BRIEFS arching s c i ^ " ^ e r !
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Off-Line Optimization of Gas Chromatographic Temperature Programs 2420 R e s u l t s from t h e c o m p u t a t i o n a l optimization agree w i t h exp e r i m e n t a l optimizations. O p t i m i z a t i o n behavior near t h e limits of allowable settings is discussed, a n d r e c o m m e n d a tions are m a d e for its handling. Eric V. Dose, Environmental Science and Engineering, Inc., Gainesville, Fla. 32602 Anal. Chem., 59 (1987)
Statistical Approach to Solvent Selection as Applied to TwoDimensional Thin-Layer Chromatography 2424
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A m e t h o d is described for predicting t h e probability t h a t a given solvent system is t h e b e s t of a set of solvent systems for separating a given m i x t u r e of solutes by two-dimensional thin-layer c h r o m a t o g r a p h y . David Nurok* and S o h r a b Habibi-Goudarzi, Department of Chemistry, Indiana University-Purdue University at Indianapolis, P.O. Box 647, Indianapolis, Ind. 46223, and Robert Kleyle, Department of Mathematical Sciences, Indiana University-Purdue University at Indianapolis, P.O. Box 647, Indianapolis, Ind. 46223 Anal. Chem., 59 (1987)
Preparation and Evaluation of Slurry-Packed Capillary Columns for Normal-Phase Liquid Chromatography 2428 P a c k i n g p r o c e d u r e s for obtaining high-efficiency LC microcolumns with silica a n d polar chemically b o n d e d p h a s e s of t h e diol, cyano, a n d a m i n o t y p e are described. F r a n c a Andreolini, Claudio B o r r a , and Milos Novotny*, Department of Chemistry, Indiana University, Bloomington, Ind. 47405 Anal. Chem., 59 (1987)
Correspondence Storage Stability of Formaldehyde Solutions Containing Pararosaniline Reagent
2432
P a r i s E. Georghiou*, Department of Chemistry, Memorial University, St. John's, Newfoundland, Canada A1B 3X7, and Linda Winsor, Geortec, Ltd., 58 LeMarchant Road, St. John's, Newfoundland, Canada A1C 2G8, and Cliffe J . Shirtliffe and J a n a Svec, Institute for Research in Construction, National Research Council of Canada, Ottawa, Ontario, Canada K1A 0R6 Anal. Chem., 59 (1987)
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1,1,3,3-Tetramethyl-1,3-bis(octadecyl)disiloxane. an Artifact Found on Octadecylsilica-Packed Chromatography Columns 2435 Uffe Anthoni, Charles Larsen, P e r Halfdan Nielsen, and Carsten Christophersen*, Marine Chemistry Section, The H. C. 0rsted Institute, University of Copenhagen, Universitetsparken 5, DK2100 Copenhagen, Denmark Anal. Chem., 59 (1987)
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1128 A · ANALYTICAL CHEMISTRY, VOL. 59, NO. 19, OCTOBER 1, 1987