Contents
VOL.
18,
J A N U A R Y / F E B R U A R Y 1970
5
Residual Lime Effect in Soils on Certain Mineral Elements in Barley, Fescue, a n d Oats Nelson O. Price and W. W. Moschler
9
Enzymatic Solubilization of Nitrogenous Constituents of M u n g Beans Y. D. Hang, W. F. Wilkens, A. S. Hill, K. H. Steinkraus, andL. R. Hackler
13
N o n e n z y m a t i c Browning in a Lactose-Casein Model System A/do Ferretti, V. P. Flanagan, and J. M. Ruth
19
Volatile C o m p o n e n t s of Bartlett Pear. Higher Boiling Esters R. K. Creveling and W. G. Jennings
25
F a t t y Acid Composition of Oils of Some Edible Seeds of Wild Plants Carola Engelter and A. S. Wehmeyer
27
Phenolic a n d Sugar C o m p o n e n t s of Armavirec Variety Sunflower {Helianthus annum) Seed Meal K. L. Mikolajczak, C. R. Smith, Jr., and/. A. Wolff
33
Proximate Composition and Proteins of Three G r a i n Sorghum Hybrids and Their Dry-Mill Fractions R. W.Jones and A. C. Beckwith
37
Protein Composition of Proso Millet R. W. Jones, A. C. Beckwith, U. Khoo, andC. E. /nglett
40
Hemicelluloses of Milled Rice A. V. CartanoandB. O.Juliano
43
Effect of Commercial Processing Techniques o n Lindane- and D D T - 1 4 C Residues in Rapeseed Oil J. G. Saha, M. A. Nielsen, and A. K. Sumner
45
Structure Activity Analysis of Some Ο,Ο-Dialkyl (p-Methylthio, /?-Methylsulfonyl) Phenyl Phosphates and Phosphorothioates Prepared for Their Insecticidal Activity W. B. Neely, W. E. Allison, W. B. Crummett, Kenneth Kauer, and Walter Reifschneider
50
Synthesis a n d Microbial Toxicity of Dinitrobutadienes and Related C o m p o u n d s J. A. Durden,Jr., D. L. Hey wood, A. A. Sousa, and H. W. Spurr
57
Synthesis a n d Nematocidal Activity of 2-Pyridyl Alkanesulfonates Martin Hamer, C. W. Huffman, and S. S. Ristich
60
Herbicidal Activity of 1,3,4-Thiadiazole Derivatives Hiroshi Kubo, Rokuro Sato, Isao Hamura, and Takuo Ohi
66
Acetylcholinesterases of Organophosphate-Susceptible and -Resistant Spider Mites H. R. Smissaert, Simon Voerman, Lies Oostenbrugge, and Nel Renooy
NO.
1
©
C O P Y R I G H T
EDITOR: PHILIP Κ. BATES ADVISORY BOARD Evan F. Binkerd, Ricardo Bressani, Ron G. Buttery, Edgar A. Day, Francis A. Gunther, John H. Nair, III, Alvin B. Phillips, W. F. Phillips, E. Y. Spencer, Cecil H. Van Etten, J. Wade Van Valkenburg, Jr., Emily L. Wick
2 J. AGR. FOOD CHEM.
1970
BY
THE
AMERICAN
CHEMICAL
SOCIETY
EDITORIAL HEADQUARTERS 1155 Sixteenth St., N.W. Washington, D.C. 20036 Phone 202-737-3337 Teletype WA 23 Manager, Manuscript Reviewing: Katherine I. Biggs Assistant Editor: Norma Yess
AMERICAN CHEMICAL SOCIETY PUBLICATIONS
PRODUCTION OFFICE 20th and Northampton Sts. Easton, Pa. 18042 Manager: Charles R. Bertsch Assistant Editor: Elizabeth R. Rufe
Publication Manager, Journals: David E. Gushee
Director of Publications: Richard L. Kenyon Director of Business Operations: Joseph H. Kuney
Contents Continued 148
Rapid Determination of Sorption Affinity of Phosphine by Fumigation within a Gas Chromatographic Column B. BerckandF. A. Gunther
154
Determination of Carbaryl as an Amide Derivative by Electron-Capture Gas Chromatography R. L. Tilden andC. H. Van Middelem
159
Determination of Residues of GC-9160 in Cabbage, Lettuce, and Citrus Fruit Annemarie Westlake, W. E. Westlake, andF. A. Gunther
162
Disappearance of Malathion Residue in Broccoli during Cooking and Freezing Lois Kilgore and Frances Windham
164
Flame Photometric Determination, Extraction, and Cleanup Procedures for GS-13005 [0,0-Dimethyl-S-2methyloxy-l,3,4-thiodiazol-5-(4//)-onyl-(4)-methyl-dithiophosphate (4)] and Metabolite Residues in Egg Yolk and Poultry Feed R. W. Young
168
Distribution of Dieldrin- 14 C in Pheasant Tissues after a Single Administration D. W. Lamb, Y. A. Greichus, and R. L. Linder
172
Stereochemistry of Ring A in Gibberellic Acid as Indicated by Use of Nuclear Overhauser Effects Nagabhushanam Mandava and E. L. Gooden
COMMUNICATIONS 174
Whiskey Composition : Formation of a- and/3-Ionone by the Thermal Decomposition of/3-Carotene E. G. LaRoe and P. A. Shipley
176
Determination of Carbonyl Concentration in Aqueous Citrus Essences Yigal Peleg and Chaim H. Mannheim
178
Determination of Dursban Insecticide in Water, Mud, Vegetation, Fish, Ducks, Insects, and Crustacea M. E. Dûsch, W. E. Westlake, andF. A. Gunther
180
Sulfate Ester Conjugates: A One-Step Method for Replacing the Sulfate with an Acetyl Group G. D. Paulson and C. E. Portnoy
182
Identity of the Pisum Gibberellin Yosh Kimura
183
Guide for Authors
184
Gas Chromatographic Methods
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