Lockheed Dialog - Analytical Chemistry - ACS Publications - American

May 25, 2012 - Lockheed Dialog. Anal. Chem. , 1980, 52 (13), pp 1447A–1447A. DOI: 10.1021/ac50063a783. Publication Date: November 1980. ACS Legacy ...
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New Products Hybrid Scanning System for Transmission Electron Microscopes The hybrid scanning system is designed to be used with any Philips EM 400 transmission electron microscope having a scanning capacity. Rocking beam or subspecimen scanning allows a diffraction pattern to be displayed using a scanning monitor and provides for possible on-line diffraction analysis. Full use can be made of all STEM capabilities. A feature of the system is conical scan with an adjustable angle of tilt and a manually or automatically controlled beam rotation. N.V. Philips' Gloeilampenfabrieken 417 UV/vis Spectrophotometric A b s o r b a n c e Standards The set includes nine filters permitting a check up to 3 A. The effect of reflections is compensated for by providing a clear glass filter in the set for zeroing. To prevent distortions and inaccuracy, the filters are mounted in a frame that puts no physical stress on them. Sargent-Welch Scientific Co. 420

Chemicals A m y l a s e Reagent Enzymatic amylase reagent, DeltaTest Amylase (UV) is a lyophilized, singlecomponent reagent that produces glucose when it acts on a modified carboxymethylated starch substrate in the presence of glucoamylase. The glucose produced is measured kinetically at 340 nm using hexokinase and G-6-PD. The reagent is available in 10 X 6.5 mL and 10 X 16 mL put-ups. After reconstitution, the reagent is stable 8 h at room temperature, up to 3 h at 37 °C, and 3 d when refrigerated or frozen. Upper limit for the reagent's dynamic range is 2000 U/L. The normal range at 37 °C is 74-258 U/L. Adaptable to automated instrumentation, it can be used at 25, 30, or 37 °C. Princeton Biomedix 428 L a c t a t e Ester S o l v e n t s The solvents are sugar-derived vs. petroleum-based. Three forms are available: ethyl-, isopropyl-, and butyl-lactate. Each is a clear, colorless, nontoxic liquid of low volatility, manufactured from L (+) lactic acid. The esters are miscible in the following organic solvents: aliphatic and cycloaliphatic hydrocarbons, aromatics, chlorinated hydrocarbons, alcohols, esters, ketones, DMF, DMSO, and water. Limited miscibilities are observed for ethyl lactate with the higher alkanes (e.g., octane) and for butyl lactate with DMSO and water. Ethyl lactate has a high tolerance for water. High dilution ratios are observed. Pettibone-Chicago, Inc. 429 Ferruginous Bauxite R e f e r e n c e Material

Headspace Analyzer HS 250, an accessory to a GC, avoids permanently restricting one GC to headspace analysis. Designed to fit all Carlo Erbe Strumentazione 2000 and 4000 Series GCs, the HS 250 can be used with packed columns, WCOT or SCOT capillary columns and used during multidetector operations when flame ionization, sulphur selective, nitrogen or phosphorous, or wire detectors are in use. Specifications are: temperature range 30-120 °C; sample size up to 2.5 mL vapor; solid sample size 1-2 g; liquid sample size 0.5-5 mL liquid. Analysis may be programmed up to 99 min. Carlo Erba Strumentazione 402

The material was prepared and analyzed by more than 12 international laboratories. The following are the provisional values for the major compounds: A l 2 0 3 % = 37.38 ± 0.40; Fe 2 0 3 % = 35.83 ± 0.61; S i 0 2 % = 1.21 ± 0.08; and T i 0 2 % - 3.15 ± 0.10. To obtain a 50 g (