Magnetic Resonance of Carbonaceous Solids ... - ACS Publications

Downloaded by 117.253.96.79 on February 27, 2016 | http://pubs.acs.org Publication Date: December 9, 1992 | doi: 10.1021/ba-1993-0229.fw001

Magnetic Resonance of Carbonaceous Solids

In Magnetic Resonance of Carbonaceous Solids; Botto, Robert E., et al.; Advances in Chemistry; American Chemical Society: Washington, DC, 1992.



ADVANCES

IN C H E M I S T R Y S E R I E S

Magnetic Resonance of Carbonaceous Solids Robert E. Botto, EDITOR


Argonne National Laboratory

Yuzo Sanada, EDITOR Hokkaido University

Developedfroma symposium sponsored by the International Chemical Congress of the Pacific Basin Societies

American Chemical Society, Washington, DC 1993


229

Library of Congress Cataloging-in-Publication Data Magnetic resonance of carbonaceous solids: developed by a symposium sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989 / Robert E. Botto, editor, Y ū z ōSanada, editor. p. cm. — (Advances in chemistry series, ISSN 0065-2393 ; 229) Includes bibliograhical references and index. ISBN 0-8412-1866-8


1. Coal—Analysis—Congresses. 2. Carbon—Analysis—Congresses. 3. Nuclear magnetic resonance spectroscopy—Congresses. I. Botto, Robert E., 1946. II. Sanada, Yūzō, 1932III. International Chemical Congress of Pacific Basin Societies (1989: Honolulu, Hawaii) IV. Series. QD1.A355 no. 229 [TP325] 540 s—dc20 [662.6'22]

92-36495 CIP

The paper used in this publication meets the minimum requirements of American National Standard for Information Sciences—Permanence of Paper for Printed Library Materials, ANSI Z39.48-1984. Copyright © 1993 American Chemical Society All Rights Reserved. The appearance of the code at the bottom of the first page of each chapter in this volume indicates the copyright owner's consent that reprographic copies of the chapter may be made for personal or internal use or for the personal or internal use of specific clients. This consent is given on the condition, however, that the copier pay the stated per-copy fee through the Copyright Clearance Center, Inc., 27 Congress Street, Salem, M A 01970, for copying beyond that permitted by Sections 107 or 108 of the U.S. Copyright Law. This consent does not extend to copying or transmission by any means—graphic or electronic—for any other purpose, such as for general distribution, for advertising or promotional purposes, for creating a new collective work, for resale, or for information storage and retrieval systems. The copying fee for each chapter is indicated in the code at the bottom of thefirstpage of the chapter. The citation of trade names and/or names of manufacturers in this publication is not to be construed as an endorsement or as approval by ACS of the commercial products or services referenced herein; nor should the mere reference herein to any drawing, specification, chemical process, or other data be regarded as a license or as a conveyance of anyrightor permission to the holder, reader, or any other person or corporation, to manufacture, reproduce, use, or sell any patented invention or copyrighted work that may in any way be related thereto. Registered names, trademarks, etc., used in this publication, even without specific indication thereof, are not to be considered unprotected by law. PRINTED IN THE UNITED STATES OF AMERICA


1993 Advisory Board Advances in Chemistry Series M. Joan Comstock, Series Editor V. Dean Adams

Bonnie Lawlor

Tennessee Technological University

Institute for Scientific Information

Douglas R. Lloyd Robert J. Alaimo

The University of Texas at Austin

Procter & Gamble Pharmaceuticals, Inc.

Robert McGorrin


Kraft General Foods

Mark Arnold University of Iowa

Julius J. Menn

David Baker

Plant Sciences Institute, U.S. Department of Agriculture

University of Tennessee

Vincent Pecoraro Arindam Bose

University of Michigan

Pfizer Central Research

Marshall Phillips Robert F. Brady, Jr.

Delmont Laboratories

Naval Research Laboratory

George W. Roberts Margaret A. Cavanaugh

North Carolina State University

National Science Foundation

A. Truman Schwartz Dennis W. Hess

Macalaster College

Lehigh University

John R. Shapley Hiroshi Ito IBM Almaden Research Center

University of Illinois at Urbana-Champaign

Madeleine M. Joullie

Peter Willett

University of Pennsylvania

University of Sheffield (England)

Gretchen S. Kohl Dow-Corning Corporation


FOREWORD


The A D V A N C E S IN C H E M I S T R Y SERIES was founded in 1949

by

the American Chemical Society as an outlet for symposia and collections of data in special areas of topical interest that could not be accommodated in the Society's journals. It provides a medium for symposia that would otherwise be fragmented because their papers would be distributed among several journals or not published at all. Papers are reviewed critically according to ACS editorial standards and receive the careful attention and processing characteristic of ACS publications. Volumes in the A D V A N C E S IN CHEMISTRY SERIES maintain the integrity of the symposia on which they are based; however, verbatim reproductions of previously published papers are not accepted. Papers may include reports of research as well as reviews, because symposia my embrace both types of presentation.


ABOUT THE EDITORS


R O B E R T E . B O T T O is a research chemist

in the Chemistry Division at Argonne National Laboratory in Argonne, Illinois. His research involves the characterization of fossil fuels, polymers, and heterogeneous catalysts by solid-state N M R spectroscopy and imaging. He currently holds the position of Director of the Chemistry Division N M R Laboratory. In addition to authoring more than 50 scientific publications, he has presented as many papers at national and international meetings and has organized numerous national and international symposia. He is a member of the Sigma X i Honorary Research Society and the American Chemical Society, where he served as Secretary of the Fuel Chemistry Division from 1987 to 1989 and Newsletter Editor in 1990. He received his A B . degree in chemistry in 1968 from Rutgers College in New Brunswick, New Jersey. He received his M.S. degree in chemistry from Michigan State University in East Lansing, Michigan, in 1970. Following two years of service in the U.S. Army Science and Engineering Corps, he returned to Michigan State University where he received his PhD. degree in 1975.



Y u z o S A N A D A is a professor with the Faculty of Engineering of the Metals Research Institute at Hokkaido University. After receiving his B.Eng. degree from Toyama University and his Ph.D. from Tohoku University, he performed his postdoctoral work with the Research Council of Alberta in Edmonton. Before joining the faculty at Hokkaido University, he performed research for the Resources Research Institute (1954-1965) and was a senior researcher at the National Research Institute for Pollution and Resources (1965- 1975). His research expertise is in coal chemistry, heavy hydrocarbons, and carbon material science, and he specializes in the constitution and structural analysis of coal and related carbonaceous materials, the chemistry of coal liquefaction, and the pyrolysis and carbonization of coal and pitch. He received the Japan Petroleum Institute Medal in 1975 and 1990 and the Fuel Society of Japan Medal in 1976. He has written several books on coal and carbonization engineering. He has also authored more than 200 papers. In addition, he is a member of the Editorial Advisory Board of Energy and Fuels and a board member of both the Fuel Society of Japan and the Carbon Society of Japan.


Magnetic Resonance of Carbonaceous Solids ... - ACS Publications

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