2784
NOTES
Vol. 56 TABLE I THEPREPARATION OF HIGHER BROMIDES
The writer gratefully acknowledges the advice and assistance of the late Dr. W. J. Keith, who suggested this research. S c a o o ~OF CHEMISTRY AND PHYSICS PENNSYLVANIA STATECOLLEGE RECEIVED OCTOBER 9, 1934 STATECOLLEGE, PENNA.
The Preparation of Higher Aliphatic Bromides BY JOHN R. RUHOFF,~ ROBERT E. BURNETT AND E. EMMET REID
Reaction temp.,
Conco. MeOH for washing,
Alcohol
OC.
%
Cyclohexyl n-Heptyl Dodecyl Tetradecyl Octadecyl
80-100 80-100 100-120 100-120 100-120
65 50 50 50 90
Sols.. of bromide in wash MeOH, g. per 100 cc.
