Oxygen elimination in the direct polarographic determination of trace

pressure in less than 15 min. Capsules with only air sealed inside(contain approximately 90-200 Mg of N) were evacuated and analyzed for nitrogen. The...
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2372

Anal. Chem.

1981,53, 2372-2374

half. The possibility of atmospheric contamination of sample and capsule surfaces, activated by vacuum and/or heat pretreatment, is prevented with the new sampling system, because sample capsules are never exposed to the atmosphere after preanalysis treatment, as they were with the previous sample loading system. This is important in the analysis of samples with low nitrogen concentrations (