Electrocatalytic reduction of carbon dioxide by associative activation

Sullivan, Holden. Thorp, Terrence R. O'Toole, Alison. Downard, and Thomas J. Meyer. Organometallics , 1988, 7 (1), pp 238–240. DOI: 10.1021/om00091a...
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Organometallics 1988, 7, 238-240

238 Scheme I11

Scheme IV

PhMeSiFa- K' -b-crown-6

PhpSdOMe)p

+

I-PrMgBr (2 equiv)

PhMezSiF; K*-18-crown-6

THF 7 Ph28(/-Pr)OMe

17 */e

17 h

a. MrMgBr (1 cquiv) Et 2 0 ,-30 'C I < 5 min