MAXIMIZE YOUR

Box 371856 • Cincinnati, OH 45222-1856. (800)543-4461 Sales ... John M. Charles worth, DSTO, Materials Research Laboratory,. P.O. Box 50, Ascot Vale...
0 downloads 0 Views 1MB Size
MAXIMIZE YOUR SENSITIVITY... for Volatile Organic Compounds by Dynamic Headspace Concentration

BRIEFS Multivariate Analysis of Carbon-13 Nuclear Magnetic Resonance Spectra. Identification and Quantification of Average Structures in Petroleum Distillates 49 Two series of distillate fractions from North Sea petroleum samples are investigated using D E P T 13C NMR and multivariate analysis. The content of saturated isoprenoid structures is quantitated and is used to discriminate between the two oils in all fractions. Trond Brekke*, Tanja Barth, Olav M. Kvalheim, and Einar Sletten, Department of Chemistry, University of Bergen, Bergen N-5007, Norway Simultaneous Monitoring for Parent Ions of Targeted Daughter Ions: A Method for Rapid Screening Using Mass Spectrometry/ Mass Spectrometry 56 A screening method used with MS/MS instruments that employ a quadrupole mass filter as the first analyzer is described. Scott A. McLuckey*, Gary L. Glish, and Barry C. Grant, Analytical Chemistry Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831-6365 Laser Desorption/Fourier Transform Ion Cyclotron Resonance Mass Spectrometry of Polymer Additives 61 The formation of both N a + and K + adducts of the additives allows for the recognition of the quasimolecular ions in a mixture spectrum. In one polyethylene extract, the molecular weights of seven compounds are determined, and two of the compounds are identified. Bruce Asamoto*, Judy R. Young, and Robert J. Citerin, BP Research, Warrensville Research Center, 4440 Warrensville Center Road, Cleveland, OH 44128-2837 Precise Relative Ion Abundances from Fourier Transform Ion Cyclotron Resonance Magnitude-Mode Mass Spectra 70

5 ml Coffee on Tekmar's LSC 2000 and Capillary Interface

Flavor/Fragrance Competitive Analysis Off Flavor/Odor Analysis Packaging Materials Pharmaceuticals/Residual Solvents Building Products/Outgassing Studies Polymers Residual Monomers/Solvents

The best FT/ICR measure of relative ion abundance is based on least-squares fit to an (unphased) magnitude-mode spectrum. Zhenmin Liang and Alan G. Marshall*, Department of Chemistry, The Ohio State University, 120 West 18th Avenue, Columbus, OH 43210

Ask for our FREE bibliography of reprints on a wide range of applications

IIJJlMIJ^lJJliyMl>'WlNt/.'.tJ>'IMlfWM:W.',l

Tekmar® P.O. Box 371856 · Cincinnati, OH 45222-1856 (800) 543-4461 Sales · (800) 874-2004 Service CIRCLE 130 ON READER SERVICE CARD 8 A · ANALYTICAL CHEMISTRY, VOL. 62, NO. 1, JANUARY 1, 1990

Determination of Organic Acids in Dilute Hydrocarbon Solution Using Poly(ethylenimine)-Coated Piezoelectric Crystals 76 Piezoelectric crystals coated with a water-soluble basic polymer are used as sensing devices for organic acids dissolved in neutral hydrocarbons. Their application as selective LC detectors is demonstrated. John M. Charlesworlh, DSTO, Materials Research Laboratory, P.O. Box 50, Ascot Vale, Victoria, Australia 3032