Laboratory Manual for First Year College Chemistry - Journal of

Laboratory Manual for First Year College Chemistry. William E. Morrell. J. Chem. Educ. , 1953, 30 (1), p 48. DOI: 10.1021/ed030p48. Publication Date: ...
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JOURNAL O F CHEMICAL EDUCATION 0

LABORATORY MANUAL FOR FIRST YEAR COLLEGE CHEMISTRY

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John W. Barker, Professor of Chemidq, Wittenberg College, and Carthage College. Paul K. Glasoe, Professor of Che-, 186 pp. McGraw-Hill Book Co., Inc., New York, 1951. xi 21.5 X 28 cm. $3.

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LABORATORY MANUAL FOR BRIEF COLLEGE CHEMISTRY

Leon B. Richardson, Emeritus Professor of Chemistry, Dartmouth College, and Andrew J. Scarlett, Professor of Chemistry, Dartmouth College. Revised edition. Henry Holt and Co., New 232 pp. 18 figs. 21.5 X 28 cm. Spring York, 1951. viii binding. $2.

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"THIS laboratory manual is designed to provide s full year of THE51 emeriments in this manual are of varvine leneth and laboratory instruction consisting of six hours of laboratory time ner , . - week. - - ~ The first half is devoted to a studv of the chemistrv ol somp impwtrrut r~onmrt?lsand thr demon~rmrionoi rl~mm~c:~l prinriplw ullidt are t,s.icntiaI for the nndcrsr:~ndingof il.vrnic.tl tlsurL.i HMI I,,u.z.. T1.c CWOIIII hnlf dcd'1 with qu.~litiativt!9naly- in experiments and directions concerning technique are kept to sin of both cations and anions in a routine manner. Although a minimum. Report sheets with questions and spaces for anthis manuel was prepared primarily to accompany the authors' swers are inoluded. There is no systematic qualitative analysis 'First Year College Chemistry' text, it should prove satisfactory except for anions, the tests for cations being parts of experiments for use with other texts. The sequence in whiehthe ex~eriments on the individual metals. Only four organic experiments are are performed could be changed to conform with the &aterial in included. another text." (Quoted from authors' preface.) In general the experiments are of conventional types. Several 0 LABORATORY EXPWMENTS IN. GENERAL CHEMare quantitative. "The sc.h,hemeof qualitative analy8is is a more ISTRY AND QUALITATIVE ANALYSIS or less conventional hydrogen sulfide system. One variation is the use of sodium sulfide rather than the polysulfide in the separa- George W. Watt, Professor of Chemistry, University of Texas. tion of the copper and arsenic groups," following oxid&m of Second edition. McGraw-Hill Book Co., Ine., New York, 1951. 230 UP. stannous to stannie. (Quotation from preface.) Parallel ma- x .. 47 figs. 24 X 28 cm. Surinq . .hindinq. $2.75. cedures, semimicro andmacro, are given for the analyses, inciudTHEk s t part of this book consists of 49 general and inorganic ing speoific, step-by-step instructions. The approach followed can ~ e r h a p best s he oharacterized by quoting from the preliminary experiments. Directions are complete, questions are thoughtinstructions on page 134: "For each group a schematic method of provoking, but only a minimum of introductory discussion is separation and identification is given. . . . Study the analytioal given. Many experiments were adapted from directions given and references are included. To in papers published in THISJOURNAL scheme csrefully, and transpose it to the flow-sheet form. expedite your work, this flow chart should be learned in its en- A very large proportion of the experiments are quantitative in Obtain s. sample. .which contains all thecations of the approach. A desirable feature is the insistence on safety pretirety.. group to he analyzed. Follow the schematic method of analysis, cautions, including approval of apparatus. The latter portion of the book is devoted to a standard system." checking at each point with the flow chart. The manual provides blank spaces in which answers are to be atic scheme of oualitative malvsis. usine H A Directions are written. The pages are perforated and punched, so that they can he torn out as used, and kept in a three-ring binder, or t,he Pages are perforated for reports to he handed in and are paper-covered manual can he kept intact. The drawings and directions. are clear, and the general makeup of the book is punched to fit a standard note hook. Lists of apparatus and of reagents needed for experiments are in the appendix. attractive.

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EXPERIMENTAL STUDIES IN BASIC COLLEGE CHEMISTRY Everette L. Henderson, Professor of Chemistry, University of 246 pp. Detroit. Thomas Y. Crawell Co., New York, 1951. x 48 figs. 3 graphs. 20 X 27 cm. $2.50.

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ESSENTIALS OF EXPERIMENTAL CHEMISTRY

Alfred Benjamin Garrett, Joseph Frederic Haskins, Harry Hall Sisler, and Margaret H.Kurbatov, all of the Ohio State 328 pp. 102 Univer6ty. Ginn and Co., Boston, 1951. x figs. 19.5 X 26.5 cm. $2.80.

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This is a laboratory manual containing 73 experiments designed for use either as student experiments, as lecture demonstrations, or as a combination of both. Sufficient ohoice and variety is included to allow for selection or alternation of experiments. Nine experiments require no laboratory work. Only a few emeriments involve quantitative technique. Emeriments are grauped in eight units-of related interests. No qualitative analysis is included. This manual is written for terminal students of average ability with no previous experience in chemistry, Explanstions and directions are detailed with many questions regarding all phases of the work. The emphasis on descriptive material make8 this book more suitable for students with nonmathematical interests such as agriculture and home economics. Pages are perforated to hand in and are punched to fit a standard note hook. Also included in the appendix are lists of apparatus needed and quantities of reagents for ten students.

THEREare 48 experiments of approximately equal length in this manual. Directions are complete and easily understood, preceded by disoussion of principles involved and followed by review questions and problems. Spaces are included for results and answers to quentions. The arrangement of the book is such that pages must be left attached and the whole book handed in for correction. No quslitative analysis and only three organic experiments are included. 0

CHEMICAL SYMBOLISM AND CALCULATIONS

Stanley W. Morse, Professor of Physical Science, San Francisco State College. The National Press, Millbrae. Calif., 1950. viii 144 pp. 4 tahles. 22 X 27.5 cm. Spiral binding $2.

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THIS workhook is intended for use as a supplement to any regular textbook in general chemistry. I t supplies more detailed direotions about use of symbols, formulas, equations, and the solving of problems of all kinds than most textbooks do. In each section of the hook there is a review of the principles involved, examples of each kind are solved with accompanying explanation, sets of practice problems are given with answers, and