C O N T K I B U T I U N FROM 'THE L)BPAKTMEXI. U F CHEMIS1.K'r',
CAKSEOIE-MELLON UNIVERSITY, PITTSBURGH, PENSSVLVASIA 16213
The Crystal and Molecular Structure of trans-C hloro - 2 - (pheny1azo)phenyl bis (triet h ylphosphine)palladium (I I) B Y D. L. WEAVER Keceiued iVo;oeenzber 20, 19/69
T h e structure of the compound ~i.c~ns-chloro-2-(phenylazo)phenylbis(triethy~phosphine)palladium(II), PdCl(C12HgSa)(P(C2HS)3)2, has been determined by single-crystal X-ray diffractometry. This complex crystallizes in the sFace group P21/c (C2h5)with eight molecules in a unit cell of dimensions Q = 19.521 (7) A, b = 16.694 (6) ,