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a GE XRD-5 automated diffractom- eter with its b axis ... weight w is 1/ 2(7'0) and c(F0), the standard deviation of F0, is ..... 5..72 (61). C(13). 0...
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C O N T K I B U T I U N FROM 'THE L)BPAKTMEXI. U F CHEMIS1.K'r',

CAKSEOIE-MELLON UNIVERSITY, PITTSBURGH, PENSSVLVASIA 16213

The Crystal and Molecular Structure of trans-C hloro - 2 - (pheny1azo)phenyl bis (triet h ylphosphine)palladium (I I) B Y D. L. WEAVER Keceiued iVo;oeenzber 20, 19/69

T h e structure of the compound ~i.c~ns-chloro-2-(phenylazo)phenylbis(triethy~phosphine)palladium(II), PdCl(C12HgSa)(P(C2HS)3)2, has been determined by single-crystal X-ray diffractometry. This complex crystallizes in the sFace group P21/c (C2h5)with eight molecules in a unit cell of dimensions Q = 19.521 (7) A, b = 16.694 (6) ,