Reactions of 2-phenylethyl and 3-phenylpropyl carbinols with

J. Org. Chem. 1990,55, 1338-1344

1338

Table V. HPLC Analysis of the Four Amide Products internal standard amide liquid phase tR, 8 (tR,5) 5 50 vol % CH30H-H20, 0.1 269 2-chloro-5-hydroxyM "AN09 toluene (798) 6 66 vol %'CHiOH-H20, 0.1 402 none used M ",NO, 7 20 vol %-CHiOH-H20,0.1 685 p-ClCsH4S0