PITTSBURGH CONFERENCE - ACS Publications - American

Feb 1, 1985 - PITTSBURGH CONFERENCE. Anal. Chem. , 1985, 57 (2), pp 134A–150A. DOI: 10.1021/ac50001a001. Publication Date: February 1985...
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The 36th Pittsburgh Conference and Exposition on Analytical Chemistry and Applied Spectroscopy will be held in the New Orleans Convention Center, New Orleans, La., Feb. 25March 1,1985. This year more than 100 technical sessions are scheduled, including 18 planned symposia and more than 1200 papers. The Exposition of Modern Laboratory Equipment will feature over 660 exhibitors in more than 1850 booths showing the latest in analytical instruments and related chemicals and publications. Several awards will be presented during the conference to honor scientists who have contributed extensively to analytical chemistry and applied spectroscopy. The 1985 Pittsburgh Analytical Chemistry Award, sponsored by the Society for Analytical Chemists of Pittsburgh, will be presented to Bruce Kowalski for his contributions to chemistry. The presentation will take place a t an award symposium on Tuesday, The 1985 Pittsburgh Spectroscopy Award, sponsored by the Spectroscopy

Feb. 27. Griffiths is being recognized for his contributions to the theory and practice of FT-IR. The Maurice F. Hasler Award will be presented to Paul Lauterbur on Wednesday, Feb. 27. Lauterbur is 134A

ANALYTICAL CHEMISTRY, VOL. 57, NO. 2, FEBRUARY 1985

being recognized for his achievements in whole-body NMR imaging. The Williams-Wright Industrial Spectroscopy Award, sponsored by the Coblentz Society, will be presented to two scientists: Clara Craver for her work in applications of vibrational spectroscopy and Richard Nyquist for his work with IR and Raman spectroscopy. The award will be presented on Thursday, Feb. 28. The Society for Electroanalytical Chemistry will present its Charles 3. Reilley Award to Ralph Adams in recognition of his contributions to solid electrode voltammetry, organic oxidation mechanisms, and in vivo electrochemistry. The award will be presented on Tuesday, Feb. 26. The 1984 Pittsburgh Conference Memorial National College Grants, sponsored by the Pittsburgh Conference on Analytical Chemistry and Applied Spectroscopy, Inc., the Spectroscopy Society of Pittsburgh, and the Society for Analytical Chemists of Pittsburgh, have been awarded to the following colleges: Adrian College, Adrian, Mich.; Andrew College, Cuthbert, Ga.; Clackamas Community College, Oregon City, Ore.; Colorado College, Colorado Springs, Colo.; Graceland College, Lamoni, Iowa; Lindsey Wilson College, Columbia, Ken.; Monmouth College, Monmouth, Ill.; Mount Holyoke College, South Hadley, Mass.; and Palm Beach Atlantic College, West Palm Beach, Fla. In 1985, five colleges will be selected to receive $2500 awards, based on their submitted proposals, for the purchase of scientific equipment, audiovisual and other teaching aids, and for library materials to be used in the

Program teaching of science a t the undergraduate level. Further information about the 1985 awards appears in the January issue (p. 49 A). Advance registration is urged. The deadline for advance registration is Feb. 2, 1985; registrations received after that date will be processed and the registration package made available in the convention hall a t the advance registration desk, but they will be subject to payment of the on-site registration fee. Registration forms may be obtained from John Queiser, Registration Chairman, 2523 Greenboro Lane, Pittsburgh, Pa. 15220. Registration fees are as follows: $30 for advance registration; $50 for registration a t the conference; $10 for students; $10 for advance and $15 for onsite registration for spouses; and $10 for admission to the exposition only. An expanded continuing education program will again be offered including a short course, six mini courses, and a workshop. Final arrangements and registration information will appear in the preliminary program. In addition, the American Chemical Society is sponsoring 20 short courses in New Orleans in conjunction with the conference. For additional information on ACS short courses, see the December 1984 issue of ANALYTICAL

Longue V u e Gardens, a privately owned estate i n N e w Orleans, is located within m i n u t e s of Canal Street CHEMISTRY(p. 1562 A) or contact the Department of Educational Activities, American Chemical Society, 1155 16th St., N.W., Washington, D.C., 202872-4508. An employment bureau will again be available to regular conferees and students during the conference. Preregistration information for prospective employers and candidates will be

included in the preliminary program. The Spouses Committee has planned varied activities for the spouses of conferees. The Spouses Hospitality Suite will be in the New Orleans Hilton and will be open daily to registered spouses. For information, contact Billie Weill, Spouses Program Chairman, 10 Rodgers Drive West, Pittsburgh, Pa. 15238. (continued o n page 138 A )

Conference Officials 1985 Board of Directors President: Allen Sharkins President-Elect: Richard Danchik Elected Designate-Immediate Former President: Robert Baudoux Chairman, Spectroscopy Society of Pittsburgh: John Jackovitz Chairman-Elect, Spectroscopy Society of Pittsburgh: Jane Judd Chairman, Society for Analytical Chemists of Pittsburgh: Ann Cibulas Chairman-Elect, Society for Analytical Chemists of Pittsburgh: Gerald Carlson Treasurer: Victor Zadnik Assistant Treasurer: John Auses Secretary: Richard Obrycki

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Allen Sharkins President

Richard Danchik President-Elect

Victor Zadnik Treasurer

Peter Castle Exposition C h a i r m a n

Paul Bauer Program C h a i r m a n

John Queiser Registration Chairman

ANALYTICAL CHEMISTRY, VOL. 57, NO. 2, FEBRUARY 1985

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10 45 1016) Microorganism Characterlzatlon by Multi-Product Fluorescence Rate Analyses-A P SNYDER 1 T Wang Dept of the Army D B Greenberg

Monday, February 25, 1985 SYMPOSIUM

11 00 tot71 Prellmlnary Studies 01 Optical Flber-Based Biorensors-M A University o f Iowa

ARNOLD

11 15 10181 Choline and Acethylchollne Sensor lor Brain Extract Analysls-M

MASCINI

D Moscone G Palleschi Unlversith di Roma Tor Vergata

TOXIC Waste Analysis/Water Pollution Analysis -arranged

by H v Drushel,

Exxon Research and Development Laboratories

11 30 10191 Revolutionary, New Amlno Acld Analysis by Both Cation and Anion Exchange Chromatography-J KORPI C LinCOln DiOnex Corporation

Monday Morning, Room 44 Y Drushel Presiding

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Introductory Remarks-H V DRUSHEL

9 05 (0011 Directing and Managing the EPAs Contract Laboratory Program-s P KOVELL R R Thacker US Ervironmental Protect Agency

9 4C Agency

10021 EPAs National Dioxin Study-4 E DUPUY JR

US Env ronmental Protect

10 15 IC031 An Evaluation 01 Promulgated AnaIytIcaI Methods for Priority POllutantS and Appendix vlll Compounds-J E NORRIS CIEA GElGY Corp

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11 OC io041 Evolution of Gas Chromatography-Mass Spectrometry Analytlcal Methods lor Analysis of Pollutants in Water-W A TELLIARD US Environmental Protect Agency D R Rtishneck I t 35 0051 Integration 01 GC. GCMS, and AAS Analytlcal Results with Data Interpretation and Display Formats lor Environmental Monitoring Studies-E E OVERTON LoLisiana State University I R Deleon C J Eyrne C F S l e e k

Monday Morning, Rooms 33/35 G Schomburg Presiding Max Planck institute tor Coal Research

9 00 1020 Separation and Identlllcatlon of Polychlorlnated Dibenzo-p-Dioxlnes and Dlbenzofuranes Using Multidimenaional Gas Chromatography at High Efllciency-G SCHDMEURG H Husmann Max-Planck inst Iur Kohlenlorschung 9 15 (021 Unique Application of a Two-Oven Gas Chromatograph-J 0 WALKER S M Sonchik IEM lnslrurnents Inc 9 30 1022 Two Oven GC Applications Comparing Valveand Valveless Switching-S SONCHIK J 0 Walker l6M Instruments inc

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9 45 (0231 The Analysis of Oxygenated Compounds in Gasoline by Multldimensional Capillary Goa Chromatography-J WASSDN HachICarle Chromatography

SYMPOSIUM

10 00

Advances i n Mass Spectrometry.

arranged by A.G. Sharkey, Plttrburgh Enerpy Technology Center1U.S. Department 01 Energy ~~

Monday Morning, Room 28 A Sharkey Presrding A MCCLOSKEY Un versity 01 Jlah 9 4C 10071 Secondary ion Mass Spectrometry ot Biomolecules-A BENNINGHOVEN der Uniiersitat Munster

RECESS

10 15 (0241 Peak Clusterlng lor PNA Accuracy Improvcment-H SPAANS A C Analytical Controls B V 10 30 (0251 Determination of Trace Components with Coupled Column Systems in a Double Oven GC-A C HEIM J K Goekeler M S Alper ES Industries 10 45

9 00 Introductory Remarks-A G SHARKEY 9 05 (0061 Biochemistry and Mass Spectrometry-J

13 15

Development and Application of Multidimensional Gas Chromatography

0261 Naphtha Analysis The Advantages 01 a Multiple Packed Column Method-

E G EOEREN Packard Instrument B V 11 00 102i! The Analysis 01 C h C 4 Alcohols and MTBE In Motor Gasolines by MultiDimensional G C with Macro-bore Capillary Column and Micro Packed Column-L Hewlett Packard Co Z Naizhong

GREEN

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I O 30 10081 Negative Chemical ionization Mass spectrometry Analytical Chemistry-R C DOUGHERTY Florida State University

In En*ironmental

1 1 05 10091 Ouantitative Applications 01 Thermospray LC1MS-A L Liberato k V Esteban Nat I Ins1 of Health

YERGEY

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General Analysis I Monday Morning, Room 8

9 00 i028r A Scheme tor the Separation, Characterization and Analysis 01 Detergent Formulations A Multi-Technique Approach-W C CAMPBELL H Hinchcliffe IC1 PLC

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Biochemical Analysis

9 15 10291 Niobium Nuclides In Nuclear Power Plant Waste-S Science Applications Inc

Monday Morning, Room 13 N Alperf Presid n g 9 00 l O l O I Binding Proleinsas Reagentsln Enzyme-Linked Competitive Binding Assays -M E MEYERHOFF L G Eachas Universitj of Michigan 9 15 I0111 Amino Acid Analysis Using Phenyl Isothlocyanate Matrix Ellects on Amino Acid Yields and the Influence 01 Reacllon Conditions-S A COHEN T L Tariin D L 6owles B A Bidlingmeyer Waters Chrom Div Millipore

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9 3c 10121 Colorimetric Determination 01 -Carboxyglutamrc Acld in the Presence 01 Other Amlno Acids-0 K MORGAN Y P Wti N D Danielson Miami University J L Glaich 9 45 10131 Separation of Blologlcal Macromolecules by Reversed Phase and Size Exclusion Chromatography-A GOLDBERG E I du Pont de Nemours & Go 10 00 10141 Chromatographic Prollllng Measurements Related to Diabetes and Starvation Conditions i n Experimental Anlmals-M YANCEY R Stuart D Wiesler M Novotny Indiana University 10 15

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10 30 10151 Considerations In Using Stable Isotopes 01 Selenium in Metabolic Tracer Studies-C VEILLON S A Lewis 0 A Levander P A McAdam N Hardison L Wood U S Dept 0 1 Agriculture K Helzlsouer

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ANALYTICAL CHEMISTRY, VOL. 57, NO. 2, FEBRUARY 1985

S HAY K L Wright

9 30 0301 A Thermal Soil Desorptlon/Metal Foil Collectlon1Flash VaporizationIFlame Photometry Technique lor Mineral and Petroleum Explorallon-C J EARINAGA S 0 Fa well University 01 Idaho 9 45 10311 Novel Analytical Applications of UV Light Photolysis to Organic Elemental Analysis-D V VINJAMOORI Monsanto C o 10 00 10321 Certillcation 01 a Diesel ParlIcuIate Standard Relerence Material-L HILPERT WE May W F Kline H X Gu National Bureau of Slandards 10 15

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0331 The Determination 01 Carbon Contamination Metal Sur(aCeS with an Automated Elemental Analyzer--9 F CULM0 The Perkin Elmer Corp 10 45 0341 Comparison 01 Elliclencies of Methods Yielding Rate l r o m Data Following A 1030

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B-A H KALANTAR G H McKinnon C J Backhouse University Of Alberta

11 00 035) Spectral Studies01 Ditellurato Ferrate (Ill)Complex-H University 01 Calcutta L C W Baker

G MUKHERJEE S De

11 15 036) Synergic Extraction and Spectrophotometric Determlnatlon 01 Titanium (1V)p-C P SAVARIAA K Vijayan University of Calicut

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SYMPOSIUM Biomedical InfraredSpectroscopy: The BiomedicalApproachW R.J.

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SYMPOSIUM

New Instrumentation Frontiers Monday Morning, Room 10

Biomedical Infrared Spectroscopy The Biomedical A p p r O a C h - a r r a n g e d

A Pebier Presidrng

by R J Jakobaen. Batteiie-Coiumbur Laboratorlea Monday Alternoon, Room 28 R M Gendreau Presiding Battelie-Columbus Laboratories

Westinghouse Research 8 Development 9 0 0 (0911 A New AmmoniaAnalyzer-D E BURGE Wescan instruments Inc R M Carlson 9 15 (092) Rapid Scan Fourier Tranrform ion Mobility Spectrometry-W F SIEMS F J Knorr R L Eatherton H H Hill Jr Washington Slate University

9 30 1093) Organochlorlde Optrode lor Underground WaIer Conlaminatlon DetectionF MILANOVICH H Miller T Hirschfeid Lawrence Livermore National Lab 9 45 (094) Use 01 Low Temperature Magnetic Circular Dlchrolrmaaan Oplicai Probaol Metal Centerr I n Bloioglcal Syatemr-D

BENNETT M Johnson Louisiana State University

10 00 1095) Reactor Thermionic i o n i u l i o n A n a l y r i r o l Solidand Llquid Subrtancea-P t PATTERSON Detector Eng 8 Tech Inc 10 15

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1030 (096) Fault Goa Datocllon In 011-Fllled Power Tranrtormera-A Westinghouse R&D Center R Kurz

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1045 (0971 A New Viscority Mearuring Unlt with Precirion Senaing. for Making Mearurementr on Ail Klndr 01 Llquida-M RUFINO Schott America M Detemple H Hiibner 11 00 (098) Caplllary Zona Electrophorealr I n Non-Aqueoua and Mixed Medla-Y WALBROEHL J W Jorgenson Univ North CarolinaiChapel Hill 11 15 (099) A New Compact Titrator lor Dedicaled Applicatlona-P FRUH Mettier lnstrumenle AG 11 30 (099Ai A New Automated Sampling Syrtem lor u r e wlth ion Chromatographa-D MAR J P Rouland J Thompson B Evans Dionex Corporation

2 20 (120) Modeling olProteln Adaorption from FT-IRIAlr Data-K Columbus Labs

K CHITTUR Battelle

2 55 (121) Qualitative and Quantltatlve Monitorlng 01 Fermentatlon Media by FT-IRJ C ALBERT1 and J A Phillips Lehigh University 330 RECESS 3 40 (122) FT-IR Studlea 01 Blood Proteln-Anticoagulant Binding-A D ORAM J s Schultz University of Michigan 4 15 (123) Klnetica 01 Fibrinogen Adaorpllon Behavlor using FT-IR-S M SLACK T A Horbett University of Washington

SYMPOSIUM Computers in Analytical Instrumentation: Towards Intelligent Tools for the Laboratory. arranged by J.P. Avery, University 01 Colorado and S.R. Crouch, Michigan State Univeraity Monday Alternoon, Room 40 J Avery and S Crouch Presiding

POSTER PRESENTATIONS

1 4 5 1124) Elements 01 the New inatrumentation Science-S R CROUCH Michigan State Universit)

Poster Papers will be on display from 9:30 AM4:OO PM. Authors will be available from 2.90 PM4:OO PM. Posters

1 45 (119) Perapectlves 01 Biomedical FT-IR and Current Rerearch at Balleiie-R J JAKOBSEN Battelle-Columbus tabs

2 20 (125) Mlcrocomputera and Mlcrocomputer Subryaleml lor Intelligent Laboratory inatrumentallon - A Unlque Synergirm-G HORLICK University o f Alberta

- Gas-, Ion, 7Xin Lager-,and Liquid Chromatography

2 55 (126) Chemirtry and the Smart inrtrument-P DRYDEN Hewlett-Packard Corp 3 30 RECESS 3 40 ,127) Artificial intelligence, Expert Syrtems lor Acquiritlon and interpretation 01 Data in Analytical Chemistry-c

Monday, Rooms 23 and 29 1100) Application of G U M S and GC/Mi/FTiR lo Fluid Degradation Studlea-A BOPARAI G T Reedy Argonne National Lab

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WONG Lawrence Livermore National Labs

4 15 ,128) The Laboratory information Package' The Electronic Olflce, Data Baser and Expert Syatemr lor Sclentirta-K CASERTA Procter and Gamble Corp 4 50 PANEL DISCUSSION-Computer. i n the Laboratory: Where Do We Go From Here?v?-J P AERY S R Crouch G Horlick P Dryden C Wong K Caserta C G Enke

(101) Environmental Anaiyrir by GCiMatrix IrolationiiR-J F SCHNEIDER G T Reedy D G Ettinger Argonne National Lab (102) Anaiyrls 01 Flavor VoiaIiiea in Alcoholic Beverager-R G WESTENDORF Tekmar Co (103) A Headapace Capillary Gar Chromatographic Semi-Quantitative Screening Method lor Voialiler In Aqueoua Fooda-H C HOLLlFlELD C V Breder FDA 1104) Methoda lor the Analysis of Glycols in Water-D F CLARK M F Martin J C Peterson N Wieser Bureau o f Chemistry 1105) Sample Pretreatment Technlquer lor Food Analysis by Single Column ion Chromatography-R W ANDREWS R M Griffin R Keenan J Morrison C W Schubert E W Zink ESA inc

(1061 Appiicalion of Single Column ion Chromatography to the Produclion of High Purity Water and Semiconductor Materials-C McCRORY-JOY ATBT Bell Labs

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(106A) Gradient Elution in Ion Chromatography-R Heberiing Dionex Corporation

ROCKLlN J Stillian J Riviello

11071 Solvent Optimization i n HPTLCof Drugs-M L BLACKMON M R Beckert K 0 Holmes Jr Burroughs Wellcome Co (1081 Quantitative Burroughs Weilcorne Co

Thin

Layer Chromatography-6

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(109) Deconvolutlon 01 Three Overlapping Chromalographic Peaka-R F LACEY Hewlett-Packard Co

SYMPOSIUM Microbore Liquld Chromatography- arranged by J.Q. Walker, iBM instruments Monday Afternoon, Room 44 J 0 Walker Presiding 145 11291 lntroductlon and Overview-J

0 WALKER

2 20 1301 State 01 the Art. Microbore Liquid Chromatography-J Edinburgh

H KNOX University O f

2 55 1131) Syatem Design Conriderations lor Microbore HPLC instrumentation-J HiGGlNS R G Brownlee H E Schwartz Brownlee Labs inc

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3 30 11321 Unique Applications 01 Microbore HPLC-R A HARTWICK Rutgers University

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RECESS

4 15 1131 Analytical Capabiiitier Associated with the Liquid-Chromalographic Columns of Capillary Dimenrions-M L NOVOTNY Indiana University 4 50 (134) Conventlonai HPLC

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Microbore LC-L R SNYDER Lloyd R Snyder Inc

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1110) HPLC Melhod Development Using Simplex Optimization-K J PLATT 0 J Thoennes American Cyanamid Co

Application and Measurement of Gas Chromatographic Retention Indices/New Column and Stationary Phase Technologies

(111) New Rigid Polymer Baaed HPLC Packing8 lor Mono/Oligo/Poiy Saccharide Anaiyria-F P WARNER L L Lloyd T N Tweeton Polymer Laboratories Lld (112) Resolution 01 Enantiomerr by HPLC on Poiysaccharides Derivatives-Y YUKi T Shibata I Okamoto A lchida H Namikoshi Y Toga Daicel Chemical Ind Lld

Monday Afternoon, Room 36 C M White Presiding United States Department of Energy

1113) Ultratrace Speciation of Organometallic Speciea i n Natural Systems, Using

P -Bore and Capillary Technlquer wlth an Epiliuoreacence Mlcroscopic Imaging DetectorE J PARKS W R Blair G J Olson F E Erinckman National Bureau of Standards M C Vaieiras Price J C Means (114) Electrochemical Detection 01 Purinerand Pyrimldinea-E G E JAHNGEN JR T Tougas D P Maiiiaros M J DeBenedetto University of Lowell (115) Meaaurement 01 Antioxidant Mixtures by Thermospray MCFADDEN S Lammert J Wellby Finnigan MAT

LC/MS-W

1 45 (1351 Gas Chromatographic Retention information Used lor the Prediction of Chemical, Physical, and Thermodynamic Properties of Polycyclic Aromatic HydrocarbonsC M WHITE U S Dept of Energy

2 00 (136) Applications ot a Capillary GC/Retentlon index Llbrary-S LEU J F SprOUSe A Varano S Stephenson Sadlier Research Labs 2 15 1137) Assessing the Accuracy of Capillary Gar Chromatography lor Eatimating Vapor Presaurea 01 Pesticides and Induatrlal Organic Chemicals-T F BIDLEMAN National Swedish Environmental Protection Board

(116) The Liquid Chromatographlc Analysis of Acidic Drugs Uslng an ion-Pairlng Extractor-J R LANG University of Tennessee

2 30 (138) Vapor Presrure Estimates 01 PCB Isomers and Commercial Fluids lrom Gar Chromatographlc Retention Data-'& T FOREMAN T F Bidleman University of South Carolina

1117) Determination of Butylated Hydroxyl Anisole i n Dehydraled Food Products by HPLC with a Dual Coulometric Detector-C J HSU D T Munsey Carnation Rsh Lab

2 45 (139) Computerized Gas Chromatography Analysis Based on Calibrated Peaks andReiativeRelentlon Indices-V C STAMOUDIS K C Picel D I Eikens J C Demirgian Argonne National Lab

(118) Optimization 01 3 iim LCEC System for Biogenic Amine Analyses-C L BLANK P Y T Lin University of Oklahoma

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ANALYTICAL CHEMISTRY, VOL. 57, NO. 2 , FEBRUARY 1985

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