Nov. 5, 1952
FREERADICAL REARRANGEMENTS IN DECARBONYLATION OF ALDEHYDES
5381
drazine sulfate solution to ethanolic solutions of the fracB~~~~~~~ for his interest and adprofessor tions. After chromatography 011 alumina followed by two crystallizations from ethyl acetate-95% ethanol this was vice during the present investigation and Dr* A* obtained as deep orange needles, m.p. 248.5249' ( d e ~ . ) , ~ *Vandenheuvel, Atlantic Fisheries Experimcntal undepressed on admixture with an authentic sample. Station, Halifax, N. S., in whose laboratory thc
initial observation was made.
(48) C . F.I