa Cell IR Imaging Data Chemometric Analysis of a Simple Method for Detection of Dipicolinic Acid and Other Biomarkers from Bacterial Endospores Automated Wavelength Selection for NIR Spectroscopy Based on Particle Swarm Optimization Choosing Chemometrics Tools Application of Hierarchical Band-Target Entropy Minimization Curve Resolution to IR Imaging Data from Cellular Studies Robustness of Variable Selection Based on the SIMPLISMA New Pure Variables Theory and Analytical Applications of the Temperature-Constrained Radial Basis Function Neural Networks Multivariate Self-Modeling Curve Resolution of in Situ R AIR Spectra from Surface Chemistry Studies

Analysis of Hydroxide, Sulfur Species, and Oxalate in Kraft Liquors by CE with Direct UV Detection Applications of Ion Chromatography Systems with Eluent Regeneration Characterization and Quantification of Polyelectrolytes Flocculants at Trace Level in Water by Pyrolysis GC/MS Improved Multitechnique Approach for the Analysis of Complex Environmental Samples Using IR, Raman, and MS Techniques Analysis of Fluoride in Drinking Water in the Presence of Interfering Matrix Ions such as Iron and Aluminum Analysis of Emerging Haloacid Disinfection By-Products Using Automated Postcolumn Reaction Ion Chromatography with Nicotinamide Fluorescence Determination of Trihalomethane Concentrations in Drinking Water Using Capillary Membrane Sampling/GC/MS Implications of False Cyanide Formation for Laboratories Testing Drinking Water Samples

Electrochemical Biosensors, Room 270

GC/MS of Environmental Samples, Room 242

Nanoparticle Labels/Electrochemical Immunoassay for Detection of Protein Biomarkers Nanocatalyst-Amplified Electrochemical Immunosensor Monitoring Nitrogen Compounds in Surface Waters by IonSelective Electrodes

Chemical Characterization of Obscurant Aerosols Obtained from Mini-Jet-Based Aerosol Generator Laundering Effects on the Bite Protection and Permethrin Content of Production Level Factory-Treated Marine Corps Combat Utility Uniforms

Chemometrics, Room 274

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Validation of the TD GC/MS Method for the Determination of Brominated Fire Retardants in Polymeric Materials Determination of Polybrominated Diphenyl Ethers in Fish Oil and Other Dietary Supplements by HRGC/HRMS Isotope Dilution GC/MS/MS Method for Steroid Hormones in Water Optimization of a GC/MS Method for Analyzing Polychlorinated Biphenyls in Human Serum High-Concentration VOC Air Toxics Technique Using EPA Method TO-15 without a Dilution Quantification of Polychlorinated n-Alkanes in Environmental Matrices: Comparison of Performances of GC/EIMS and GC/EIMS/MS with GC/EcNI/MS and GC/ECD

Photolithographically Patterned Carbon-Nanotube-Containing Polymer Thin Films for Sensing Applications Breath-Ammonia Conducting-Polymer Nanojunction Sensor Quantum-Dot-Based Nanosensors for the Measurement of Sodium Flux during Action Potentials Electrospun Nanomaterials for Use as Separation Media in Small-Scale Fluidic Devices Hindered Transport of Polyelectrolytes in Single Cylindrical Nanopores Prepared by Focused Ion Beam Milling in Polymethylmethacrylate Membranes Synthesis of Colloidal Uranium Dioxide Nanocrystals Aptamer Conjugated Au–Ag Nanorods for Selective Cell Targeting

Imaging: Surface Analysis/Nanotechnology, Room 260

Sensors III, Room 350

High-Resolution Imaging and Chemical Characterization of Heterogeneous Materials with the Confocal Raman AFM AFM Tip-Integrated Solid-State pH Microsensors Mapping Magnetic Domains Using Magnetic Sample Modulation AFM: Characterization of Nanopatterns of Ferritin Batch Fabrication and Application of Single-Walled Carbon Nanotube AFM Probes Fabrication of Periodic Arrays of Metal Nanostructures Produced with Electroless Deposition and Particle Lithography Characterization Using Magnetic Modulation AFM Investigation of Surfaces and Depth Profiles by Glow Discharge Optical Emission and Atomic Emission Spectroelectrochemistry Orientation Analysis by Nonlinear Optical Stokes Ellipsometry Preparation and Characterization of Porous Gold and Its Application as a Platform for Immobilization of Acetylcholine Esterase

Biosniffer with Drug-Metabolizing Enzyme for Breath Odor Analysis Highly Sensitive SAW-Based Sensor System for Workplace Monitoring Acid Degradable Stabilized Phospholipid Vesicles for Biological Sensing and Delivery All-Inkjet-Printed Low-Cost Multianalyte Chemical Sensing Chips for Quantitative Analysis Easily Manufactured Microcytometer Annular Sheath Flow Automatic Viscosity Control System for the Preparation of Pharmaceutical Tablet Coating Solution Detection of Ammonia Vapor by SPR Using Gold-Nanoparticle-Embedded Polymers Chemically Modified Micro-Resonator Sensors

Microfluidic “Hardware”, Room 263

Fluidic Communication between Multilayered Microchip Channels Interconnected with Nanocapillary Array Membranes Assessing the Performance of a Dynamic-Loading Electrokinetic Injection in Chip CE Label-Free Native Fluorescence Detection Results for GelPlane and Microchip Electrophoresis Separation Devices Development and Application of a Microfabricated Device for Use in Photothermal Detection Development of a Microfabricated Coulometric Array Detection System Evaluation of Low-Power, Noncontact Heating Sources for Thermocycling in a Plastic Chip: Towards a Portable PCR Instrument Integration of Microdialysis Sampling with Microchip Electrophoresis and Amperometric Detection for Neurotransmitter Analysis Magnetic and Thermal Actuation of Phospholipids for Microfluidic Flow Control Nanotechnology, Room 262 554


Thermal Analysis (half session), Room 349

Simultaneous Measurement of Transformation Energetics, Mass Changes, and Evolved Gas Analysis Using Advanced Thermal Analysis Instrumentation Benchtop Calorimeter for Process Design and Material Characterization QC Using Standardized Thermal-Analysis Techniques UV–vis for Materials Analysis (half session), Room 348

Applications of Attenuated Total Reflection Far-UV Spectroscopy to Measurement of Aqueous and Nonaqueous Solutions Frequency-Domain, Planar Waveguide Spectroelectrochemistry: Development and Application to Optical Switching and Molecular Orientation in Organic Thin Films Methodology for Nondomestic Pollution Diagnosis in an Urban Wastewater Network with UV Spectrophotometry Optical Chirality Sensing of Liquid Interfaces

Thursday

afternoon

Symposia ACS Division of Analytical Chemistry: Advances in Ion Exchange Chromatography, Room 276

Prehistory of Ion Exchange Chromatography


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Computer Simulation and Optimization of Separations in Suppressed Ion Chromatography Using Combined Isocratic and Gradient Elution Profiles On-Line Gas-Free Electrodialytic Eluent Generator for Capillary Ion Chromatography Electrostatically Attached Hyperbranched Condensation Anion Exchange Polymers: State of the Art New Possibilities in Capillary Ion Chromatography

Microextraction Analytical Microextraction across Supported Liquid Membranes: Efficient Preconcentration and Cleanup Based on Passive Diffusion and Electrokinetic Migration Miniaturized Sample Preparation Approaches for Microseparation Techniques Interfaces between Real Samples and Microseparation Techniques

Integrated Sensing and Processing, Room 272


CRISP Techniques for Optical/Acoustic Spectrometry Integrated Optics, Electronics, and Software for Embedding Multivariate Regression Vectors into Data Collection Schemes Beyond ISP: Intense Laser Hamiltonian Control for Selective Sensing Compressive Sensing Multivariate Optical Computing in Industrial Processes Metallomics: New Melding of Atomic Spectrometry and Bioscience, Room 255

Metallomics Approaches for Studying Pharmaceutical or Clinical Samples Characterization of Posttranslational Modifications of Cytochromes by ICPMS ICPMS and Metallomic Tags To Flag Leukemia Stem Cells High-Resolution Atomic MS for Metallomics Dual-Source ICP-ESI-TOFMS: New Tool for Metallomics New Reagents for Biologic Imagery, Room 265

Quantum Dots for Lymphatic Mapping and Sentinel Lymph Node Detection Coordination Chemistry of Molecular Imaging Probes Development of New Nanocrystal Molecules for Biological Sensing and Detecting Nano-PEBBLE Sensors for Reliable in Vitro and in Vivo Imaging of Intracellular Chemistry Visible and NIR Emitting Polymetallic Lanthanide Dendrimer Complexes for Biologic Imaging and Sensing Placement, Patterning, and Applications of Single Molecules in Controlled Chemical Environments, Room 252

In Search of Brain Nanobiosensors: Small-Molecule Recognition as an Important First Step Trapping and Manipulating Single Molecules in Solution Fundamental Issues in Electron Transfer between a Biomolecule and an Electrode Patterning and Measuring Molecules Inserted into Controlled Self-Assembled Monolayer Matrices Sample Preparation Approaches for Microseparation Techniques, Room 267

Sample Preparation Strategies for Microseparations: Overview Immobilization of Short-Chain Polyethylene Glycols via Ionic-Liquid-Mediated Sol–Gel Process for SolventFree Preconcentration of Polar Analytes by Capillary

ACS Division of Analytical Chemistry: Small Instrumentation for a Small World, Room 243

Cystamine-Modified Gold Nanoparticles for SERS-Based Real-Time Perchlorate Detection and Monitoring in Biochemical Environments Development of a New AFM Imaging Mode Using Magnetic Sample Modulation Investigating Diffusion of Single Molecules at Solid/Liquid and Membrane/Liquid Interfaces Using Total-Internal Reflection Fluorescence Microscopy Kinetics in Levitated Drops Multianalyte Microphysiometry: Electrochemical Sensors in Very Small Volumes Rapid Combined Autoimmune and Infectious Disease Serodiagnostic Microarray: Investigation of Links between Infection and Autoimmune Disease Robotization of Microfluidics for Fast and Automated ELISA CE with Laser-Induced Fluorescence Detection To Analyze Turnip Yellow Mosaic Virus Integrated Approaches for Impurity and Degradant Identification, Room 262

Case Studies of Impurity Analysis in Drug Products and Drug Substances by LC/MSn Understanding the Use of Temperature Regulation To Optimize Mass Transfer in Fast Gradient RPLC Integrating Automated Data Analysis with Optimized LC-DAD-ELSD-CLND/MS Ultralow-Flow-Rate Electrospray: Exploration of Equimolar Response, Limits, and Applications High-Resolution LC/MS Methodologies for Structural Characterization of Impurities and Degradation Products in Drug Substances New Approach to Ion Sampling in LC/MS/MS: Going with the Flow from Theory to Practice Application of DART and DESI Techniques for Direct Analysis of Impurities and Degradants Repository for Impurity and Degradant Analytical Characterization Data

Oral sessions Analytical Tools for Pharmaceutical Applications, Room 242

Aptamers Evolved from Cell-SELEX as an Effective Platform F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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for Drug Delivery and Release Robust Calibration Design in the Pharmaceutical Measurements of Tablet Content Uniformity with NIR Spectroscopy Developing Robust Linear and Nonlinear Chemometric Tools for On-Line Content Uniformity Determination Using NIR Spectrometry Multifunctional Nanostructures for Cancer Cell Diagnostics and Therapy Determination of Pharmaceutical Residual Solvents Using Headspace SPME/GC × GC DOSY NMR: New Tool for Analysis of Fake Drugs Residual Solvents in Drug Products Using Liquid Phase Microextraction/GC

Early Detection of Cataracts Using Planar Array IR Spectroscopy: Current Capabilities and Future Prospects Molecular Switching of Singlet Oxygen Generation Based on Photosensitizer Molecular Beacon Aptamer Raman Spectroscopic Grading of Brain Tumors: Dealing with Limited Sample Numbers Age and Muscle Type Influence on Protein Carbonylation in Rat Skeletal Muscle Mitochondria Separation of Endogenous Fluorophores in Normal and Cancer Cells by CE Surface-Enhanced Raman Scattering of Mitochondria for Diagnosis and Disease Progression

Assessing Cytotoxicity and Cellular Morphology, Room 263

Development of NIST Standard Reference Materials for Trace Explosives Detectors Chemical Warfare Agent Detection Using SIFT-MS Detection of Leaking Toxic Industrial Chemicals with an Ex-proof Gas Detector Array Using an Ion Mobility Spectrometer Agent and Simulant Decontamination Studies on Aircraft Surfaces Validation of a Mechanistic Model for IPE Airflow Mapping Mechanisms of Emission Signal Enhancement in Laser-Induced Plasma Determination of Extraction Efficiencies of LSD from SugarBased Matrices

High-Throughput Biosensor for Studying the Cytotoxicity of Microcystin-LR on Cultured Cells Investigation of the Interactions between Silica-Surfaced Nanoparticles with Human Lung Cancer Cells Using a Single-Cell Imaging System Electrochemical Studies of the Effect of Cholera and Botulinum Toxins on Cellular Metabolism Determination of 8-Iso Prostaglandin F2 in Cultured Cancer Cell after Exposure to Nanoparticles by LC/MS Hyperspectral Confocal Fluorescence Imaging: Enhanced Autofluorescence during Host–Pathogen Interactions Electrochemiluminescent Arrays for Genotoxicity Screening Employing Liver Microsomes Deciphering the Effect of Low Oxygen Tension on Red Cells Using Microflow Methods Determination of ζ-Potential and Tortuosity in Rat Organotypic Hippocampal Cultures Using Feedback Control Bioanalytical Applications of CE, Room 269

Amine Metabolites Separations of Fruit Flies Using Micellar Electrokinetic Capillary Chromatography–Electrochemical Detection Quantifying Phycoerythrin Pigment Concentrations in Marine Bacteria by CE-LIF Separation and Detection of Dynorphin A 1-17 and Its Major Metabolites Using CE with Both UV and Electrochemical Detection and MS Determining the Amino Acid Content of Human Tears Doxorubicin and Metabolites by Micellar Electrokinetic Chromatography with Laser-Induced Fluorescence Detection Directly Sampled from Human Liver Tissue Cross-Section Analysis of Cellular Signaling in Primary Cells Using Recombinant Molecular Reagent Peptides and CE Toward the Determination of the Phosphorylation Sites in the Tight Junction Protein ZO1 Biospectroscopy Applications, Room 264

Conformational Characterization of Peptides by UV Resonance Raman Spectroscopy 556


Chemical Applications and Development for Homeland Security and Forensics, Room 349

Chiral Separation in CE, Room 270

Understanding Bile Salt Micelle Formation Interactions and Bile Salt Micelles’ Chiral Recognition Interactions Utilizing MEKC and NMR Multivariate Approach for the Enantioselective Optimization of Binaphthyl Derivatives in Micellar Electrokinetic Chromatography/MS Multistage Separations of Chiral Amino Acid Mixtures on a Multilayered Polymer Hybrid Nanofluidic/Microfluidic Device Utility of Ionic Liquids for Difficult Separations of Positional and Optical Isomers in CE Chiral Recognition and Determination of Enantiomeric Composition of Amino Acids Using a Fluorescent Resorcinarene Enantiomeric Separation of Chiral Ruthenium(II) Complexes Using CE Optimized Separation of Blockers with Multiple Chiral Centers Using Capillary Electrochromatography/MS Developments in High-Throughput Chemical Analysis (half session), Room 245

Novel Multisorbent 96-Well Plate for Automated SPE: Ideal Combination of Sorbents for Universal Method Development Regenerable Tethered Lipid Membrane Arrays and Their Characterization Using SPR Imaging Toward Integrated Mid-IR Photonic Sensors


General Interest: Atomic Spectroscopy/Elemental Analysis (half session), Room 271

Nebulizer Comparison Studies of ICP Atom and Ion Emission Profiles Utilizing Acousto-Optic Tunable Filter Hyperspectral Imaging Total Multiline ICP Analysis of Biodiesel Samples Do ICPMS Sample Introduction Techniques Improve Environmental Performance on ICP Systems? Laser-Ablation ICPMS/ICP-OES-Quantitative Element Determination in Industrial Materials

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Ion Suppression as a Function of Mobile Phase pH in the Analysis of Polar Basic Drug Compounds in Samples of Biological Origin by ES + LC/MS/MS Metabolic Profiling of Phospholipids in Rat Plasma Utilizing Ultra-Pressure LC and oa-TOFMS Capillary LC/MS for High Sensitivity Metabolomic Analysis of Islets of Langerhans Determination of Glutathione Conjugates of 4-Hydroxy2(E)-Nonenal as Indicators of Transport Non-Digest Liberation of Biomarkers from Plasma: Novel Two-Stage Ultrafiltration Approach

High-Throughput Chemical Analysis, Room 241

Screening Peptide Catalysts in a Novel Capillary-Based Microreactor High-Throughput pK a Measurements and Chiral Separations by Multiplexed CE with UV Detection High-Throughput Analysis by Laser-Diode Thermal Desorption MS New SPME/LC/MS/MS Automated System for the Determination of Ochratoxin A in Human Urine Automation of SPME in High-Throughput Format Using Multiwell Plates and Applications to Therapeutic Drug Monitoring and Drug–Protein Binding Studies Advancing Performance in the Analysis of Highly Dissolved Solid Solutions by ICP-OES through Innovative Design Application of a New ICPMS Sample Introduction System for High-Throughput Analysis of Environmental Samples with Minimal Memory Effects Fast Algorithm and Software for Analysis of FTICR Data

LC: Pharmaceutical Applications, Room 261

Impact of Stationary Phase Chemistry on Retention and Selectivity in Aqueous-Normal Phase/HILIC Separations Analysis of Metabolized Nucleoside Reverse Transcriptase Inhibitors through Ion-Exchange HPLC Comparison between On- and Off-Line Heart-Cut 2D LC for Impurity Profiling of Pharmaceutical Compounds Multistage Sample Injection: Effective Way To Reduce Band Broadening in LC Development of an Automated Forced Degradation Instrument Parallel Multiple Channel Microflow LC Method Development for Complex Separations: Emerging Instrumental Technique Evaluation of New 3 µm HILIC Column for Hydrophilic Compounds Column Diameter’s Role in the Performance of Small-Scale Preparative Columns

Imaging Cells, Room 274

Single-Cell and Imaging MS Studies of Biochemical Changes in the Nervous System Following Drug Administration MS Imaging in Mated Tetrahymena thermophila: Following the Formation of Lipid Domains Measuring Water Transport across Endocytic Organelle Membranes in Living Cells Using Ratiometric Fluorescence Imaging General Fluorescence Resonance Energy Transfer Assay for Studying Cell-Membrane-Protein Clustering and Signaling Improving MS Imaging of Cholesterol in Single Cells Probing Nanoscale Chemical Heterogeneities of a Single Bacterial Cell: Soft X-ray Spectromicroscopy Study Single-Cell Electroporation Using 2 2-µm Tip Capillaries with Improved Distance Control, Temperature Control, and Cell Synchronization Characterization of Giant Mitochondria in Rat Myoblasts and Skeletal Muscle Tissue LC/MS Biological Applications II, Room 260

Biological Agent Classification and Identification Using MSBased Bioinformatics Proteomics Approach Validation of a HPLC/Particle Beam MS with Electron Impact and GD Ionization Sources for Botanical Extracts Increasing the Speed of LC/MS/MS in Pharmacokinetic Study Using Microflow HPLC and Sub-3-µm Particles

LC: Pharmaceutical Applications—Chiral Separations (half session), Room 271

Chiral HPLC/SFC Prep Purification: Robust Collection of Enantiomer Peaks Using the ±Derivative of an Advanced Laser Polarimeter Signal Chiral Piece of the Pie: Optimizing Chiral Separations through Selective Sample Slicing and Column Switching Optimized Chiral Separations and Enantiomeric Excess Determined via an Automated Parallel Chromatographic Scouting System Chiral HPLC Method Screening: Automated Method Screening Using a New Low-Pressure Gradient Mixer with up to 24 Independent Inlet Ports Ultrasensitive Detection in Bioanalysis (half session), Room 245

Effects of Photon Shot Noise and Molecular Counting Error on Single-Molecule Fluorescence Anisotropy Compact Single-Molecule Detection Instrument for Monitoring Point Mutations Using Single Pair FRET Pattern-Recognition Nanopore Sensor for Single-Molecule Detection of Biomolecules Pb2+ Detection in Hybrid Nano/Microfluidic Device Utilizing DNAzymes Immobilized on Gold-Coated Nanocapillary Array Membranes F e b r u a r y 1 , 2 0 0 8 / A n a ly t i c a l C h e m i s t r y

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Pittcon Technical Program - ACS Publications - American Chemical

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