Introduction to Microwave Sample Preparation: Theory and Practice

May 30, 2012 - Introduction to Microwave Sample Preparation: Theory and Practice. Anal. Chem. , 1989, 61 (3), ... C&EN Online News. C&EN Online Curren...
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The Kinetics of Environmental Aquatic Photochemistry

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ere at last—a single-volume source on the theory and practice of the kinetics of environmental aquatic photo­ chemistry. Get a solid foundation on this fast developing field with easy-to-understand explanations on such topics a s . . . kinetics of direct and indirect (sensitized) Aau"* tic photoreaction in aquatic media in the environment... absorption and transmission of sunlight in the atmos phere and in natural body water... m, measuring rates of direct and indiI rect aqueous photoreaction... >>aam. ^ ^ a ^ a v r a V a v a a H B a V a V actinometry in dilute aqueous solutions... and more. Learn more on experimental procedures for obtaining requisite kinetic data. Become more familiar with the mathematical concepts through simple, step-by-step derivations. Examples are also provided that illus­ trate how to use data from experiments when estimating rates of photo­ reaction. Tables of solar irradiance as a function of latitude and season of the year in the northern hemisphere also are given. Get complete and practical information on determining direct and indi­ rect (sensitized) photoreaction rate constants and half-lives with this handy and useful reference. by Asa Leifer, PhD. ACS Professional Reference Book ISBN 0-8412-1464-6 LC 88-16718

336 pages (1988) Clothbound US & Canada $59.95 Export $71.95

Order from: American Chemical Society. Distribution Office Dept. 96 1155 Sixteenth St., N.W., Washington, DC 20036

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Introduction to Microwave Sample Preparation: Theory and Practice

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ew microwave techniques are making sample preparation procedures faster, more convenient, and more controlled. This revolutionary new book gives you what ' you need to know to get started.. the history of the technique, the relevant methodological details, the all-important safety precautions, and a number of specific applications. Eleven chapters describe equipment and techniques that have been found most effective. They offer direct practical applications of the meth-1 ods to a variety of sample types, including microwave digestion of botani­ cal, biological, and food samples; selenium analysis; Kjeldahl nitrogen determination; remote operation of microwave systems; and more. As a unique feature, this book presents a fundamental thermodynamic equa­ tion relating acid (sample) size, final temperature, heat capacity, and transformations of the basic equation predicting time and temperature for digestion. A truly multi-disciplinary volume, this book can be used in inorganic ele­ mental analysis, sample digestion, food analysis, environmental sample preparation chemistry, and other areas. H.M. Kingston and L.B. Jassie, Editors ACS Professional Reference Book 300 pages (1988) Clothbound ISBN 0-8412-1450-6 LC 88-8139 US & Canada $49.95 Export $59.95 Order from: American Chemical Society, Distribution Office Dept. 95 1155 Sixteenth St., N.W., Washington, DC 20036

800-227-5558

PITTCON 9:50 (1241) Detection of Solvent Vapors Using Piezoelectric Sensors and Surface Acoustic Wave Devices—D.A. GUSTOWSKI. Louisiana State University. L.H. Grande, H.P. Dharmasena, P. Klinkhachorn. C.S. Milan, G.R. Newkome, E.B. Overton 10:10 RECESS 10:25 (1242) A Novel GC Laser-Based Detector—J.Β MORRIS. US Army Ballistic Research Lab, BE. Forch, R.C. Sausa, AW. Miziolek 10:45 (1243) A New Burner for Flame Atomic Absorption Spectrometry— DE. SHRADER, Varian Associates. J.B. Willis, B.O. Frary, B.T. Sturman 11:05 (1244) Optimization of a New Flame Infrared Emission (FIRE) Detec­ tion System lor Chromatography—D.C. TILOTTA, Baylor University, R. Srinivasan, MA. Busch, K.W. Busch 11:25 (1245) Rapid Analysis and Archiving of TLC Plates Using Video Densitometry—P.B. OLDHAM, Mississippi State University, J.S. Bernstein 11:45 (1246) Remote Sensing of Chemical Carcinogens Using a Microscale Regenerable Biosensor—M.J. SEPANIAK, University of Tennessee, A.M. Hoyt, J.P. Alarie, T. Vo-Dinh

Laboratory Robotics Thursday Morning, Room 157 P. Cole, Presiding CAP Industry Limited 8:30 (1247) Standard Robotics Methods Using Knowledge Frames—JR. LEE, Kansas State University, T.L. Isenhour, J.C. Marshall 8:50 (1248) Automated Pesticide Residue Analysis Using Laboratory Robotics R. JOHNSON, Zymark Corporation 9:10 (1249) Application of Laboratory Robot to Fire Assay for Precious Metals Analysis—J. B0ZIC, Inco Ltd., R. Delvecchio, P. Donato 9:30 (1250) Residual Chlorine Analysis Using an Artificial Intelligence Driven Robot System—S.E. ECKERT, Kansas State University, T.L. Isenhour 9:50 (1251) Software for Robotics: A New High Level Natural Chemistry Operating Environment—S MATHES, Intellibotics, Inc., L.S. Yago 10:10

RECESS

10:25 (1252) Fully Automated Tablet Dissolution Testing—Basket and Pad­ dle Methods—A.M. PAUL, Zymark Corporation, K.A. Tucker, C. Werner 10:45 (1253) The Development and Optimization ol Sample Preparation Procedures Employing a Robotic Workstation—P. TIMMONEY, MilliLab/Waters Chrom. Division, P.C. Beals, S. Newton 11:05 (1254) A Fully Automated Sample Preparation and HPLC Analysis System tor Theophylline and Its Major Metabolites from Serum—J.J T0MLINS0N, Zymark Corporation, B. Lightbody 11:25 (1255) A Robotic and Vision System for the Microbiological Assay ol Clinical Samples—J. ZYNGER, Eli Lilly and Company, R.J. Lykins, D.L. Coleman, C.L. Winely 11:45 (1256) Fully Automated Microplate Management System for Biotechnology—D.C. LAPEN, Zymark Corporation, CM. Cuthbert

Liquid Chromatographic Analysis of Food and Radiopharmaceuticals Thursday Morning, Room 363 D. Dalsis, Presiding The Coca Cola Company 8:30 (1257) Liquid Chromatographic Characterization and Biological Dis­ tributions ol Technetium Labeled Phophonacetic Acid Radiopharmaceuticals— M.A.A. NASSER, University of Cincinnati, E. Deutsch, W.R. Heineman 8:50 (1258) Observed Binding of 99m-Technetlum Radiopharmaceuticals to Human Serum Protein as a Function of Internal Surface Reversed Phase HPLC Column Length—L.L. WEYMAN, University of Cincinnati, E. Deutsch 9:10 (1259) Internal Surface Reverse Phase HPLC Analysis ol the Protein Binding and Metabolism of 99m-TcCI(Dioxlme)3BR Complexes In Serum—W HIRTH, Squibb Instit. for Medical Res., S. Jurisson, D.P. Nowotnik, AD. Nunn 9:30 (1260) Determination of the C I — > OH Exchange Rates of Techne­ tium Dioxlme Complexes—W. HIRTH, Squibb Instit. for Medical Res., S. Jurisson, K. Linder, T. Feld. AD. Nunn 9:50 (1261) Use of an Integrated HPLC System for Radio-Labeled Metabolites—L.L. R0BISON, Beckman Instrument, Inc., J. Quint 10:10 10:25 (1262) EM Science

RECESS Ion Interaction HPLC of Foods and Beverages—L. HENRICH.

10:45 (1263) Separation and Determination of Copper(ll) and Chlorophyllin and Iron(lll) Chlorophyllin by High Performance Liquid Chromatography—K. FURUYA, Keio University, H. Inoue, T. Shirai

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220 A · ANALYTICAL CHEMISTRY, VOL. 6 1 , NO. 3, FEBRUARY 1 , 1989