ON ANALYTICAL CHEMISTRY AND APPLIED SPECTROSCOPY

PITTSBURGH CONFERENCE ON ANALYTICAL CHEMISTRY AND APPLIED SPECTROSCOPY

AND

Conference on Analytical Chemistry Applied Spectroscopy and Exposition of Modern Laboratory Equipment will be held March 1 to 6, 1970, at the Cleveland Convention Center, Cleveland, Ohio. This annual meeting is jointly sponsored by the Spectroscopy Society of Pittsburgh (Pittsburgh Section, Society for Applied Spectroscopy) and the Society for Analytical Chemists of Pittsburgh (Analytical Group, American Chemical Society). Registration is open to all interested persons. The fee is $6.00 for regular registration; student registration is $1.00; wives of conferees are registered free, at the Activities Desk. A pocket tab will be provided free to those who wish to visit the Exposition only. Housing accommodations should be made through the Convention Housing Committee before February 12. Forms and information on housing arc available from T. J. Garland, c/o Pittsburgh Conference Housing Committee, Cleveland Convention and Visitors Bureau, Inc,, 511 Terminal Tower, Cleveland, Ohio 44113. This year’s technical program, the largest ever, will consist of 45 sessions and the presentation of over 310 scientific papers covering a broad range of analytical topics. The Exposition will have exhibits from over 240 companies with emphasis on new instrumentation and laboratory equipment. 21st Pittsburgh rpHs and

The program includes papers from 37 of the 50 states and foreign countries: England, Germany, Canada, Japan, France, Australia, The Netherlands, Spain, Switzerland, Hungary, and Scotland. Symposia of special interest include one on "Analytical Chemistry—A Fading Discipline?" presided over by Foil A. Miller of the University of Pittsburgh. Positive and negative answers to the question will be given by M. Kent Wilson of the National Science Foundation and W. Wayne Meinke of the National Bureau of Standards, re11

EXPOSITION OF MODERN LABORATORY

CONVENTION

CENTER CLEVELAND, OHIO MARCH 1 to 6

EQUIPMENT

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Robert Mainier

William G. Fateley

Edward L. Obermiller

Joseph A. Feldman

ANALYTICAL CHEMISTRY, VOL. 42, NO. 2, FEBRUARY 1970

Harry Fracek

spectively. Other facets of the discipline itself will be discussed by university and industrial chemists. A symposium on analytical techniques in space will be held Tuesday afternoon. Results from some of the analyses of lunar samples from the Apollo 11 mission will be given. The Spectroscopy Society of Pittsburgh 1970 Award will be presented to Ellis R. Lippincott of the University of Maryland at a special Award Symposium scheduled for Wednesday afternoon. Professor Lippincott’s Award Address is entitled “Polywater and Related Materials.” At the Coblentz Society Symposium on Raman Spectroscopy, Thursday afternoon, the 1970 Coblentz Award will be presented to James R. Durig of the University of South Carolina by Charles Angell, President of the Society. Professor Durig will present a paper on “Anharmonic Vibrations in Far Infrared Spectroscopy.” Technical tours planned for interested conference participants include visits to SCM Corp.; Dwight T. Scott Research Center, Standard Oil Co. of Ohio; Research Laboratory of Union Carbide Corp.; Parma Technical Center; NASA-Lewis Research Center; General Electric Co. Lighting Institute; Chase Brass & Copper; Tubing Mill, Jones & Laughlin Steel Corp.; BOF and Strip Mill; and General Motors Corp., Fisher Body Div. In addition to the technical sessions, tours, and Exposition, there is a full social program. A social hour will be held at the beginning of the conference, Sunday evening, for all conferees. Light refreshments will be served. Tuesday evening all registrants are invited as guests of the sponsoring societies to a Conference Mixer. Monday evening, for $10 per person, a Turn of the Century Saloon Dinner (Gay Nineties Party) will be given at Pickle Bill’s Saloon on the Cuyahoga

River. A special dinner and ice follies party may be attended by participants on Wednesday evening, if desired, and Thursday evening there will be a wine-tasting party at the Sheraton-Cleveland Hotel. Ladies are invited to all the above functions. Besides, a special ladies’ program has been arranged which includes a wig show and tea, lunch at Pier W, a tour of Hixson’s Flower Barn, a tour of Cleveland Health Museum, and a tour of the Cleveland Plain Dealer. An employment bureau will be maintained at the Convention Center. Advance registration is urged. Job candidate’s and employer’s forms may be obtained from Harold A. Sweeney, Koppers Co., Inc., 440 College Park Dr., Monroeville, Pa. 15146. Short courses being offered in conjunction with the conference include an infrared workshop, sponsored by the Coblentz Society, to be held Friday, March 6; a course on quantitative thin layer chromatography, sponsored by Nester/ Faust, for Wednesday afternoon; and an ACS-sponsored course on gel permeation chromatography which will be held February 28 through March 1. During the course of the week various committees and subcommittees of the American Society for Testing and Materials will be meeting including ASTM Committee E-2 on Emission Spectroscopy, Committee E-13 on Molecular Spectroscopy, and others. The Coblentz Society and the Society for Applied Spectroscopy will have meetings, and the Society for Industrial Analytical Chemists will have an organizational meeting. The conference officials, the condensed and detailed technical program, and a listing of the Exposition exhibitors and their products are included in the following pages of Analytical Chemistry.

CONFERENCE OFFICIALS

CONFERENCE COMMITTEES

1970 BOARD OF DIRECTORS

EDWARD L. Program Chairman: OBERMILLER, Consolidation Coal

President: ROBERT MAINIER, Koppers Co., Inc. Vice President: WILLIAM G. FATELEY, Carnegie-Mellon University Treasurer: HARRY FRACEK, Fisher Scientific Co. Immediate Past President: GERALD L. CARLSON, Carnegie-Mellon University Chairman (Society for Analytical Chemists of Pittsburgh): EDWARD OBERMILLER, Consolidation Coal

Co.

Program Chairman-Elect: JOHN JACKOVITZ, Westinghouse Research Labs

JOSEPH A. Exposition Chairman: FELDMAN, Duquesne University Exposition Chairman-Elect: CHARLES J. McCAFFERTY, Jr., PPG Industries, Inc.

SUBCOMMITTEES

Co.

Chairman-Elect (Society of Analytical Chemists of Pittsburgh): GEORGE VASSILAROS, Crucible Steel Corp. Chairman (Spectroscopy Society of Pittsburgh): FRANK E. DICKSON, Gulf Research & Development Co. Chairman-Elect (Spectroscopy Society of Pittsburgh): CHARLES J. McCAFFERTY, Jr., PPG Industries, Inc. Secretary: JANE HARTER, Westinghouse Electric Corp. Assistant Treasurer: ROBERT WITKOWSKI, Westinghouse Research Labs

Program Analytical

Chemistry:

FOIL

ment Co.

Molecular

R. A. Spectroscopy: FRIEDEL, U. S. Bureau of Mines New Techniques and Mass Spectrometry: WILLIAM M. HICKAM, Westinghouse Research Labs Polymer Characterization: ROBERT J. LIMPERT, Waters Associates, Inc. Space and Thermal Analysis: RICHARD E. HEIN, H. J. Heinz Co. Steel & Electrochemistry: WILLIAM A. STRAUB, United States Steel Corp. X-ray and Emission: GEORGE L. VASSILAROS, Crucible Steel Corp.

A.

MILLER, University of Pittsburgh Atomic Absorption and Flame Spectroscopy: JOHN FROHLIGER, Uni-

versity of Pittsburgh

opment Co., and JAMES PETROCELLI, Gulf Research & Develop-

Award Symposia: FRANK E. DICKSON, Gulf Research & Development Co., and WILLIAM G. FATELEY, Carnegie-Mellon University ROBERT W. Chromatography: FREEDMAN, U. S. Bureau of Mines LAUREN Computer Applications: COUSINS, Gulf Research & Devel-

Activities Chairman: MAX KATZ, United States Steel Corp. Chairman-Elect: HERBERT L. RETCOFSKY, U. S. Bureau of Mines Assistants: JAYNE S. CARSON, United States Steel Chemicals; R. W. BAUDOUX, United States Steel Corp.; ELEANOR M. CAMPBELL, Republic Steel Corp.; MARIANNE HARRISON, Ferro Corp.


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Ladies’ Program

STADLER, Carnegie-Mellon Univer-

Chairman: SARAH DEGENKOLB, United States Steel Corp. Chairman-Elect: NITA STONE, Consultant, Cleveland, Ohio

Arrangements

Housing

Assistants: JOHN GRAHAM, Koppers Co., Inc.; DANIEL MANKA, Jones & Laughlin Steel Corp.; JACK PETTY, Calgon Corp.

Chairman: THOMAS J. GARLAND, Gulf Research & Development Co. Chairman-Elect: C. ELLEN GONTER, Cyrus Wm. Rice Co.

Chairman-Elect: JOSEPH R. RYAN, Harbison Walker Refractories Co.

sity

Special Projects

Chairman: HECTOR SILVA, Westinghouse Research Labs Chairman-Elect: S. DAVID ClFRULAK, United States Steel Chemicals

Printing

Pittsburgh-Cleveland Liaison

Chairman: EDWIN S. HODGE, Carnegie-Mellon University

Meetings

Chairman:

Chairman (Analytical Group Cleveland GERRIT DRAGT, General ACS): Electric Corp. Chairman (Cleveland Section ACS): HARRY R. GARNER, Harshaw Chemical Co.

Publicity Chairman: FLORENCE MELNICK, Jones & Laughlin Steel Corp. Chairman-Elect: ROBERT K. SCOTT, Harbison Walker Refractories Co.

OSWALD E. WILKINSON, Alcoa Research Laboratories Chairman-Elect: CLINTON WOLFE, Westinghouse Research Labora-

tories

Chairman:

Chairman: HAROLD A. SWEENEY, Koppers Co., Inc. Chairman-Elect: DAVID F. PENSEN-

President 1967: FRANK E. DICKSON, Gulf Research & Development Co.

Registration Employment

Advisory

ALEXANDER J. KAVOULAKIS, Shenango, Inc. ROBERT N. PINChairman-Elect: CHOK, United States Steel Chemicals

President 1969: GERALD L. CARLSON, Carnegie-Mellon University

Administrative Assistant EDWIN S. HODGE, Carnegie-Mellon

University

CONDENSED PROGRAM

All Sessions Are in the Convention Center P.M.

A.M. MONDAY MARCH 2

TUESDAY MARCH 3

WEDNESDAY MARCH 4

X-ray and Optical Emission Spectroscopy Spectroscopy—Varied Techniques Atomic Absorption—Instruments and Equipment Polymer Characterization X-ray and Optical Emission Spectroscopy Infrared Spectrophotometers and Fourier Transform Spectrometers Flame Emission Spectroscopy Chromatography—Gas and Liquid Symposium on Analytical Techniques on the Horizon

Ultraviolet—Visible Spectroscopy Symposium—Molecular Spectroscopy of Minerals and Related Inorganics Analysis of Water and Air Pollutants A FadSymposium—Analytical Chemistry ing Discipline? Chromatography—Gas and Liquid Infrared Spectroscopy—Instrumentation and ...

THURSDAY MARCH 5

FRIDAY MARCH 6

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Techniques Ion-Selective Electrodes and Related Electrochemical Sensors Computer Systems for Analytical Chemistry Mass Spectrometry Symposium on High Speed Chromatographic Analysis Infrared and Laser Raman Spectroscopy New Directions in Titrimetry

Interfacing Computers and Gas Chromatographs Gas Chromatography—Determinations


X-Ray and Optical Emission Spectroscopy

Ultraviolet—Visible Spectrophotometers Atomic Absorption—General Symposium on Polymer Characterization Symposium on X-ray & Optical Emission Spectroscopy Symposium—Molecular Spectroscopy of Minerals and Related Inorganics Atomic Absorption and Flame Spectroscopy— Applications

Chromatography—Liquid Symposium on Analytical Techniques in Space Visible Spectrophotometric Analyses and Microbalance Steel Analysis SSP Award Symposium Thermal Methods—Polymers and General Application Gas Chromatography—Apparatus and Accessories

Electrochemistry Symposium on Computers in Analytical Chem-

istry Coblentz Society Symposium Symposium on High Speed Chromatographic Analysis and Gas Chromatography—Techniques Molecular Spectroscopy and Spectral Methods in Pollution Research Nuclear Magnetic Resonance Spectroscopy and Computers in Spectroscopy On-Line Computer Applications in Analytical Chemistry Chromatography—General

PITTSBURGH

CONFERENCE ON ANALYTICAL APPLIED

MARCH

1

CHEMISTRY

AND

SPECTROSCOPY

CONVENTION CLEVELAND, OHIO

to 6

CENTER

PROGRAM ATOMIC ABSORPTION—INSTRUMENTS AND EQUIPMENT

MONDAY, MARCH 2

Monday Morning

X-RAY AND OPTICAL EMISSION SPECTROSCOPY Monday Morning

J. T. Rozsa, Presiding

Improved Excitation Electrode for Laser Microprobe. A. W. Fagan, Poco Graphite, Inc., P. O. Box 2121, Decatur, Tex. 76234; R. A. Manning, C. F. Lentz, Texas Instruments, Inc., Dallas, Tex. 75222 9:20 Application of Neutron Activation Analysis of Halogens as Assay Method in Pharmaceutical Control. Michael Margosis, J. T. Tanner, and Jos. P. F. Lambert, Bureau of Science, Food and Drug Administration, USDHEW, Washington, D. C. 9:40 New Photoelectron Spectrometer. G. A. Errock, B. N. Green, and J. M. Watson, A.E.I. Scientific Apparatus, Ltd., Barton Dock Road, Manchester, England 10:00 On-Stream Analysis of Hafnium and Zirconium in Solutions. A. H. Smallbone, Applied Research Laboratories, P. O. Box 129, Sunland, Calif. 91040 10:40 Chemical Instrumental Determination of Gold Using Highly Selective Chelating Resin-Loaded Paper. S. L. Law, T. E. Green, and W. J. Campbell, U. S. Department of Interior, Bureau of Mines, College Park Metallurgy Research Center, College Park, Md. 20740 11:00 Laser-Induced High Sensitivity Fluorimetry with Cary 14. R. Bender, R. Jankow, and W. Renken, Cary Instruments, Monrovia, Calif. 91016. 11:20 Aluminum Alloy Sorting and Analysis Using Portable X-Ray Analyzer. N. Christ, Reynolds Metals Co., Fourth and Canal Sts., Richmond, Va. 23219 9:00

R.

Panning, Presiding

9:00 Microwave-Excited Electrodeless Discharge Lamps as Sources for Atomic Absorption Spectroscopy. G. C. Hayward and A. A. Fisher, Beckman R.I.I.C. Ltd., Worsley Bridge Road, London S.E. 26, England 9:20 Atomic Absorption Analysis by Flameless Atomization in Controlled Atmosphere. H. M. Donega and T. E. Burgess, Research and Development Laboratory, Sprague Electric Co., North Adams, Mass. 9:40 Analysis of Lubricating Oils with Model 303B Atomic Absorption Spectrophotometer. G. E. Peterson and H. L. Kahn, The Perkin-Elmer Corp., Norwalk, Conn. 06852 10:00 High-Solid Samples in Atomic-Absorption Flame Photometry. August Hell and Juan Ramirez-Munoz, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 10:40 Atomic Absorption System for Automatic Background Correction. Theodore J. Poulos, Jarrell-Ash Division, Fisher Scientific Co., 590 Lincoln Street, Waltham, Mass. 11:00 Automated Atomic Spectroscopy. Stanley B. Smith, Jr., Thomas S. Bissett, and Fredric J. Feldman, Instrumentation Laboratory, Inc., 113 Hartwell Ave., Lexington, Mass. 02173 11:20 New Dimension in Optical Spectrum Analysis. William G. Elliott, Spectrametrics, Inc., Northwest Park, Burlington, Mass. 01803 11:40 Evaluation of Atomic Fluorescence Excitation Sources. A. Hell and S. Ricchio, Beckman Instruments, Inc., 2500 Harbor Blvd. Fullerton, Calif. 92634

SPECTROSCOPY—VARIED TECHNIQUES

POLYMER CHARACTERIZATION

Monday Morning

9:00 New System for Rapid Microbiology Utilizing Firefly Luciferin-Luciferase Enzyme System. Paul F. Levy, Anthony J. D’Eustachio, George R. Long, and John D. McGhee, E. I. Du Pont de Nemours & Co., Instrument and Equipment Division, Wilmington, Del. 19898 9:20 Chemical Applications of E.S.C.A. (Photoelectron Spectroscopy). A. Melera and R. Moody, Hewlett-Packard Laboratories, Palo Alto, Calif. 9:40 Recording Circular Dichroism Spectropolarimeter. J. J. Duffield, A. Abu-Shumays, G. E. Hooper, and A. H. Hinds, Cary Instruments, 2724 South Peck Road, Monrovia, Calif. 91016 Measurement of Magnetic Circular Dichroism Using 10:00 A. Abu-Shumays, G. E. Alternating Magnetic Fields. Hooper, and J. J. Duffield, Cary Instruments, 2724 South Peck Road, Monrovia, Calif. 91016 10:40 Report on Performance of New Circular Dichroism Spectrophotometer. M. Velez and J. McCallum, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 11:00 Dynamic Reflectance Spectroscopy: Application to Thermochromic Compounds. W. W. Wendlandt and W. S. Bradley, University of Houston, Houston, Tex. 77004 11:20 New Engineering Look at a UV-VIS SpectrophotomIrvin C. eter with Linear Absorbance (TAC) Presentation. Rebeschini, John J. J. Staunton, and Henry A. Marquardt, Coleman Instruments Division of Perkin-Elmer Corp., Maywood, III. 60153 11:40 Research to Routine in Spectrophotometry. Melvin E. Ebeling and Frank J. Vetrovec, Coleman Instruments Division of the Perkin-Elmer Corp., Maywood, III. 60153

Monday Morning

Robert J. Limpert, Presiding

9:00 Applications of High Speed Liquid Chromatography to Analysis of Polymer Intermediates and Additives. Richard A. Henry, E. I. du Pont de Nemours & Co., Wilmington, Del. 19898 9:20 Exclusion Chromatography at Extreme Operating Conditions. Harold I. Suchan, E. I. du Pont de Nemours & Co., Wilmington, Del. 19898 9:40 Use of Control Charts in Monitoring Gel Permeation Chromatography Calibration Curves. H. Walser and D. Alliet, Xerox Corp., Webster, New York, N. Y. 14580 10:00 Ion Exchange Network Characterization. David H. Freeman, National Bureau of Standards, Washington, D. C. 20234 10:40 Direct Determination of Phenyl Content of Silicone Compounds by Infrared Spectrometry. Fred N. Larsen and Marsha A. Verbanic, The Bendix Corp., P. O. Box 1159, Kansas City, Mo. 64141 11:00 New Method for Determination of Molecular Weights of Compounds in Mixtures. D. G. Paul, Chemalytics, Inc., R. D. 1, Street Road, Kennett Square, Pa. 19348; Gerald R. Umbreit, R. E. Nygren, and A. J. Testa, Greenwood Laboratories, Inc., Chadds Ford, Pa. 19317 11:20 Design and Performance of Molecular Weight Analyzer. F. W. Karasek, University of Waterloo, Waterloo, Ont., Canada; R. S. Gohlke, Finnigan Instrument, 2631 Hanover St., Palo Alto, Calif. 94304 11:40 Performance and Some Novel Applications of Polymer Permeation Analyzer. R. A. Pasternak, G. L. Burns, Stanford Research Institute, Menlo Park, Calif. 94025; J. A. McNulty, Infotronic Corp., Mt. View, Calif. 94040


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Pittsburgh Conference X-RAY AND OPTICAL EMISSION SPECTROSCOPY Monday Afternoon

W. Ritchey,

Presiding

2:00 Use of Direct Reading Spectrometer with D.C. Arc Excitation and Total Sample Combination in Analysis of High Purity Materials. B. S. Cooper and D. J. Hobbs, Johnson Matthey Chemicals Ltd., Hertfordshire, England 2:20 Reduced-Regression Interelement Corrections in X-Ray Fluorescence Analysis. S. D. Rashberry and K. F. J. Heinrich, National Bureau of Standards, Washington, D. C. 20234 2:40 Buffers for X-Ray Fluorescence Spectroscopy. H. A. Johnson, Univac, Division of Sperry Rand, 2750 West 7th St., St. Paul, Minn. 55116 3:00 Advances in Sequential Surface Analysis of Metal Alloys by Ultrasonic Chemical Milling Measurement. C. J. Belle and J. D. Johnson, Westinghouse Electric Corp., P. O. Box 158, Madison, Pa. 15663 3:40 Universal Readout Console. R. M. Ajhar and W. E. Fowler, Applied Research Laboratories, P. O. Box 129, Sunland, Calif. 91040 4:00 Normal-Pulse Laser Sampling of Copper-Zinc Alloys. Jon M. Baldwin, Idaho Nuclear Corp., P. O. Box 1845, Idaho Falls, Idaho 83401 4:20 Sub-Microgram Encapsulation Chemistry. David H. Freeman, National Bureau of Standards, Washington, D. C. 20234 4:40 Computer Techniques for Emission Spectrometer Calibration. Herman G. Eldering, Baird Atomic, 125 Middlesex Turnpike, Bedford, Mass. 01730

Rains, T. A. Rush, and O. Menis, Analytical Chemistry Division, National Bureau of Standards, Washington, D. C.

20234 3:40 Interferences Among Refractory Elements in Nitrous Oxide-Acetylene Flame. G. G. Welcher and Jerry Y. Marks, Pratt and Whitney Aircraft, Advanced Materials Research and Development Laboratory, Middletown, Conn. 06457 4:00 Evaluation of Photomultiplier Tubes as Detectors in Atomic Spectroscopy. Thomas S. Bissett, Fredric J. Feldman, and Stanley B. Smith, Jr., Instrumentation Laboratory, Inc., 113 Hartwell Ave., Lexington, Mass. 02173 4:20 Computer Program for Atomic Absorption and Data Processing. Robert C. Gabler, Jr., Raymond E. Brown, and Jack G. Haymes, Department of the Interior, U. S. Bureau of Mines, College Park Metallurgy Research Center, College Park, Md. 20740

SYMPOSIUM ON POLYMER CHARACTERIZATION Monday Afternoon

Robert J.

Limpert, Presiding

2:00 Application of High Resolution NMR to Study of F. A. Bovey, Bell Telephone Laboratories, Polymers. Murray Hill, N. J. 07974 2:30 Infrared Characterization of Polymers. J. J. Shipman, B. F. Goodrich Research Center, Brecksville, Ohio 44141 3:00 Pyrolysis Gas Chromatography of Polymers: Stateof-the-Art. Clarence J. Wolf, McDonnell Douglas Corp., St.

Louis, Mo. Practice of Gel Permeation Chromatography in Polymer Research and Development. Dale J. Harmon, B. F. Goodrich Research Center, Brecksville, Ohio 44141 of 4:20 Characterization Polymers by Differential Thermal Analysis. Bernard Wunderlich, Rensselaer Polytech InstiY. N. 12180 tute, Troy,

3:50

ULTRAVIOLET-VISIBLE SPECTROPHOTOMETERS Monday Afternoon

F. E.

Dickson, Presiding

Some Applications in Analytical Laboratory for New UV/Visible Spectrophotometer. Robert E. Anacreon, The Perkin-Elmer Corp., Norwalk, Conn. 06852; Francis E. Dunstan, Perkin-Elmer, Ltd., and T. P. Michaels, Merck, Sharp & Dohme, Inc., West Point, Pa. 19486 2:20 Spectrophotometer Designed for Digital Control and Data Collection. J. Holly, K. P. George, and R. Wolfe, Cary Instruments, 2724 South Peck Road, Monrovia, Calif. 91916 2:40 Digital Scan Control Accessory. Russell W. Wolfe and Joseph M. Marino, Cary Instruments, 2724 South Peck Road, Monrovia, Calif. 91016 3:00 New Series of UV-Visible Spectrophotometers. W. S. Gallaway, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 3:40 Performance of New Ultraviolet Spectrophotometer. Robert J. Manning, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 4:00 Versatile Automatic Spectrophotometer System, Based on New Ultraviolet and Visible Double Beam Grating Spectrophotometer. M. R. Sharpe, Pye Unicam Ltd., Research and Development Laboratories, Cambridge, England 4:20 Double Beam Grating Spectrophotometer Designed for Color Measurement and Formulation Control by Virtue of Computer Data Handling. F. T. Simon, Clemson University, Clemson, S. C.; R. E. Schatzmann and A. T. Mason, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 4:40 Double Wavelength Spectroscopy: Direct Recording of First Derivative Absorption Spectra at Ambient and Low Temperature. H. F. Smith, S. D. Kullbom, K. Yasuda, and T. Honkawa, Perkin-Elmer Corp., Norwalk, Conn. 06852

2:00

ATOMIC ABSORPTION—GENERAL Monday Afternoon

J. Frohliger,

Presiding

Graphite Tube Furnace in Atomic Absorption Spectroscopy. D. C. Manning and F. Fernandez, The PerkinElmer Corp., Norwalk, Conn. 06852 2:20 Non-Flame Sampling Technique for Atomic Absorption with Automatic Background Correction. Frederic J. Feldman, Instrumentation Laboratory, Inc., 113 Hartwell Ave., Lexington, Mass. 02173 2:40 Some Studies in Non-Flame Atomization for Atomic Absorption Spectroscopy. M. D. Amos, P. A. Bennett, P. W. Y. Lung, and G. P. Thomas, Varian Techtron Ry. Ltd., Melbourne, Australia and Walnut Creek, Calif. 3:00 Selection of Appropriate Absorbing and Non-Absorbing Line for Use in Atomic Absorption Spectrometry. T. C. 2:00

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ASTM COMMITTEE E-13 MOLECULAR SPECTROSCOPY Main Committee Meeting

Guests Welcome

Monday, March 2, 3:30 P.M.

TUESDAY, MARCH 3 X-RAY AND OPTICAL EMISSION SPECTROSCOPY Tuesday Morning

E. S.

Hodge, Presiding

9:00 Instrument Parameters or X-Ray Analysis of Platinum and Rhodium. F. D. Seidel and K. M. Davis, Mattey Bishop, Inc., Malvern, Pa. 19355 9:20 Bonding and Chemical Combination Studies Using Electron Microbeam Probe. W. L. Baun, Air Force Materials Laboratory (MAYA), Wright-Patterson AFB, Ohio 45431; James S. Solomon, University of Dayton Research Institute, Dayton, Ohio 45409 9:40 Concentration-Spectrographic Determination of Parts per Billion of Some Impurities in Metallurgical Products. M. G. Atwell, M. Carlson, and G. S. Golden, United Aircraft Research Laboratories, East Hartford, Conn. 06108 10:00 Spectrographic Determination of Traces of Bismuth, Lead, and Tin in Nickel-Base Alloys by a Carrier Distillation Technique. M. G. Atwell and G. S. Golden, United Aircraft Research Laboratories, East Hartford, Conn. 06108 10:40 Closing Porosity of Spectroscopic Electrodes. A. W. Fagan and R. F. Wehrmann, Poco Graphite, Inc., P. O. Box 2121, Decatur, Tex. 76234 11:00 Spectrochemical Method for Analysis of Polyvinyl Chloride. R. H. Hall and R. J. Plenzler, Owens-Illinois, Inc., 1700 N. Westwood, Toledo, Ohio 43607 11:20 Trace and Ultra-Trace Analysis Using Working Curves Plotted to High Statistical Confidence. B. S. Cooper and D. J. Hobbs, Johnson Matthey Chemicals Ltd., England 11:40 Constant Energy Spectroscopic System. George Chaplenko and Donald O. Landon, Spex Industries, Inc., J. N. 08840 Metuchen,


Pittsburgh Conference INFRARED SPECTROPHOTOMETERS AND FOURIER TRANSFORM SPECTROMETERS Tuesday Morning

W. G. Fateley,

Presiding

New Low Cost Infrared Spectrophotometer. M. Pattison, Philips Electronic Instruments, Mount Vernon, N. Y.; J. R. Firth, and P. A. Cooke, Pye Unicam, Ltd., Research and Development Laboratories, York Street, Cambridge,

9:00

England 9:20 New High Performance Electric Null Double Beam Infrared Spectrophotometer. John M. Roche, Perkin-Elmer Corp., Norwalk, Conn. 06852 9:40 Developments in Design, Performance, and Applications of Medium-Sized Infrared Spectrophotometers. K. E. Stine and R. J. Manning, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 02634 10:00 New Low-Cost Infrared Spectrophotometer with Fast Recording Characteristics. Harry H. Hausdorff, Wilks Scientific Corp. (Hilger & Watts, Ltd.), South Norwalk, Conn. 06856 10:40 “Real-Time” Far-Infrared Fourier Spectrometer System. R. C. Milward, Societe Coderg, 92 Clichy, France 11:00 Recent Developments in Far Infrared Interferometry. L. W. Thorpe and G. C. Hayward, Beckman—R.I.I.C. Ltd., Worsley Bridge Road, London, S. E. 26, England 11:20 Design and Construction of Computer-Controlled Mid-Infrared Fourier Transform Spectrometer. T. Hirschfeld and P. R. Griffiths, Dunn Analytical Instruments, Silver Spring, Md. 20902 11:40 Solution of Difficult Problems in IR Spectroscopy by Use of FTS. Peter R. Griffiths, Block Engineering, Inc., 19 Blackstone St., Cambridge, Mass. 02139

FLAME EMISSION SPECTROSCOPY Tuesday Morning

Don Burfiend, Presiding

9:00 Investigations into Use of Shielded Flames in Spectroscopy. M. D. Amos, Varian Techtron Ry. Ltd., Melbourne, Australia 9:20 Characteristics of Organic Liquid Fuel Flames. B. W. Bailey and J. M. Rankin, N.Y.S. Health Department, Division of Laboratories and Research, New Scotland Ave., Albany, N. Y. 12201 9:40 Use of Volatile Inorganic Chelates in Flame Spectroscopy. B. W. Bailey and F. C. Lo, N.Y.S. Health Department, Division of Laboratories and Research, New Scotland Ave., Albany, N. Y. 12201 10:00 Flame Emission Spectroscopy with Nitrous OxideAcetylene Flame. Gary D. Christian, University of Kentucky, Lexington, Ky. 40506; Fredric J. Feldman, Instrumentation Laboratory, Inc., 113 Hartwell St., Lexington, Mass. 02173 10:40 Determination of Boron by Molecular Emission Spectroscopy in Flames. B. W. Bailey and F. C. Lo, N.Y.S. Health Department, Division of Laboratories and Research, New Scotland Ave., Albany, N. Y. 12201 11:00 Selected Comparisons between Atomic Absorption and Flame Emission, with Emphasis on Determination of Phosphorus. J. D. Kerber, W. B. Barnett, and H. L. Kahn, The Perkin-Elmer Corp., Norwalk, Conn. 06852 11:20 Sulfur and Phosphorus Band Emission from Sheathed Hydrogen Flames. Claude Veillon and John Y. Park, University of Houston, Department of Chemistry, Houston, Tex. 77004 11:40 New Technique for Measurement of Heats of Combustion Utilizing Flame Emission Spectrometry. M. L. Parsons, J. Kroeten, and H. Moody, Arizona State University, Tempe, Ariz. 85281

9:40 Design and Performance of Gravimetric Detector for Liquid Chromatography. James L. Radawski and Colin J. Williams, Cahn Division, Ventron Instruments Corp., 7500 Jefferson St., Paramount, Calif. 90723 10:00 New Spherical Ceramic Material for Solid Supports in Gas-Liquid Chromatography. Nicholas T. Castellucci, Pittsburgh Corning Corp., 800 Presque Isle Dr., Pittsburgh, Pa. 15239; Paul R. Eisaman and James J. Headings, Mellon Institute, Pittsburgh, Pa. 15213 10:40 Separation of Amines by Gas-Liquid Chromatography. Nicholas T. Castellucci, Pittsburgh Corning Corp., 800 Presque Isle Dr., Pittsburgh, Pa. 15239; Paul R. Eisaman and James J. Headings, Mellon Institute, Pittsburgh, Pa. 15213 11:00 Gas Chromatography Packings with Chemically Bonded Stationary Phases. James N. Little, William A. Dark, Philip W. Farlinger, and Karl J. Bombaugh, Waters Associates, Inc., 61 Fountain St., Framingham, Mass. 01701 11:20 Variable Selectivity Stationary Phases for Gas Chromatography. Raymond Annino and Peter F. McCrea, The Foxboro Co., Neponset Ave., Foxboro, Mass. 02035 11:40 Amine Separations by Gas Chromatography. H. G. Collier, Pennsalt Corp., Development Laboratory, 4655 Biddle Ave., Wyandotte, Mich. 48193 SYMPOSIUM ON ANALYTICAL TECHNIQUES ON THE HORIZON Tuesday Morning

Tuesday Morning

O. E.

Wilkinson, Presiding

9:00 Small Dead Volume Light Absorption, Refractive Index, and Heat of Adsorption Detectors for Liquid Chromatography. Miner Munk, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598 9:20 Temperature Effects on Liquid Chromatographic ColIts Use in Routine Analysis. T. E. Young, Pye umns. Unicam Ltd., Cambridge, England; F. Kabot, Philips Electronic Instruments, Inc., 750 South Fulton Ave., Mount Vernon, N. Y. 10551 54 A

•

Hickam, Presiding

Ion Emission Microanalysis. R. Castaing, Faculte des Sciences, d’Orsay, France 9:40 Chemiluminescence and Enzyme-Catalyzed Chemiluminescence. H. H. Seliger, The Johns Hopkins University, Baltimore, Md. 10:40 Application of Solid Electrolytes to Monitoring of Gases and Liquid Metals. R. Littlewood, The Steel Co. of Canada, Hamilton, Ont. 11:20 Thermomagnetic Analysis. R. G. Charles, Westinghouse Research Laboratories, Pittsburgh, Pa. SYMPOSIUM ON X-RAY AND OPTICAL EMISSION SPECTROSCOPY Tuesday Afternoon

G. L.

Vassilaros, Presiding

2:00 Progress of Automation in X-Ray Spectrochemical Analysis. Kurt Togel, Siemens-Ag, 75 Karlsruhe, Rheinbruckenstrasse, West Germany 2:40 X-Ray Excited Optical Fluorescence Spectroscopy. A. P. D’Silva, E. DeKalb, and V. A. Fassel, Institute for Atomic Research, Iowa State University, Ames, Iowa 50010 3:00 Capabilities and Limits for X-Ray Spectrographic Analysis in Specialty and Light-Metal Industries. B. Thiele, Siemens, 75 Karlsruhe, Rheinbruckenstrasse, West Germany 3:40 Two-Thousand (2000) Channel Emission Spectrometer. Marvin Margoshes, Dunn Analytical Instruments, Division of Block Engineering, Silver Spring, Md. 20907 4:20 Improving Detection Limits and Precision of Solution Analysis. John A. Norris and G. R. Zachau, Jarrell-Ash Division, Fisher Scientific Co., 590 Lincoln St., Waltham, Mass. 02154 4:40 Sequential Surface Analysis of Metal Alloys by Glow Discharge Emission Spectrography. J. D. Johnson and C. J. Belle, Westinghouse Electric Corp., Advanced Reactors Division, Madison, Pa. 15663 SYMPOSIUM: MOLECULAR SPECTROSCOPY OF MINERALS AND RELATED INORGANICS Tuesday Afternoon

CHROMATOGRAPHY—GAS AND LIQUID

W. M.

9:00

R. A.

Friedel, Presiding

2:00 Infrared Spectral Properties of Some Anhydrous Mineral Carbonates, Sulfates, Phosphates and Related Substances. Hans H. Adler, U. S. Atomic Energy Commission, Division of Raw Materials, Washington D. C. 20545 2:40 Characterization of Layer Silicates by Infrared Spectroscopy: Brittle Micas, Phengites, and Celadonites. V. C. Farmer, Department of Spectrochemistry, The Macaulay Institute for Soil Research, Craigiebuckler, Aberdeen, AB9 2QJ, Scotland 3:35 Infrared Spectra and Properties of Layer Silicates. Willem Vedder, General Electric Research & Development Center, P. O. Box 8, Schenectady, N. Y. 12301.


Pittsburgh Conference 4:05 Infrared Spectrophotometry, Geochemical Tool. J. D. Stephens and W. M. Tuddenham, Metal Mining Division, Research Department, Kennecott Copper Corp., P. O. Box 11299, Salt Lake City, Utah 84111 4:35 Investigation of Rare-Earth Crystalline Compounds Through Their Lattice Spectra. Neil T. McDevitt and Conrad M. Phillippi, Air Force Materials Laboratory (MAYA), Wright-Patterson Air Force Base, Ohio 45433 Symposium will be continued

on

Wednesday morning

ATOMIC ABSORPTION AND FLAME SPECTROSCOPY APPLICATIONS Tuesday Afternoon

M. Y. Flynn, Presiding

2:00 Application of Organic Liquid Fuels to Flame Spectroscopy. B. W. Bailey and J. M. Rankin, N.Y.S. Department of Health, Division of Laboratories and Research, New Scotland Ave., Albany, N. Y. 12201 2:20 Atomic Absorption Spectroscopy of Rhodium. P. Johns and W. J. Price, Pye Unicam Ltd., Cambridge, England 2:40 Determination of Trace Metallic Impurities in Brine by Atomic Absorption Spectroscopy. John L. Randall, James E. Noble, and R. Kenneth Lee, PPG Industries, Industrial Chemical Division, P. O. Box 1000, Lake Charles, La. 70601 3:00 Routine Analytical Determination of 24 Elements in Siliceous Materials by Atomic Absorption Spectroscopy. Richard B. Muter and Charles F. Cockrell, West Virginia University, Coal Research Bureau, 219 Mineral Industries Building, Morgantown, W. Va. 26506 3:40 Atomic Absorption Applications to Battery Research. W. A. Rowe, J. A. Wieczorek, and B. M. Olsen, Gould, Inc., Research Division, 2630 University Ave., S.E., Minneapolis, Minn. 55414 4:00 Determination of Major Alloying Elements in HighTemperature Cobalt-Base Alloys by Atomic Absorption Spectrophotometry. G. G. Welcher and Owen H. Kriege, Pratt & Whitney Aircraft, Advanced Materials Research and Development Laboratory, Middletown, Conn. 06457 4:20 Comparison of Atomic Absorption and Automatic Colorimetry for Determination of Calcium in Biological Materials. A. P. Husbands, W. J. Price, and C. Mitchell, Pye Unicam, Ltd., Cambridge, England 4:40 Comparative Analysis of Potassium in Biologic Fluids by Atomic Absorption, Flame Photometry and Specific-Ion Electrodes. L. Kopita, E. Rosen, and H. Shwachman, The Children’s Hospital Medical Center and the Harvard Medical School, 300 Longwood Ave., Boston, Mass. 02115

CHROMATOGRAPHY—LIQUID Tuesday Afternoon

T. J. Garland, Presiding

2:00 Liquid Chromatographic Packings—Evaluations and Applications. James N. Little and Dennis F. Horgan, Waters Associates, 61 Fountain St., Framingham, Mass. 01701 2:20 Ion-Exchange Behavior of Bile Acid Species. Michael S. Weingarten, Michael T. Goldstein, and Gilbert E. Janauer, State University of New York at Binghamton, Department of Chemistry, Binghamton, N. Y. 13901 2:40 New Materials for Gel Permeation Chromatography. W. Heitz, K. Klatyk, F. Kraffczyk, K. Pfitzner, and D. Randau, E. Merck A.G., Darmstadt, Germany. Paper will be presented by G. Scheuerbrandt, 7 Woodlot Lane, Huntington, N.Y. 11743 3:00 Improved Molecular Sieving Procedure for Determination of Total Paraffins in Paraffin and Microcrystalline Waxes. T. A. Washall, S. Blittman, and R. S. Mascieri, ARCO Chemical Company, Research Division, 2700 W. Passyunk Ave., Philadelphia, Pa. 19145 3:40 Modular Approach to High-Efficiency Liquid Chromatography. Fred R. MacDonald Research and Development, Varian Aerograph, 2700 Mitchell Drive, Walnut Creek, Calif. 94598 4:00 Eluent Programmer for Liquid Chromatography. David G. Bailey, Eastern Utilization Research and Development Division, Agricultural Research Service, U. S. Department of Agriculture, 600 East Mermaid Lane, Philadelphia, Pa. 19118 56 A

•

4:20 Chromatography of Steroids by Centrifugation through Microparticulate Gel. Edgar Ribi, Charles J. Filz, and Ken-ichi Yamamoto, NIH, NIAID, Rocky Mountain Laboratory, and Ivan Sorvall, Inc., Instrument Research Laboratory, Hamilton, Mont. 59840 4:40 Applications of High-Speed Liquid Chromatography to Drug Analysis. John A. Schmit and Richard A. Henry, E. I. du Pont de Nemours & Co., Instrument and Equipment Division, Wilmington, Del. 19898

SYMPOSIUM ON ANALYTICAL TECHNIQUES IN SPACE Tuesday Afternoon

R. E.

Hein, Presiding

2:00 Chemical Analysis of Lunar Sample. Frank Cuttitta, Harry J. Rose, Jr., and Charles S. Annell, U. S. Geological Survey, Washington, D. C. 20242 2:30 Instrumental Neutron Activation Techniques as Applied to Analysis of Meteorites and Lunar Materials. William D. Ehmann and John W. Morgan, University of Kentucky, Lexington, Ky. 40506 3:00 Mineralogy and Petrology of Apollo 11 Lunar Samples and Their Bearing on Origin of Lunar Maria. Robin Brett, NASA Manned Spacecraft Center, Houston, Tex. 77058 3:50 Mass Spectrometric Studies of Radiogenic Isotopes in Cosmic Matter. Truman P. Kohman, Carnegie-Mellon University, Pittsburgh, Pa. 15213 4:20 Approach of Analytical Scientist to Establishing Trace Element Composition of Recovered Extra Terrestrial Material. A. A. Smales, Analytical Sciences Division, AEC Establishment, Harmell, Berkshire, England

WEDNESDAY, MARCH 4 ULTRAVIOLET—VISIBLE SPECTROSCOPY Wednesday Morning

J. J. McGovern, Presiding

9:00 Application of Spectrophotometric Kinetic Measurements for Chemical Analysis. J. D. McCallum and R. L. Litle, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 9:20 Ultraviolet Photometric Standards. W. S. Gallaway, A. C. Roddan, and N. Shifrin, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 9:40 Electronic Spectra of Alkyl-Substituted Phenethylamines. Louis A. Strait and Michael K. Hrenoff, Spectrographic Laboratory, School of Pharmacy, University of California, San Francisco, Calif. 94122 10:00 Quantitative in Situ Determination of TLC Spots by Reflectance Spectrophotometry. Jurg Meier and Eugen Felber, Analytical Department, Cl BA Ltd., Basle, Switzerland 10:40 Determination of Anionic Surfactants in Water. B. W. Bailey, J. M. Rankin, and R. Weinbloom, N.Y.S. Department of Health, Division of Laboratories and Research, Albany, N. Y. 12201 11:00 Solvent Extraction and Photometric Determination of Nitrite with Some Aromatic Ortho Diamines. Eyih Lin and K. L. Cheng, Department of Chemistry, University of Missouri, Kansas City, Mo. 64110 11:20 Dynamic Relationships in Automatic Cuvette Fillers. Jerome A. Majesty, John J. J. Staunton, and Ronald J. Benedict, Coleman Instruments Division of Perkin-Elmer Corp., Maywood, III. 60153

SYMPOSIUM: MOLECULAR SPECTROSCOPY OF MINERALS AND RELATED INORGANICS Wednesday Morning

John R. Ferraro, Presiding

Infrared Spectroscopic Determination of Minerals in Coal and Coal Products. Patricia A. Estep, John J. Kovach, Edward E. Childers, and Clarence Karr, Jr., Morgantown Coal Research Center, Bureau of Mines, U. S. Department of the Interior, Morgantown, W. Va. 26505 9:30 Interaction of Zeolites with Propyl Chloride. C. L. Angell, Union Carbide Research Institute, Tarrytown, N. Y. 10591

9:00


Pittsburgh Conference 10:00 High-Temperature Sorption of Water on Clay Mineral Surfaces. James V. Kennedy, Mellon Institute, Pittsburgh, Pa. 15213; William T. Granquist and Alan C. Wright, Baroid Division, National Lead Co., P. O. Box 1675, Houston, Tex. 77001 10:45 IR Characterization of Water and Hydroxyl Ion in Moon-Milk Minerals. William B. White, Materials Research Laboratory, The Pennsylvania State University, University Park, Pa. 16802 11:15 Infrared Studies of Proton Delocalization in Kalcinite. Joe L. White, Anitra Laycock, and Maribel Cruz, Department of Agronomy, Purdue University, Lafayette, Ind. 47907 11:45 Perturbation of Stretching Vibration of OH Groups in Phyllosilicates by Interlayer Cations. M. Fernandez and J. M. Serratosa, Instituto De Edafologia Y Biologia Vegetal, C.S.I.C., Madrid, Spain, and W. D. Johns, Washington University, St. Louis, Mo.

ANALYSIS FOR WATER AND AIR POLLUTANTS C. Ellen

Wednesday Morning

Gonter, Presiding

Extension of Microcoulometric Determination of Total Bound Nitrogen in Hydrocarbons and Water: 0.1 PPM to 1% Nitrogen. R. T. Moore, R. J. Joyce and M. E. Riddle, Dohrman Instrument Co., 1062 Linda Vista Ave., Mountain View, Calif. 94040; R. L. lannacone, Cities Service Oil Co., Drawer 2, Cranbury, N. J. 08512; Y. Takabashi, Loenco, Inc., 1062 Linda Vista Ave., Mountain View, Calif. 9:20 Determination of Nanogram to Microgram Amounts of Organically Bound Chlorine in Hydrocarbons and Water: 0.2 PPM to 1000 PPM Chlorine. R. J. Joyce, R. T. Moore, and M. E. Riddle, Dohrman Instrument Co., 1062 Linda Vista Ave., Mountain View, Calif. 94040; R. L. lannacone, Cities Service Oil Co., Drawer 2, Cranbury, N. J. 08512 9:40 Simultaneous Determination of Inorganic Water Pollutants by Atomic Absorption and Flame Emission Spectroscopy. Jae Y. Hwang and Fredric J. Feldman, Applications Laboratory, Instrumentation Laboratory, Inc., 113 Hartwell Ave., Lexington, Mass. 02173 10:00 Indirect Chelometric Method for Sulfate. T. C. Woodis, Jr., F. J. Johnson, and J. M. Cummings, Jr., Division of Chemical Development, Tennessee Valley Authority, Muscle Shoals, Ala. 35660 10:40 Devices for Preparing Low-Level Gas Mixtures. Aaron J. Martin, Marlabs, Inc., Kennett Square, Pa. 19348; Gerald R. Umbreit, Greenwood Laboratories, Chadds Ford, Pa. 19317; Fredrick J. Debbrecht, Analytical Instrument Development, Inc., West Chester, Pa. 19380 11:00 Analytical Applications of Low-Level Gas Mixtures. Frederick J. Debbrecht and Edward M. Neel, Analytical Instrument Development, Inc., West Chester, Pa. 19380; Aaron J. Martin, Marlabs, Inc., Kennett Square, Pa. 19348 11:20 Mutual Comparisons of Five Spectrophotometric Methods for Determination of Ozone in Air, in Order to Determine Stoichiometry of Reactions with Ozone. G. Bergshoeff, Research Institute for Public Health and Engineering TNO, Division for Analytical Chemistry, Postbox 214, Delft, The Netherlands

9:00

SYMPOSIUM

ANALYTICAL CHEMISTRY—A FADING DISCIPLINE? Wednesday Morning

Foil A. Miller, Presiding

9:00 Yes!. M. Kent Wilson, Head, Chemistry Section, National Science Foundation, 1800 G St. N.W., Washington, D. C. 20550 9:30 No!. W. Wayne Meinke, Chief, Analytical Chemistry Division, National Bureau of Standards, Washington, D. C. 20234 10:00 View of Practicing Analytical Chemist in Industry. William A. Straub, United Steel Corp., Applied Research Laboratory, 125 Jamison Lane, Monroeville, Pa. 15146 10:30 View of Department Chairman. Frederick R. Duke, Chairman, Department of Chemistry, The University of Iowa, Iowa City, Iowa 52240 11:00 Analytical Chemistry in Universities—Present and Future. David N. Hume, Department of Chemistry, Massa58 A

•

chusetts Institute of Technology, 77 Massachusetts Ave., Cambridge, Mass. 02139 11:30 Training of Chemists: Supply and Demand. George H. Morrison, Department of Chemistry, Cornell University Ithaca, N. Y. 14850 12:00 Objectives and Realities in Analytical Chemistry. S P. Cram, Department of Chemistry, University of Florida! Gainesville, Fla. 32601

(End of Symposium)

CHROMATOGRAPHY—GAS AND LIQUID Wednesday Morning

a. E. Kostyo, Presiding

9:00 New Liquid Chromatograph. Karl J. Bombaugh, R. N. King, and A. J. Cohen, Waters Associates, Inc., 61 Fountain St., Framingham, Mass. 01701 9:20 Significance of Gradient Elution in High-Speed Liquid Chromatography. Robert Stevenson, Dennis Gere, and Kervin Harrison, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598 9:40 Application of High-Speed Liquid Chromatography to Analyses of Dyes and Dye Intermediates. R. J. Passarelli and E. S. Jacobs, Research and Development Division, Jackson Laboratory, Organic Chemicals Department, E. I. du Pont de Nemours & Co., Wilmington, Del. 19899. 10:00 Rapid Separation and Determination of Metal Chelates by Column Liquid Chromatography Using EV-Detector. J. F. K. Huber and J. C. Kraak, Lab of Analytical Chemistry, University of Amsterdam, and H. Veening, Bucknell University, Lewisburg, Pa. 17837 10:40 Some New Applications for New Hewlett-Packard Phosphorus Detector. J. L. Bernard and J. V. Wisniewski, Hewlett-Packard Co., Avondale Division, Route 41 and Starr Road, Avondale, Pa. 19311 11:00 Apparatus and Procedure to Reduce Impurities in Helium to Less Than One Part per Billion. C. A. Seitz, W. M. Bodine, and C. L. Klingman, Helium Research Center, Bureau of Mines, U. S. Department of Interior, P. O. Box 10085, Amarillo, Tex. 79106 11:20 Quantitative Gas Chromatography: A Practical Reaction Coulometer Detector. Karl-Dieter S. Myrenne, Melabs, Inc., 3300 Hillview Ave., Palo Alto, Calif. 94304 11:40 Reaction Coulometer as Absolute Standard for Calibration of Flame Ionization Detector in Gas Chromatography. Anthony B. Littlewood, School of Chemistry, The University, Newcastle-upon-Tyne, England NE1 7RU, and W. Antony Wiseman, Reaction Coulometers Ltd., Boyn Valley Road, Maidenhead, Berks, England

VISIBLE SPECTROPHOTOMETRIC ANALYSES AND MICROBALANCE Wednesday Afternoon

J. A. Queiser, Presiding

2:00 Rapid Spectrophotometric Determination of Trace Vanadium in Titanium Tetrachloride. N. Curtis Radcliffe and James R. Parker, PPG Industries, Chemical Division, P. 0. Box 191, New Martinsville, W. Va., 26155 2:20 Spectrophotometric Investigation of Formation of 12-Molybdosilica Acid. L. G. Hargis, Louisiana State University in New Orleans, La. 70122 2:40 Spectrophotometric Compositional Analysis of Tantalum-Aluminum Alloy Films. F. Huber and D. Jaffe, Bell Telephone Laboratories, Inc., 555 Union Blvd., Allentown, Pa. 18103 3:00 Simultaneous Spectrophotometric Determination of Cobalt, Nickel and Copper with 2,3-Quinoxalinedithiol. R. W. Burke and E. R. Deardorff, Analytical Chemistry Division, National Bureau of Standards, Washington, D. C. 20234 3:40 Analysis of Copper-Based Alloys by High-Precision Automatic Spectrophotometry. P. Johns and W. J. Price, Pye Unicam Ltd., Cambridge, England 4:00—Trace Determination of Iron Using New Spectrophotometric Reagent. Lawrence Stookey, Hach Chemical Co., 713 South Duff, Ames, Iowa 50010 4:20 Recent Developments in Microbalance. D. C. Tappin, Beckman R.I.I.C., Worsley Bridge Road, London, S.E. 26, England


Pittsburgh Conference STEEL ANALYSIS Wednesday Afternoon

SSP AWARD SYMPOSIUM W. A. Straub, Presiding

Frank E. Dickson, Presiding

Wednesday Afternoon

2:00 Spectrophotometric Determination of Vanadium in Steels as /3-lsopropyltropolone Complex. Oscar Menis and C. S. P. Iyer, Analytical Chemistry Division, National Bureau of Standards, Washington, D. C. 20234 2:20 Determination of Sulfur and Phosphorus in Low Alloy Steels with Aerosol Generator/Capillary Arc Source. Charles H. Anderson, T. H. Zink, and A. L. Davison, Applied Research Laboratories, 9545 Wentworth Ave., Sunland, Calif. 91040 2:40 Rapid Combustion-Spectrophotometric Method for Determination of Sulfur in Silicon Iron, Nickel Iron, and Related Alloys and Materials. R. B. Fricioni and M. A. McMahon, Allegheny Ludlum Steel, Research Center, Brackenridge, Pa. 15014 3:00 Consolidated Automated Determination of Silicon in Iron Ores, Sinters, Slags, or Iron and Steel. Om P. Bhargava, George F. Pitt, and W. Grant Hines, The Steel Co. of Canada, Ltd., Chemical & Metallurgical Laboratories, Wilcox St., Hamilton, Ont., Canada 3:40 Evaluation of Leco 589-800 Automatic Nitrogen Analyzer. R. W. Cline, H. S. Karp, and L. M. Melnick, U. S. Steel Corp., Applied Research Laboratory, 125 Jamison Lane, Monroeville, Pa. 15146 4:00 Determination of Nitrides in Cast Steel. D. G. Swinburn and P. J. Melia, Steel Casters Research and Trade Association, East Bank Road, Sheffield, England 4:20 On Difference between Analytical Values of Oxygen in Iron Obtained by Vacuum Fusion Method and IodineMethanol Method. M. Ihida, S. Tsuchida, and T. Ishii, Technical Research Center, Nippon Kokan Kabushiki Kaisha, Kawasaki, Japan 4:40 Modified Coulter Counter for Determining Size Distribution Macroinclusions in Plain-Carbon Steels. D. A. Flinchbaugh, Homer Research Laboratories, Bethlehem Steel Corp., Bethlehem, Pa. 18016

SPECTROSCOPY SOCIETY OF PITTSBURGH 1970 AWARD

2:00 Presentation of 1970 SSP Award. Frank E. Dickson, Chairman, Spectroscopy Society of Pittsburgh to PROFESSOR ELLIS R. LIPPINCOTT, UNIVERSITY OF MARYLAND, COLLEGE PARK, MD.

AWARD ADDRESS:

POLYWATER AND RELATED MATERIALS

3:30 Laser Raman Spectroscopy of Amorphous Glasses and Polymers. Marvin C. Tobin, Perkin-Elmer Corp., 50 Danbury Rd., Wilton, Conn. 06852. 4:00 Vibrational Spectra and Structures of Haloacetic Acids. J. E. Katon and T. P. Caril, Miami University, Oxford, Ohio 45056 4:30 Torsional Vibrations. W. G. Fateley, Carnegie-Mellon University, Pittsburgh, Pa. 15213 THERMAL METHODS—POLYMERS AND GENERAL APPLICATION Jack Koenig, Presiding

Wednesday Afternoon

2:00 Application of New Flame Ionization Thermal Analyzer to Total Organic Analysis. W. H. Butz and A. C. Stapp, Carle Instruments, Inc., 1141 East Ash Ave., Fullerton, Calif. 92631 2:20 Extension of Thermal Mechanical Analysis to Measurement of Samples in Tension. Paul F. Levy, Gerald W. Miller, and Donald L. Casey, E. I. du Pont de Nemours & Co., Instrument and Equipment Division, Wilmington, Del. 19898

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2:40 Dilatometric Accessory for Use with Thermal Mechanical Analyzer to Allow Rapid Determination of Volume Coefficients of Expansion. Paul F. Levy, Gerald W. Miller, Donald L. Casey, and Andrew A. Loehr, E. I. du Pont de Nemours & Co., Instrument and Equipment Division, Wilmington, Del. 19898 3:00 New EGA System with True Flow Through Capability. Abund O. Wist, 155 Longuevue Dr., Pittsburgh, Pa. 15228 3:40 Thermogravimetry of Epoxy Resin Systems. Thomas Gedemer and James Gahl, Materials Application Laboratory, McGraw-Edison Power Systems Division, 2700 Ninth Ave., South Milwaukee, Wis. 53172 4:00 Applications of Concurrent Differential Thermal and Amperometric Thermal Analysis. D. J. David, Tracor, Inc., Analytical Instruments Division, 6500 Tracor Lane, Austin, Tex. 78721 4:20 Heat Loss Influence in Differential Scanning Calorimetry. Abund O. Wist, 155 Longuevue Dr., Pittsburgh,

3:00 Partially Resolved GC Peaks: Analytical Accuracy with Electronic Integrator. Louis Mikkelsen, Hewlett-Packard Co., Avondale, Pa. 19311 3:40 Simple Automatic Single Component Analyzer Based on Gas Chromatography. Raymond Annino, The Foxboro Co., Research Center, Neponset Ave., Foxboro, Mass. 02035 4:00 On-Site Chromatographic Analysis. Fredrick J. Debbrecht and Edward M. Neel, Analytical Instrument Development, Inc., 250 South Franklin St., West Chester, Pa., 19380 4:20 Fast On-Line Gas Chromatograph Analysis of Hz, O,, and C02 in Off Gas from Reactor Experiment. J. L. Power, NASA Lewis Research Center, Cleveland, Ohio 44135 4:40 High-Speed Gas Chromatographic Separations of High-Molecular Weight 0-Deketones Under Conditions of Time Normalization. R. W. McCoy and S. P. Cram, University of Florida, Department of Chemistry, Gainesville, Fla. 32601 .

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4:40 Determination of Isothermal Polymer Properties Using Thermal Mechanical Analyzer. David Machin and C. E. Rogers, Case Western Reserve University, Cleveland, Ohio 44106

INFRARED SPECTROSCOPY INSTRUMENTATION AND TECHNIQUES

GAS CHROMATOGRAPHY—APPARATUS AND ACCESSORIES

New Matrix Temperature Programmer. U. Christen, D. Guidinger, and S. Karageorge, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598. 2:20 Gas Chromatographic Performance with New Matrix Temperature Programmer. B. E. Wadsworth and C. H. Hartmann, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598 2:40 Automatic Sampler-Injector for GC Analysis. Gene E. Lightner and John Poole, Hewlett-Packard Co., Avondale, Pa. 19311

2:00

"first

J. F. Jackovitz, Presiding

Thursday Morning

A. J. Kavoulakis, Presiding

Wednesday Afternoon

THURSDAY, MARCH 5

Internal Reflection Spectroscopy: Reflection Plates 9:00 for Microsampling. N. J. Harrick, Harrick Scientific Corp., P. O. Box 867, Ossining, N. Y. 10562 9:20 Gas Chromatography—Infrared Accessory with InLine Enrichment. A. C. Gilby, Wilks Scientific Corp., P. O. Box 441, South Norwalk, Conn. 06856 9:40 Silver Chloride Encapsulation—New Approach to Infrared Sample-Handling. Gregory D. Propster, Barnes Engineering Co., 30 Commerce Rd., Stamford, Conn. 06904 10:00 Authentication of Valuable Printed Matter by Internal Reflection Infrared Spectroscopy. Paul A. Wilks, Jr., Wilks

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Scientific Corp., P. O. Box 441, South Norwalk, Conn. 06856 10:40 New Double-Beam Infrared Spectrophotometer. M. Lu and S. L. Pratt, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 11:00 Application of Fourier Transform Spectroscopy to On-Line Spectral Measurement of GC Peaks. J. O. Lephardt and P. R. Griffiths, Block Engineering, Inc., 19 Blackstone St., Cambridge, Mass. 02139 11:20 High-Temperature, High-Vacuum Cell for Infrared Surface Studies. G. L. Haller, Mason Laboratory, Yale University, New Haven, Conn., and A. C. Gilby, Wilks Scientific Corp., P. O. Box 441, South Norwalk, Conn. 06856

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ION-SELECTIVE ELECTRODES AND RELATED ELECTROCHEMICAL SENSORS Thursday Morning

R. T.

Oliver, Presiding

Improved Reference Electrode for Continuous Process Measurement. Truman S. Light, The Foxboro Co., 38 Neponset Ave., Foxboro, Mass. 02035 9:20 Continuous Measurement of Water Hardness Using Ion Selective Electrode. Richard T. Oliver and Richard F. Mannion, The Foxboro Co., 38 Neponset Ave., Foxboro, Mass. 02035 9:40 Low-Level Sodium Ion Measurement with Glass Electrode. Edgar L. Eckfeldt and William E. Proctor, Jr., Leeds & Northrup Co., Corporate Research Department, North Wales, Pa. 19454 10:00 Application of Electrochemical Sensors for Controlling Flowing Systems. E. Pungor, K. Toth, I. Gavaller, Z. Feher, and G. Nagy, Department of Analytical Chemistry, University of Chemical Industries, Veszprem, Schonherz Z.u.12, Hungary 10:40 Use of Selective Ion Electrodes in Food Industry. Clark Westcott and Theron Johns, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 11:00 Semiconductor Electrodes for Measurement of Acid Concentrations. J. P. McKaveney, Garrett Research & Development Co., Inc., Division of Occidental Petroleum Corp., La Verne, Calif. 91750, and C. J. Byrnes, Crucible Steel Division, Colt Industries, Pittsburgh, Pa. 15230 11:20 Recent Developments in Field of Solid State Ion Selective Electrodes. Gerard M. Farren, Coleman Instruments Division of Perkin-Elmer Corp., Maywood, III. 60153 11:40 Differential Potentiometry with Ion Selective Electrodes. M. J. D. Brand and G. A. Rechnitz, Department of Chemistry, State University of New York at Buffalo, Buffalo, N. Y. 14214

9:00

COMPUTER SYSTEMS FOR ANALYTICAL CHEMISTRY Thursday Morning

Paul Coulter, Presiding

9:00 Computer Data Acquisition in Research Laboratory. C. E. Klopfenstein, University of Oregon, Department of Chemistry, Eugene, Ore. 97403 9:20 Distributed Computing Network for Analytical Laboratory. R. T. Barck and R. Katzive, Varian Associates, Graphics & Data Systems Division, 611 Hansen Way, Palo Alto, Calif. 94303 9:40 Sensitivity and Reproducibility of Feature Detection in Real-Time Automated Laboratory Data Reduction. J. F. Muldoon and W. R. Lund, Electronic Associates, Inc., 185 Monmouth Parkway, West Long Branch, N. J. 07764 10:00 Improved Computer Facilities for Laboratory Environment. B. D. Franza, C. H. Sederholm, and R. J. Wiley, IBM DACS Development Center, 2670 Hanover St., Palo Alto, Calif. 94304

Readers’ Service Card

ANALYTICAL CHEMISTRY, VOL, 42, NO. 2, FEBRUARY 1970

Pittsburgh Conference Standard Digital Interface for Analytical Instruments. Perkin-Elmer Corp., Main Ave., Norwalk, Conn. 06852 11:00 Literal Language for Laboratory Automation. F. W. Chambers and A. Bednowitz, IBM T. J. Watson Research Center, P. 0. Box 218, Yorktown Heights, N. Y. 10598 11:20 CLASS—Computer Language for Spectroscopy. R. B. Cook and R. W. Wolfe, Cary Instruments, Monrovia, Calif., and W. H. Holt, Software Associates, Inc., Arcadia, Calif.

Department of Chemistry, Wichita State University, Wichita, Kan. 67208

10:40

G. T. Paul, The

MASS SPECTROMETRY Thursday Morning

A. G. Sharkey, Jr., Presiding

9:00

Analytical Capabilities of Ion Microprobe Mass Analyzer. T. A. Whatley, Applied Research Laboratories, P. O. Box 129, Sunland, Calif. 91040 9:20 Extranuclear Modulated Beam Analytical Mass Spectrometer (EMBA-II). R. T. Brackmann, W. L. Fite, E. O’Malley, and J. A. Peden, Extranuclear Laboratories, Inc., P. O. Box 11512, 324 Freeport Rd., Pittsburgh, Pa. 15238 9:40 Phase Spectrometry Using EMBA-II; Ultrafast Gas Chromatography. J. A. Peden, W. L. Fite, and R. T. Brackmann, Extranuclear Laboratories, Inc., P.O. Box 11512, 324 Freeport Rd., Pittsburgh, Pa. 15238 10:00 Simple Partial Pressure Analyzer. J. W. Hedman, AMBS-Development Engineering, General Electric Co., 25 Federal St., Lynn, Mass. 01905 10:40 Improved Universal Type Mass Spectrometer Hitachi Perkin-Elmer Model RMU-6L. Y. Nakajima, T. Shiratori, M. Fukuchi, and H. Sato, Hitachi Naka Works, Ichige, Katsutashi, Ibaraki-ken, Japan 11:00 Chemical Techniques for Spark Source Mass Spectrometry. Robert Alvarez, Paul J. Paulsen, and Charles W. Mueller, National Bureau of Standards, Washington, D. C. 20234 11:20 Mass Spectral Study of Some Thallium(l) Dithiocarbamates. Vernon 0. Brandt and Robert Christian, Jr.,

SYMPOSIUM ON HIGH-SPEED CHROMATOGRAPHIC ANALYSIS Thursday Morning

R. W.

Freedman, Presiding

9:00 General Theory of Elution Chromatography Applied to Column Liquid Chromatography. J. F. K. Huber, Laboratory of Analytical Chemistry, University of Amsterdam, Nieuwe Achtergracht 125, Amsterdam, Holland 9:40 High-Performance Liquid Chromatography. Osaba Horvath, Yale University, New Haven, Conn. 10:40 High-Speed Liquid Chromatography Using Surfaced Textured Glass Beads. Barry L. Karger, Heinz Engelhardt, and Kenneth Conroe, Department of Chemistry, Northeastern University, Boston, Mass. 02115 11:20 High-Pressure Ion Exchange Chromatography as Applied to Body Fluids Analyses. Charles D. Scott, Body Fluids Analyses Group, Oak Ridge National Laboratory, Oak Ridge, Tenn. ELECTROCHEMISTRY Thursday Afternoon

Arthur

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64 A

•

Greene, Presiding

2:00 Complex System Studies by Application of Multifunctional Electrochemical Instrumentation. J. B. Flato and M. R. Hackman, Princeton Applied Research Corp., P. O. Box 565, Princeton, N. J. 08540 2:20 Kinetic Studies on Fast Oxidation-Reduction Reactions by Application of Precise Potential-Limited Cyclic Voltammetry. J. B. Flato and M. R. Hackman, Princeton Applied Research Corp., P. 0. Box 565, Princeton, N. J. 08540 2:40 Fast and Accurate Conductance Technique. D. E. Johnson and C. G. Enke, Department of Chemistry, Michigan State University, East Lansing, Mich. 48823 Edward P. Kujawa, Brinkmann 3:00 Electroiodination. Instruments, Inc., Cantiague Road, Westbury, N. Y. 11590 (Continued on page 69 A)


Mich.


3:40 Diffusion Coefficients of Ferri- and Ferrocyanide Ions, Using Twin-Electrode Thin Layer Cell. Stanley J. Konopka and Bruce McDuffie, State University of New York at Binghamton, Department of Chemistry, Binghamton, N. Y. 13901 4:00 Rapid Scan Anodic Stripping. Joseph E. Nelson, Chemtrix, Inc., P. O. Box 725, Beaverton, Ore. 97005 4:20 Pyrophosphate Determination via Cathodic Currents at Lead Dioxide Electrode. C. O. Huber and K. E. Grant, Department of Chemistry and Laboratory for Surface Studies, University Wisconsin—Milwaukee, Wis. 53201 4:40 Pulse Polarographic Study of Ytterbium in Presence of Nitrate and Simultaneous Determination of Europium, Lead, Ytterbium and Zinc. D. P. Sandoz, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598; J. W. McLaughlin, R. Z. Bachman, and C. V. Banks, Institute for Atomic Research and Department of Chemistry, Iowa State University, Ames, Iowa 50010 SYMPOSIUM ON COMPUTERS IN ANALYTICAL CHEMISTRY L. R. Cousins,

Thursday Afternoon

GAS CHROMATOGRAPHY—TECHNIQUES 3:40 Analysis of Nonvolatile Organic Materials by Curie Point Pyrolysis Gas Chromatography. L. C. Culpepper, R. E. Schavey, and M. McKeown, Packard Instrument Co., 2200 Warrenville Rd., Downers Grove, III. 60515 4:00 Chlorinated Pesticide Residue Analysis of Spinach Extracts Using Silicic Acid-Glass Fiber Sheet Instead of Usual Florisil Column for Cleanup Operation. Thomas H. Beasley, Sr., and Howard W. Ziegler, Mallinckrodt Chemical Works, Box 5439, St. Louis, Mo. 63160. 4:20 Controlled Thermolytic Dissociation of Hexadecane and Methyl Decanoate. Herbert Groenendyk, Technische Hogeschool Eindhoven, Netherlands; Eugene J. Levy, Chemical Data Systems, Oxford, Pa. 19363, and Stanley F. Sarner, University of Delaware, Newark, Del. 19711 4:40 Gas Chromatographic System of Automated Atmosphere Analysis. R. C. Frink, D. J. David, F. R. Dumbeck, J. R. Sebesta, and L. E. Philyaw, Tracor, Inc., Analytical Instruments Div., 6500 Tracor Lane, Austin, Tex. 78721

Presiding

DENDRAL: Approach to Mass Spectrometry through Artificial Intelligence. Bruce G. Buchanan, Stanford University, Stanford, Calif. 94305 Modes of Computer Automation in Chemistry Lab2:35 oratory. Jack W. Frazer, Lawrence Radiation Laboratory, University of California, Livermore, Calif. 94550 3:30 Computer Aided Evaluation of Instrument PerforA. Savitzky, R. W. Hannah, and W. B. Barnett, mance. The Perkin-Elmer Corp., Norwalk, Conn. 06852 4:05 Generalized System for Automation of Laboratory InL. Frost and O. F. Gerster, Digital Applications, struments. Inc., 866 Third Ave., New York, N. Y. 10022

FRIDAY, MARCH 6

Heuristic

2:00

COBLENTZ SOCIETY SYMPOSIUM Raman Spectroscopy Charles Angell, Presiding

Thursday Afternoon

1:30 Introductory Remarks, Charles Angell Presentation of the 1970 Coblentz Award. Dr. Charles Angell, President, The Coblentz Society, Inc. to PROFESSOR JAMES R. DURIG, DEPARTMENT OF CHEMISTRY, UNIVERSITY OF SOUTH CAROLINA,

COLUMBIA, S. C. 1:45 AWARDEE PAPER—Anharmonic Vibrations in Far Infrared Spectroscopy. James R. Durig 2:45 Raman Intensities and Bond Polarizability Model. R. G. Snyder, Shell Development Co., Emeryville, Calif. 94608 3:30 Laser Raman Studies on Biological Polymer Molecules. Warner L. Peticolas, Department of Chemistry, University of Oregon, Eugene, Ore. 97403 4:15 Raman Spectroscopy of Liquids and Oriented Crystalline Solids at High Pressure. Alvin J. Melveger, Allied Chemicals, Morristown, N. J. 07960 SYMPOSIUM ON HIGH-SPEED CHROMATOGRAPHIC ANALYSIS J. Carter, Presiding

Stationary Phases of High Order in Chromatography. Halasz, Institut Fur Physikalische Chemie, der Universitat, Frankfurt-Am-Main 1, Robert-Mayer-Strasse 11, West Germany 2:40 Factors Effecting Speed of Gas Chromatographic Separations. L. S. Ettre, Snell-Ettre Encyclopedia of Industrial Chemical Analysis, 345 Westchester Ave., Port Chester, N. Y. 10573 (End of Symposium) 2:00 I.

GENERAL MEETING—COBLENTZ SOCIETY Sheraton-Cleveland Hotel Thursday, March 5, 8:00 P.M.

Friday Morning

G. L.

Carlson, Presiding

9:00 Diffuse Reflectometer for 4 to 40/t Region. Gerhart J. Kneissl and S. Thomas Dunn, Dunn Analytical Division of Block Engineering, Inc., 3829 Plyers Mill Rd., Kensington, Md.20795 9:20 Infrared Spectra of Amino Acids and Simple Polypeptides to 33 Cirr1 at Room and Liquid Nitrogen Temperatures. W. R. Feairheller, Jr. and J. T. Miller, Jr., Monsanto Research Corp., Dayton, Ohio 45407, and F. F. Bentley, Wright-Patterson Air Force Base, Ohio 45433 9:40 Methyl Torsional Frequencies and Barriers to Internal Rotation. J. R. Durig, S. M. Craven, and J. Bragin, Department of Chemistry, University of South Carolina, Columbia, S. C. 29208 10:00 Vibrational Spectrum of Trifluoroacetyl Fluoride. C. V. Berney and A. D. Cormier, University of New Hampshire, Durham, N. H. 03824 10:40 Laser Raman Spectroscopy as Analytical Tool. James R. Allkins and Donald O. Landon, Spex Industries, Inc., 3800 Park Ave., Metuchen, N. J. 08840 11:00 Analytical Raman Spectroscopy. II. Intensity Considerations. Howard J. Sloane and Herbert S. Haver, Cary Instruments, 2724 South Peck Rd., Monrovia, Calif. 91016 11:20 Application of Laser-Raman Spectroscopy to Organic Chemistry. V. Characterization of Carbonyl Compounds by Means of Depolarization Data. Stanley K. Freeman, International Flavors & Fragrances, Research Center, Union Beach, N. J., and Dana W. Mayo, Chemistry Department, Bowdoin College, Brunswick, Me. 11:40 Raman Spectra of Some Polynuclear Aromatic Solids. Toru Yokoyama, R&D Division, Japan Electron Optics Laboratory Co., Ltd., Akishima, Tokyo, Japan, and Mitsuo Ito, The Institute for Solid State Physics, The University of Tokyo, Tokyo, Japan NEW DIRECTIONS IN TITRIMETRY

(Continued) Thursday Afternoon

INFRARED AND LASER RAMAN SPECTROSCOPY

Whitehall Room

Friday Morning

Gerrit Dragt, Presiding

9:00 Photochemical Titrations of Fluorescent Metal-Ion Chelate Complexes. J. L. Beck, J. A. Bishop, and J. M. Fitzgerald, University of Houston, Department of Chemistry, Houston, Tex. 77004 9:20 Development and Performance of "Aquatest,” Coulometric Karl Fischer Titrator. Gabor B. Levy, Joseph Williams, and David M. Seltzer, Photovolt Corp., 1115 N. Y. 10010 Broadway, New York, 9:40 New Enthalpimetric Analyzer. Joseph Jordan and Neil D. Jespersen, Department of Chemistry, Pennsylvania State University, University Park, Pa. 16802; Richard M. Reich, Herbert M. Cullis, and C. David Miller, American Instrument Co., 8030 Georgia Ave., Silver Spring, Md. 20910 10:40 New Automatic Karl Fischer Titrator. E. A. Berry and J. W. Haagen-Smit, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634 11:00 Microdetermination of Water with New Karl Fischer Titrator. Philip Ting and Theron Johns, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634


.

69 A

Pittsburgh Conference 11:40 Computerized Peak Identification of Complex Chromatographic Data. D. E. Seizinger and C. J. Raible, Bartlesville Petroleum Research Center, Bureau of Mines, Department of Interior, Bartlesville, Okla. 74003

11:20 Determination of Trace Nitrogen in Plutonium— Uranium Oxide Nuclear Fuel Materials by the Kjeldahl Method, with Constant-Current Coulometric Titration. E. J. Cokal and D. H. Schmitt, The Babcock & Wilcox Co., Nuclear Development Center, Lynchburg, Va. 24505 11:40 Improved Methods for Analysis of Water in Paper and Pulp. A. T. Giammarise, J. L. Holman, and J. J. Short, Xerox Corp., Xerox Square, W-103, Rochester, N. Y.

MEETING TO ORGANIZE SOCIETY FOR INDUSTRIAL ANALYTICAL CHEMISTS ROOM 217 A & B FRIDAY, 9:30 A.M.

INTERFACING COMPUTERS AND GAS CHROMATOGRAPHS Friday Morning

F. E.

S. Shankman, Convener

Lutinski, Presiding

9:00 Multiuser Gas Chromatography Data System with Foreground-Background Processing. Jo-L Hendrickson, David L. Wallace, and Frederick Baumann, Varian Aerograph, 2700 Mitchell Dr., Walnut Creek, Calif. 94598 9:20 Improved Method for Fused Peak Decomposition in Gas Chromatograms. D. L. Cameron, G. M. Markham, C. H. Sederholm, C. E. Walker, and D. H. Wilkinson, IBM DACS Development Center, 2670 Hanover St., Palo Alto, Calif. 94304 9:40 On-Line GLC System Designed for IBM 1130 Computer. D. A. Craven, E. S. Everett, and M. Rubel, International Flavor & Fragrances, 1515 Highway 36, Union Beach, N. J. 07735 10:00 Advances in Off-Line Automation for Small Laboratory. Jack M. Gill and James Hubbard, Vidar Corp., Autolab Division, 77 Ortega, Mt. View, Calif. 94040 10:40 Low-Cost Time-Share Data Reduction for Gas Chromatographer. Harold Shira, Hewlett Packard, Avondale, Pa. 19311 11:00 Software Oriented Data Processing and Control System for Gas Chromatographs. B. D. Brook and B. J. Richardson, Pye Unicam Ltd., York St., Cambridge, England 11:20 Computer Simulation of Chromatographic Band and Broadening Processes. T. H. Glenn and S. P. Cram, University of Florida, Department of Chemistry, Gainesville, Fla. 32601

FOR FURTHER INFORMATION, CONTACT S. Shankman 2023 South Santa Fe Ave. Los Angeles, Calif. 90021

GAS CHROMATOGRAPHY—DETERMINATIONS Helen Lang, Presiding

Friday Morning

9:00 GC Determination of Nitrogen Oxides in Air. A. Lawson and H. G. McAdie, Department Physical Chemistry, Ontario Research Foundation, Sheridan Park, Ont., Canada 9:20 Determination of Corrosive Gases by Gas Chromatography: Separation of Oa N2, CO, C02, HCI, COS, CL, S02, and COCL- James A. McKowen and James R. Parker, PPG Industries, Chemical Division, P. O. Box 191, New Martinsville, W. Va. 26155 9:40 Quantitative Determination of Trace Amounts of Antioxidants in Acrylic-Type Monomers by Gas Chromatography. Manuel H. Ehrlich, Jr., Sartomer Resins, Inc., Essington, Pa. 19029 10:00 Gas Chromatographic Analysis of TNT from ContinuR. W. Dalton, J. A. Kohlbeck, and W. T. ous Process. Bolleter, Hercules, Inc., Radford Army Ammunition Plant, Radford, Va. 24141

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Gas Chromatographic Determination of Selenium. James W. Young and Gary D. Christian, University of Kentucky, Department of Chemistry, Lexington, Ky. 40506 11:00 Isolation and Elimination of Variables Contributing to Peak Broadening in Preparative Chromatography. Roy W. Yost, Nester Faust Manufacturing Corp., Box 565, Newark, Del. 19711 11:20 Determination of PPB Concentrations of Phenol in Water. Gerald R. Umbreit, Rex E. Nygren, and Anthony J. Testa, Greenwood Laboratories, Inc., Chadds Ford, Pa. 19317 11:40 High-Precision Gas Chromatography. R. A. Culp, C. H. Lochmuller, A. K. Moreland, R. S. Swingle, and L. B. Rogers, Purdue University, Department of Chemistry, Lafayette, Ind. 47907

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72 A

•

Jeanette

Grasselli, Presiding

2:00 Lattice Dynamics of KN„. K. R. Rao, H. Prask, and S. Trevino. Explosives Laboratory, F. R. L., Picatinny Arsenal, Dover, N. J., and R. Mical, Boston College, Chestnut Hill, Mass. 02167 2:20 Infrared Spectroscopic Studies of Effects of Pressure on Hydrogen Bonded Molecules. Y. Mikawa and R. J. Jakobsen, Battelle Memorial Institute, Columbus Laboratories, Columbus, Ohio 43201 2:40 Vibrational Spectra and Normal Coordinate Analysis of Carbamate Ion. J. C. Carter and J. E. Devia, Chemistry Department, University of Pittsburgh, Pittsburgh, Pa. 3:00 Group Frequencies of Cyclobutane Compounds. J. E. Katon and Roscoe O. Carter, Miami University, Department of Chemistry, Oxford, Ohio 45056 3:40 Fluorescence Spectroscopy in Study and Control of Water Pollution. S. D. Kullbom, H. F. Smith, and P. S. Flandreau, Perkin-Elmer Corp., Norwalk, Conn. 06852. 4:00 Automotive Exhaust Analyzer for Simultaneous Monitoring of C02, CO, Hydrocarbons, and NO. Gerhart J. Kneissl and Richard B. Kay, Dunn Analytical Instruments Division of Block Engineering, Inc., 3829 Players Mill Road, Kensington, Md. 20795 4:20 Spectrophotometric Method for Determination of Sulfur Dioxide in Atmosphere. B. W. Bailey and W. C. Kelley, N.Y.S. Health Department, Division of Laboratories and Research, Albany, N. Y. 12201 4:40 Spectrophotometric Determination of Formaldehyde in Air. B. W. Bailey and J. M. Rankin, N.Y.S. Health Department, Division of Laboratories and Research, Albany, N. Y. 12201 NUCLEAR MAGNETIC RESONANCE SPECTROMETRY AND COMPUTERS IN SPECTROSCOPY Friday Afternoon

H. L. Retcofsky,

Presiding

2:00 Fluoroanilides. II. laF NMR and Infrared Study. H. Agahigian, Baron Consulting Co., Orange, Conn. 06477; J. Karabinos, Carbolabs, Inc.; J. Barrante, Southern Connecticut College; J. Babiec, New Haven College. 2:20 Cyclosilane-dis and 3-(TrimethylsiIyl)tetradeutero-Sodium-Propionate, Two New Proton-NMR Standards for High B. Hampel, L. Temperatures and Aqueous Solutions. Pohl, and M. Eckle, E. Merck A.G., Darmstadt, Germany, to E. be presented by Gunter Scheuerbrandt, Merck, A.G., 7 Woodlot Lane, Huntington, N. Y., 11743 2:40 NMR Analysis of Mono-, Di-, and Triethanolamines Utilizing Derivatization Techniques. J. Babiec, New Haven College, New Haven, Conn., and H. Agahigian, Baron Consulting Co., Orange, Conn. 06477 3:00 “Telephone Directory” Format for NMR Spectra Retrieval. M. H. Jacobs, L. Van Derslice, and C. Bernier, International Flavors & Fragrances, R & D Center, 1515 Highway 36, Union Beach, N. J. 07735

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Extended Range Infrared File Searching System. D. Computation Research Laboratory, Midland, Mich. 48640 4:00 Automated Chemical Structure Analysis of Organic Compounds. Y. Kudo, S. Ochiai, Y. Ishida, and T. Tanaka, Japan Electron Optics Laboratory; H. Abe, Department of Chemistry, Tohoku University, and S. Sasaki, Miyagi University of Education, Aoba, Sendai, Japan 4:20 Optimum Estimate of Concentrations in Multicomponent Mixtures from Spectrophotometric Data on Computer. R. L. Litle and R. A. Nesbit, Beckman Instruments, Inc., 2500 Harbor Blvd., Fullerton, Calif. 92634

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T. J. Puzniak, Presiding

2:00 Four-Channel Automated System for Chemical Analysis. Herbert L. Kahn and Sabina Slavin, Perkin-Elmer Corp., Main Ave., Norwalk, Conn. 06852 2:20 Direct-Reading On-Line Concentration Printout System for the Auto-Analyzer. Ronald H. Laessig, University of Wisconsin, State Laboratory of Hygiene, 437 Henry Mall, Madison, Wis., and Peter F. Tong, T&T Technology, Inc., 813 Stewart St., Madison, Wis. 2:40 Real-Time Computer Prediction of Endpoints in Controlled Potential Couiometry. F. B. Stephens, F. Jakob, L. P. Rigdon, and J. E. Harrar, Lawrence Radiation Laboratory, P. O. Box 808, Livermore, Calif. 94550 3:00 Real-Time Computerized Reduction and Analysis of Electroanalytical Data. J. B. Flato and G. H. Keats, Princeton Applied Research Corp., P. O. Box 565, Princeton, N. J. 08540 3:40 Some Useful Applications of Computer Data Handling in Differential Scanning Calorimetry. L. R. Scott and A. P. Gray, Perkin-Elmer Corp., Norwalk, Conn. 06852 4:00 Design of Practical Computer System for Data ProBertram R. cessing of Multiple Analytical Instruments. Willoughby and George R. Smith, Electronic Associates, Inc., 185 Monmouth Parkway, West Long Branch, N. J. 07764 4:20 Versatile and Low-Cost On-Line Data Acquisition and Processing System for Mass Spectrometry. Uwe Markwardt, Eberhard Wegner, Karleugen Habfast, Varian Mat GMBH, 28 Bremen 10, Woltmershauser Strasse 442-448a, P. O. Box 4062, West Germany 4:40 Experiences with Variety of Analytical Instruments On-Line to Large Time-Sharing Computer. E. Ziegler, D. Henneberg, and G. Schomburg, Max-Planck-lnstitut fur Kohlenforschung, Mulheim-Ruhr, Germany CH ROMATOGRAPHY—GEN ERAL Friday Afternoon

Box 755, Goleta, California 93017 ( 805 ) 967-0456 •

Meyer, Presiding

2:00 Gas Chromatographic Analysis of Alkoxyl Groups by Sealed Tube Method. C. F. Bradley, L. A. Phifer, and J. L. Bell, FMC Corp., American Viscose Division, Post Road, Marcus Hook, Pa. 19061 2:20 Factors Affecting Linearity of Flame Ionization Detector. L. E. Green and L. Mikkelsen, Hewlett-Packard Co., Avondale, Pa. 19311 2:40 Separation and Identification of Ce Iso- and Cycloparaffins in Straight-Run Gasoline. A. J. Raymond, R. T. Greyson, and T. K. Frasier, Sun Oil Co., P. O. Box 426, Marcus Hook, Pa. 19061 3:00 Applications of High Resolution MS-GC Techniques to Drug Analysis. J. R. Chapman, S. Evans, and D. Hazelby, AEI Scientific Apparatus, Ltd., Barton Dock Rd., Manchester M31, 2LD, England, and W. A. Wolstenholme, Picker Nuclear, 1275 Mamaroneck Ave., White Plains, N. Y. 10605 3:40 Identification and Estimation of Tocopherol and Tocotrienols in Some Vegetable Oils Using Gas-Chromatography-Mass Spectrometry. M. K. Govind, RAO and E. G. Perkins, The Burnsides Research Laboratory, University of Illinois, Urbana, III. 61801 4:00 New Direct-Recording Thin-Layer Detection System. R. S. Evans, L. J. Everett and E. Haahti, Packard Instrument Co., 2200 Warrenville Rd., Downers Grove, III. 60515 4:20 Detection of Pesticides in Situ Fluorescence. Paul E. Belliveau, Victorin N. Mallet, and Roland W. Frei, Department of Chemistry, Dalhousie University, Halifax, Nova Scotia 4:40 Densitometry of Silica Gel Thin-Layer Chromatograms Containing Phosphomolybdic Acid. J. C. Touchstone, T. Murawec, M. Kasparow, and A. K. Balin, University of Pennsylvania, Philadelphia, Pa. 19104


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Nanette

ANALYTICAL CHEMISTRY, VOLi 42, NO. 2, FEBRUARY 1970

ON ANALYTICAL CHEMISTRY AND APPLIED SPECTROSCOPY

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